SavedAdd your journal

Journals / Hittite Journal of Science and Engineering / 2016 / Cilt: 3 - Sayı: 2

Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade and Pekmez

Cemalettin BALTACI
Zeynep AKŞİT
Pages
91–97
Publication Date
2022-10-18
DOI
—
🏛️Bibliographic metadata and full text access for this article are provided via DergiPark.
DergiPark Record ↗
✨

AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

HMF levels in pestil, köme, jam, marmalade and pekmez samples were determined using the validated method

📌 3 Key Takeaways

🎯
Objective & Hypothesis:This study represents a high performance liquid chromatography HPLC method for the detection of 5-hydroxymethylfurfural in pestil, köme, jam and pekmez samples.
📊
Key Findings & Data:The developed method, simple and accurate, showed good recovery values 97-108% .
💡
Conclusion & Impact:HMF levels in pestil, köme, jam, marmalade and pekmez samples were determined using the validated method
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:HMF · Method validation · Pestil

Abstract

This study represents a high performance liquid chromatography HPLC method for the detection of 5-hydroxymethylfurfural in pestil, köme, jam and pekmez samples. The linearity, selectivity, decision limit, detection capability, detection limit, quantification limit, precision, recovery, ruggedness and measurement uncertainty of the method were determined. The developed method, simple and accurate, showed good recovery values 97-108% . The accuracy of the method expressed with the relative standard deviation was below 6%. The detection limit and quantification limit were 0.03 mg/kg and 0.10 mg/kg, respectively. HMF levels in pestil, köme, jam, marmalade and pekmez samples were determined using the validated method

🔖

Cite This Article

BALTACI, C., AKŞİT, Z. (2022). Validation of HPLC Method for the Determination of 5-hydroxymethylfurfural in Pestil, Köme, Jam, Marmalade and Pekmez. Hittite Journal of Science and Engineering, Cilt: 3 - Sayı: 2, 91–97. https://ajindex.com/articles/538094

📄 Full Text PDF Viewer

📄

PDF görüntüleyici hazırlanıyor...

References (15)

  1. Capuano,E. And Fogliano,V. Acrylamide and 5-hydroxymethyl-furfural (HMF), A revieew of metobolosim, toxity, occurrence in food and mitiagtion strategies. LWTFood Sci. Technol., Vol. 44 Pages 793-810. 2011
  2. Teixido, E., Nunez, O., Santos, FJ., Galceren, MT. 5-Hydroxymethylfurfural content in foodstuffs determined by micellar electrokinetic chromatography. Food Chem Vol. 126, Pages 1192, 2011
  3. Spano, N., Casula, L., Panzanelli, A., Pilo, MI., Piu, PC, Scanu, R., Tapparo, A., Sanna, G. A RP-HPLC determination of 5-hydroxymethylfurfural in honey - The case of strawberry tree honey. Talanta Vol: 68 Issue: 4 Pages: 1390-1395, 2006
  4. Ameur LA, Rega B, Giampaoli P, Trystram G, BirlouezAragon I. The fate of furfurals and other volatile markers during the baking process of a model cookie. Food Chem Vol.:111, Issue 3, Pages 758-763758, 2008
  5. Gaspar, EMSM., Lopes, JF. Simple gas chromatographic method for furfural analysis. J Chromatogr A, Vol. 1216, Issue 14, Pages 2762-2767, 2009
  6. Rada-Mendoza, M., Sanz, ML., Olano, A., Villamiel, M. Formation of hydroxymethylfurfural and furosine during the storage of jams and fruit-based infant foods. Food Chem Vol.85, Issue, Pages 605-609, 2004
  7. Kus, S., Gogus, F., Eren S., Hydroxymethyl furfural content of concentrated food products. Int J Food Properties Vol.8, Issue 2, Pages 367-375, 2005
  8. Rada-Mendoza, M., Olano, A., Villamiel, M. Determination of hydroxymethylfurfural in commercial jams and in fruitbased infant foods. Food Chemistry Vol.79, Issue 4, Pages 513-516, 2002
  9. Teixido, E., Moyano, E., Santos, FJ., Galceran, MT. Liquid chromatography multi-stage mass spectrometry for the analysis of 5-hydroxymethylfurfural in foods. J Chromatographia A Vol.1185, Issue 1, Pages 102-108, 2008
  10. TS 12677, Spreaded dried mullberry, Turkısh Standard, 24.10.2000
  11. TS 12477, Pekmez mass with decorticated fruits, Turkısh Standard, 17.11.2015 12. TS 3958, Sour Cherry Jam, Turkısh Standard, 09.03.2010
  12. Regulation on Turkish Food Codex, 29 December 2011 – 28157 14. Winkler, O.: Beitrag zum Nachweis und zur Bestimmung von Oxymethylfurfural in Honigund Kunsthonig. Z. Lebensm. Forsch. 102, 160-167, 1955
  13. White, J., Spectrophotometric Method for Hydroxymethylfurfural in Honey. J. AOAC, 509, 1979
  14. Harmonısed Methods Of The Internatıonal Honey Commıssıon http://www.bee-hexagon.net/en/network. htm
  15. Analytical Detection Limit Guidance & Laboratory Guide for Determining Method Detection Limits, Wisconsin