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Journals / Hittite Journal of Science and Engineering / 2019 / Cilt: 6 - Sayı: 1

Synthesis, Characterization, Swelling Behavior and Metal Uptake Studies of Dichloroglyoxime Crosslinked Chitosan Derivative

Mahir TİMUR
Pages
37–44
Publication Date
2022-10-18
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

According to the results of the analyses; water retention capacity and metal uptake capacity of new cross-linked chitosan derivative is higher than chitosan and metal uptake sequence are Cu II > Fe II >Cd II > Co II > Ni II respectively

📌 3 Key Takeaways

🎯
Objective & Hypothesis:New crosslinked derivative of chitosan was prepared by the condensation reaction of chitosan CS and dichloro glyoxime.
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Key Findings & Data:Structural analysis of chitosan derivative CSL was performed by elemental analysis C, H, N , SEM measurements, FT-IR, solid-state 13C CP/MAS NMR, XRD-powder and TGA.
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Conclusion & Impact:According to the results of the analyses; water retention capacity and metal uptake capacity of new cross-linked chitosan derivative is higher than chitosan and metal uptake sequence are Cu II > Fe II >Cd II > Co II > Ni II respectively
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Crosslink · Chitosan · Swelling

Abstract

New crosslinked derivative of chitosan was prepared by the condensation reaction of chitosan CS and dichloro glyoxime. Structural analysis of chitosan derivative CSL was performed by elemental analysis C, H, N , SEM measurements, FT-IR, solid-state 13C CP/MAS NMR, XRD-powder and TGA. Crosslinking ratio was determined from the elemental analysis by using the C/N and found to be 70%. The swelling behavior of derivative was investigated on pH 3-7 and 10 at 25 and 37°C. Metal ion uptake capacity was studied towards of selected transition metals Cu II , Ni II , Co II , Fe II and Cd II cations in aqueous medium. According to the results of the analyses; water retention capacity and metal uptake capacity of new cross-linked chitosan derivative is higher than chitosan and metal uptake sequence are Cu II > Fe II >Cd II > Co II > Ni II respectively

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Cite This Article

TİMUR, M. (2022). Synthesis, Characterization, Swelling Behavior and Metal Uptake Studies of Dichloroglyoxime Crosslinked Chitosan Derivative. Hittite Journal of Science and Engineering, Cilt: 6 - Sayı: 1, 37–44. https://ajindex.com/articles/537979

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