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Dergiler / Hittite Journal of Science and Engineering / 2019 / Cilt: 6 - Sayı: 1

Synthesis, Characterization, Swelling Behavior and Metal Uptake Studies of Dichloroglyoxime Crosslinked Chitosan Derivative

Mahir TİMUR
Sayfa
37–44
Yayın Tarihi
2022-10-18
DOI
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

According to the results of the analyses; water retention capacity and metal uptake capacity of new cross-linked chitosan derivative is higher than chitosan and metal uptake sequence are Cu II > Fe II >Cd II > Co II > Ni II respectively

📌 3 Maddede Bu Makale

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Amaç & Hipotez:New crosslinked derivative of chitosan was prepared by the condensation reaction of chitosan CS and dichloro glyoxime.
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Temel Bulgular & Veri:Structural analysis of chitosan derivative CSL was performed by elemental analysis C, H, N , SEM measurements, FT-IR, solid-state 13C CP/MAS NMR, XRD-powder and TGA.
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Sonuç & Katkı:According to the results of the analyses; water retention capacity and metal uptake capacity of new cross-linked chitosan derivative is higher than chitosan and metal uptake sequence are Cu II > Fe II >Cd II > Co II > Ni II respectively
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Crosslink · Chitosan · Swelling

Abstract

New crosslinked derivative of chitosan was prepared by the condensation reaction of chitosan CS and dichloro glyoxime. Structural analysis of chitosan derivative CSL was performed by elemental analysis C, H, N , SEM measurements, FT-IR, solid-state 13C CP/MAS NMR, XRD-powder and TGA. Crosslinking ratio was determined from the elemental analysis by using the C/N and found to be 70%. The swelling behavior of derivative was investigated on pH 3-7 and 10 at 25 and 37°C. Metal ion uptake capacity was studied towards of selected transition metals Cu II , Ni II , Co II , Fe II and Cd II cations in aqueous medium. According to the results of the analyses; water retention capacity and metal uptake capacity of new cross-linked chitosan derivative is higher than chitosan and metal uptake sequence are Cu II > Fe II >Cd II > Co II > Ni II respectively

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Bu Makaleye Atıf Yap

TİMUR, M. (2022). Synthesis, Characterization, Swelling Behavior and Metal Uptake Studies of Dichloroglyoxime Crosslinked Chitosan Derivative. Hittite Journal of Science and Engineering, Cilt: 6 - Sayı: 1, 37–44. https://ajindex.com/articles/537979

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