Journals / Turkish Journal of Chemistry / 2019 / Cilt: 43 - Sayı: 1

Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques

Pages
229–238
Publication Date
2019-02-01
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.

📌 3 Key Takeaways

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Objective & Hypothesis:The complexes of peripherally tetra-substituted metal-free (8), lead(II) 9), and zinc(II) (10) phthalocyanine derivatives were synthesized for the first time in this work.
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Key Findings & Data:The structures of these new complex compounds have been elucidated using many spectral methods such as electronic absorption, FT-IR, $^{1}$H NMR, $^{13}$C NMR, elemental analysis, and mass spectra.
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Conclusion & Impact:The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Metallophthalocyanine · 4-triazole · 4-nitrophthalonitrile

Abstract

The complexes of peripherally tetra-substituted metal-free (8), lead(II) 9), and zinc(II) (10) phthalocyanine derivatives were synthesized for the first time in this work. The structures of these new complex compounds have been elucidated using many spectral methods such as electronic absorption, FT-IR, $^{1}$H NMR, $^{13}$C NMR, elemental analysis, and mass spectra. The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.

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Cite This Article

NAS, A., DEMİRBAŞ, Ü., GÜMRÜKÇÜOĞLU, N., KANTEKİN, H. (2019). Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques. Turkish Journal of Chemistry, Cilt: 43 - Sayı: 1, 229–238. https://ajindex.com/articles/184538

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