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Journals / Turkish Journal of Chemistry / 2019 / Cilt: 43 - Sayı: 1

Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques

Halit KANTEKİN
Ümit DEMİRBAŞ
Asiye NAS
Nurhan GÜMRÜKÇÜOĞLU
Pages
229–238
Publication Date
2022-11-04
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The thermogravimetric behavior of compounds 8–10 was determined by thermogravimetric analysismethod in addition to these spectral methods.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:The complexes of peripherally tetra-substituted metal-free (8), lead(II) (9), and zinc(II) (10) phthalocyaninederivatives were synthesized for the first time in this work.
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Key Findings & Data:The structures of these new complex compounds have beenelucidated using many spectral methods such as electronic absorption, FT-IR, 1 H NMR, 13 C NMR, elemental analysis,and mass spectra.
💡
Conclusion & Impact:The thermogravimetric behavior of compounds 8–10 was determined by thermogravimetric analysismethod in addition to these spectral methods.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

The complexes of peripherally tetra-substituted metal-free (8), lead(II) (9), and zinc(II) (10) phthalocyaninederivatives were synthesized for the first time in this work. The structures of these new complex compounds have beenelucidated using many spectral methods such as electronic absorption, FT-IR, 1 H NMR, 13 C NMR, elemental analysis,and mass spectra. The thermogravimetric behavior of compounds 8–10 was determined by thermogravimetric analysismethod in addition to these spectral methods.

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Cite This Article

KANTEKİN, H., DEMİRBAŞ, Ü., NAS, A., GÜMRÜKÇÜOĞLU, N. (2022). Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques. Turkish Journal of Chemistry, Cilt: 43 - Sayı: 1, 229–238. https://ajindex.com/articles/601662

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