Dergiler / Turkish Journal of Chemistry / 2019 / Cilt: 43 - Sayı: 1

Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques

Sayfa
229–238
Yayın Tarihi
2019-02-01
DOI
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.

📌 3 Maddede Bu Makale

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Amaç & Hipotez:The complexes of peripherally tetra-substituted metal-free (8), lead(II) 9), and zinc(II) (10) phthalocyanine derivatives were synthesized for the first time in this work.
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Temel Bulgular & Veri:The structures of these new complex compounds have been elucidated using many spectral methods such as electronic absorption, FT-IR, $^{1}$H NMR, $^{13}$C NMR, elemental analysis, and mass spectra.
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Sonuç & Katkı:The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Metallophthalocyanine · 4-triazole · 4-nitrophthalonitrile

Abstract

The complexes of peripherally tetra-substituted metal-free (8), lead(II) 9), and zinc(II) (10) phthalocyanine derivatives were synthesized for the first time in this work. The structures of these new complex compounds have been elucidated using many spectral methods such as electronic absorption, FT-IR, $^{1}$H NMR, $^{13}$C NMR, elemental analysis, and mass spectra. The thermogravimetric behavior of compounds 8-10 was determined by thermogravimetric analysis method in addition to these spectral methods.

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Bu Makaleye Atıf Yap

NAS, A., DEMİRBAŞ, Ü., GÜMRÜKÇÜOĞLU, N., KANTEKİN, H. (2019). Characterization and purification of 1,2,4-triazole-containing phthalocyanines synthesized by microwave method and structure elucidation by spectroscopic techniques. Turkish Journal of Chemistry, Cilt: 43 - Sayı: 1, 229–238. https://ajindex.com/articles/184538

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