Dergiler / Turkish Journal of Chemistry / 2016 / Cilt: 40 - Sayı: 6

Schiff base immobilized silica gel framework as an efficient sorbent forpreconcentration of Pb and Zn ions in aqueous media

Sayfa
953–964
Yayın Tarihi
2022-11-05
DOI
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

The application of themethod was performed on snow, tap, bottled, mineral, and lake water samples and recovery percentages were in therange of 96.7%{101.6% and 96.4%{98.4% for Pb(II) and Zn(II), respectively.

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Amaç & Hipotez:A novel preconcentration method for Pb and Zn ions using a column packed with Schiff base modi ed silica gelis described.
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Temel Bulgular & Veri:The method was based on the sorption of analytes on N,N'-bis(4-methoxysalicylidene)-1,3-propanediaminemodi ed silica gel and elution with HNO3prior to ame atomic absorption analysis.
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Sonuç & Katkı:The application of themethod was performed on snow, tap, bottled, mineral, and lake water samples and recovery percentages were in therange of 96.7%{101.6% and 96.4%{98.4% for Pb(II) and Zn(II), respectively.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Alan Parametreleri

Abstract

A novel preconcentration method for Pb and Zn ions using a column packed with Schiff base modi ed silica gelis described. The method was based on the sorption of analytes on N,N'-bis(4-methoxysalicylidene)-1,3-propanediaminemodi ed silica gel and elution with HNO3prior to ame atomic absorption analysis. The parameters pH, ow rate,sample volume, eluent volume, and concentration were optimized using a central composite design. The detection limitswere 10.0 g L1for Pb and 1.1 g L1for Zn. The suggested procedure was validated with Lake Ontario water asa certi ed reference material and recovery percentages were 101.8% for Pb and 98.2% for Zn. The application of themethod was performed on snow, tap, bottled, mineral, and lake water samples and recovery percentages were in therange of 96.7%{101.6% and 96.4%{98.4% for Pb(II) and Zn(II), respectively.

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Bu Makaleye Atıf Yap

TOKAY, F., KOLUMAN, M., BAĞDAT, S. (2022). Schiff base immobilized silica gel framework as an efficient sorbent forpreconcentration of Pb and Zn ions in aqueous media. Turkish Journal of Chemistry, Cilt: 40 - Sayı: 6, 953–964. https://ajindex.com/articles/647613

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