Journals / Anatolian Current Medical Journal / 2026 / Volume: 8 Issue: 2

Effect of post-processing alcohol washing time on the hardness and flexural strength of 3D-printed permanent dental resins

Büşra Tosun(BOLU ABANT IZZET BAYSAL UNIVERSITY, FACULTY OF DENTISTRY)0000-0003-3145-4454
Zeynep Şen Yılmaz(Kartal Oral and Dental Health Center)0000-0001-5478-7708
Nur Uysal(BOLU ABANT IZZET BAYSAL UNIVERSITY, FACULTY OF DENTISTRY)0009-0006-5426-4935
Pages
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Publication Date
2026-03-10
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

These results emphasize the necessity of optimizing post-processing protocols to ensure the long-term mechanical performance and clinical durability of 3D-printed permanent restorations.

📌 3 Key Takeaways

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Objective & Hypothesis:Aims: This study aimed to evaluate the influence of different alcohol washing durations on the hardness and flexural strength of a 3D-printed permanent dental resin, considering their critical role in clinical longevity.
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Key Findings & Data:Methods: Fifty bar-shaped specimens (25×2×2 mm) were fabricated using VarseoSmile TriniQ (BEGO, Bremen, Germany) permanent dental resin.
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Conclusion & Impact:These results emphasize the necessity of optimizing post-processing protocols to ensure the long-term mechanical performance and clinical durability of 3D-printed permanent restorations.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:3D printing · dental resin · alcohol washing time

Abstract

Aims: This study aimed to evaluate the influence of different alcohol washing durations on the hardness and flexural strength of a 3D-printed permanent dental resin, considering their critical role in clinical longevity. Methods: Fifty bar-shaped specimens (25×2×2 mm) were fabricated using VarseoSmile TriniQ (BEGO, Bremen, Germany) permanent dental resin. The specimens were divided into five groups (n=10) according to alcohol washing times: 3, 5, 10, 15, and 20 minutes. Following washing in 99.5% ethanol, all specimens underwent standardized light postcuring. Hardness was measured using a Shimadzu microhardness tester, and flexural strength was assessed using an Instron universal testing machine through a three-point bending test. Data were analyzed using one-way ANOVA, with the significance level set at p<0.05. Results: Alcohol washing time had a statistically significant effect on both hardness and flexural strength (p<0.001). Specimens washed for 3 minutes (21.64±3.69) and 5 minutes (18.27±2.51) exhibited significantly higher hardness values compared to those washed for 10, 15, and 20 minutes. Flexural strength showed a similar trend, with the highest strength recorded in the 3-minute group (23.19±1.02) and a progressive decrease observed with longer washing times, reaching the lowest values in the 20-minute group (17.71±1.16). Conclusion: Prolonged alcohol washing times negatively affected the mechanical properties of the 3D printed permanent dental resin. Shorter washing durations (3-5 minutes) better preserved surface hardness and flexural strength, indicating that excessive alcohol exposure may compromise material integrity. These results emphasize the necessity of optimizing post-processing protocols to ensure the long-term mechanical performance and clinical durability of 3D-printed permanent restorations.

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Cite This Article

Tosun, B., Yılmaz, Z. Ş., Uysal, N. (2026). Effect of post-processing alcohol washing time on the hardness and flexural strength of 3D-printed permanent dental resins. Anatolian Current Medical Journal, Volume: 8 Issue: 2. https://doi.org/10.38053/acmj.1869798

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References (30)

  1. Jandyal A, Chaturvedi I, Wazir I, Raina A, Ul Haq MI. 3D printing-a review of processes, materials and applications in industry 4.0. Sustain Oper Comput. 2022;3:33-42. doi:10.1016/j.susoc.2021.09.004
  2. Perea-Lowery L, Gibreel M, Vallittu PK, et al. Evaluation of the mechanical properties and degree of conversion of 3D printed splint material. J Mech Behav Biomed Mater. 2021;115:104254. doi:10.1016/j.jmbbm.2020.104254
  3. Mayer J, Stawarczyk B, Vogt K, Hickel R, Edelhoff D, Reymus M. Influence of cleaning methods after 3D printing on two-body wear and fracture load of resin-based temporary crown and bridge material. Clin Oral Investig. 2021;25:5987-5996. doi:10.1007/s00784-021-03905-9
  4. Hassanpour M, Narongdej P, Alterman N, Moghtadernejad S, Barjasteh E. Effects of post-processing parameters on 3D-printed dental appliances: a review. Polymers (Basel). 2024;16:2795. doi:10.3390/polym16192795
  5. Wazeer A, Das A, Sinha A, Inaba K, Ziyi S, Karmakar A. Additive manufacturing in biomedical field: a critical review on fabrication method, materials used, applications, challenges, and future prospects. Prog Addit Manuf. 2023;8:857-889. doi:10.1007/s40964-022-00362-y
  6. Reymus M, Fabritius R, Keßler A, Stawarczyk B, Edelhoff D, Hickel R. Fracture load of 3D-printed fixed dental prostheses compared with milled and conventionally fabricated ones: the impact of resin material, build direction, post-curing, and artificial aging-an in vitro study. Clin Oral Investig. 2020;24:701-710. doi:10.1007/s00784-019-02952-7
  7. Karakurt I, Lin L. 3D printing technologies: techniques, materials, and post-processing. Curr Opin Chem Eng. 2020;28:134-143. doi:10.1016/j.coche.2020.04.001
  8. Revilla‐León M, Meyers MJ, Zandinejad A, Özcan M. A review on chemical composition, mechanical properties, and manufacturing work flow of additively manufactured current polymers for interim dental restorations. J Esthet Restor Dent. 2019;31:51-57. doi:10.1111/jerd.12438
  9. Jin G, Gu H, Jang M, et al. Influence of postwashing process on the elution of residual monomers, degree of conversion, and mechanical properties of a 3D printed crown and bridge materials. Dent Mater. 2022;38:1812-1825. doi:10.1016/j.dental.2022.09.017
  10. Imazato S, Horikawa D, Nishida M, Ebisu S. Effects of monomers eluted from dental resin restoratives on osteoblast‐like cells. J Biomed Mater Res B Appl Biomater. 2009;88:378-386. doi:10.1002/jbm.b.31067
  11. Jeršovaitė J, Šarachovaitė U, Matulaitienė I, Niaura G, Baltriukienė D, Malinauskas M. Biocompatibility enhancement via post-processing of microporous scaffolds made by optical 3D printer. Front Bioeng Biotechnol. 2023;11:1167753. doi:10.3389/fbioe.2023.1167753
  12. Accorinte MdLR, Loguercio AD, Reis A, Muench A, de Araújo VC. Adverse effects of human pulps after direct pulp capping with the different components from a total-etch, three-step adhesive system. Dent Mater. 2005;21:599-607. doi:10.1016/j.dental.2004.08.008
  13. Šimunović L, Jurela A, Sudarević K, Bačić I, Haramina T, Meštrović S. Influence of post-processing on the degree of conversion and mechanical properties of 3D-printed polyurethane aligners. Polymers. 2023;16:17. doi:10.3390/polym16010017
  14. Oh R, Lim J-H, Lee C-G, Lee KW, Kim SY, Kim JE. Effects of washing solution temperature on the biocompatibility and mechanical properties of 3D-Printed dental resin material. J Mech Behav Biomed Mater. 2023;143:105906. doi:10.1016/j.jmbbm.2023.105906
  15. Liu Y, Jin G, Lim J-H, Kim J-E. Effects of washing agents on the mechanical and biocompatibility properties of water-washable 3D printing crown and bridge resin. Sci Rep. 2024;14:9909. doi:10.1038/s41598-024-60450-7
  16. Drummond JL. Degradation, fatigue, and failure of resin dental composite materials. J Dent Res. 2008;87:710-719. doi:10.1177/154405910808700802
  17. ISO 4049:2009 Dentistry-Polymer-based filling, restorative, and luting materials ISO 4049:201.
  18. Öztürk Z, Tosun B. Comparison of 3D printed and conventional denture base materials in terms of durability and performance characteristics. Sci Rep. 2025;15:18234. doi:10.1038/s41598-025-01685-w
  19. Lee EH, Ahn JS, Lim YJ, Kwon HB, Kim MJ. Effect of post-curing time on the color stability and related properties of a tooth-colored 3D-printed resin material. J Mech Behav Biomed Mater. 2022;126:104993. doi:10. 1016/j.jmbbm.2021.104993
  20. Soto-Montero J, de Castro EF, Romano BDC, Nima G, Shimokawa CAK, Giannini M. Color alterations, flexural strength, and microhardness of 3D printed resins for fixed provisional restoration using different post-curing times. Dent Mater. 2022;38:1271-1282. doi: 10.1016/j.dental.2022. 06.023
  21. Xu Y, Xepapadeas AB, Koos B, Geis-Gerstorfer J, Li P, Spintzyk S. Effect of post-rinsing time on the mechanical strength and cytotoxicity of a 3D printed orthodontic splint material. Dent Mater. 2021;37:e314-e327. doi: 10.1016/j.dental.2021.01.016
  22. Jang W, Kook G-S, Kang J-H, et al. Effect of washing condition on the fracture strength, and the degree of conversion of 3D printing resin. Appl Sci. 2021;11:11676. doi:10.3390/app112411676
  23. Mohammed AQ, Mohammed AK. Evaluation the biocompatibility and hardness of 3D printed resin material with different times and many rinsing solutions. AIP Conf Proc. 2024;030023. doi:10.1063/5.0211067
  24. Schneider LFJ, Moraes RR, Cavalcante LM, et al. Cross-link density evaluation through softening tests: effect of ethanol concentration. Dent Mater. 2008;24:199-203. doi:10.1016/j.dental.2007.03.010
  25. Sideridou ID, Karabela MM, Bikiaris DN. Aging studies of light cured dimethacrylate-based dental resins and a resin composite in water or ethanol/water. Dent Mater. 2007;23:1142-1149. doi:10.1016/j.dental.2006.06.049
  26. Hwangbo N-K, Nam N-E, Choi J-H, Kim J-E. Effects of the washing time and washing solution on the biocompatibility and mechanical properties of 3D printed dental resin materials. Polymers (Basel). 2021; 13:4410. doi:10.3390/polym13244410
  27. Ito S, Hashimoto M, Wadgaonkar B, et al. Effects of resin hydrophilicity on water sorption and changes in modulus of elasticity. Biomater. 2005; 26:6449-6459. doi:10.1016/j.biomaterials.2005.04.052
  28. Di Fiore A, Stellini E, Alsayed HD, Alhotan A. Influence of different post-washing solutions on the mechanical and surface properties of 3D-printed material for definitive restorations: an in vitro study. J Dent. 2025:105980. doi:10.1016/j.jdent.2025.105980
  29. Katheng A, Prawatvatchara W, Tonprasong W, Namano S, Kongkon P. Effect of postrinsing times and methods on surface roughness, hardness, and polymerization of 3D-printed photopolymer resin. Eur J Dent. 2025;19:154-164. doi:10.1055/s-0044-1786866
  30. Finck NS, Fraga MAA, Correr AB, Dalmaschio CJ, Rodrigues CS, Moraes RR. Effects of solvent type and UV post-cure time on 3D-printed restorative polymers. Dent Mater. 2024;40:451-457. doi:10.1016/j.dental. 2023.12.005