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Journals / Fırat Üniversitesi Mühendislik Bilimleri Dergisi / 2026 / Cilt: 31 Sayı: 1

SHS İşlemi Sonrası Sinterleme İşleminin İntermetalik Kaplamaya Etkisinin İncelenmesi

Musa Kılıç0000-0001-5808-6917
Mustafa Beken0000-0001-8164-0242
Niyazi Özdemir0000-0001-8796-0060
Pages
167–176
Publication Date
2019-03-15
DOI
—
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Sonuç olarak 1100 ° C’lik sinterleme sıcaklığında metaller arası fazların tamemen çözündüğü tespit edilmiştir.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:Yanma yöntemi kullanılarak Ferritik paslanmaz çelik yüzeyi üzerine Ni 3 Al intermetalik bileşiği kaplanmıştır.
📊
Key Findings & Data:Bu kaplama yönteminde kullanılan presleme basıncı(150, 200, 250, 300Mpa) ve yanma işlemi akabinde gerçekleştirilen sinterleme sıcaklığının(1100 ° C) kaplama tabakasına etkisi incelenmiştir.
💡
Conclusion & Impact:Sonuç olarak 1100 ° C’lik sinterleme sıcaklığında metaller arası fazların tamemen çözündüğü tespit edilmiştir.
🔬Design:Araştırma Makalesi
📍Scope:Comprehensive Sample
⚙️Variables:SHS · Ni3Al · Kaplama

Özet

Yanma yöntemi kullanılarak Ferritik paslanmaz çelik yüzeyi üzerine Ni 3 Al intermetalik bileşiği kaplanmıştır. Bu kaplama yönteminde kullanılan presleme basıncı(150, 200, 250, 300Mpa) ve yanma işlemi akabinde gerçekleştirilen sinterleme sıcaklığının(1100 ° C) kaplama tabakasına etkisi incelenmiştir. Kaplama tabakasının karakterizasyon işlemleri optik mikroskop, SEM, XRD ve EDX analizleri kullanılarak gerçekleştirilmiştir. Analizler sonucunda kaplama tabakası ile alt tabaka arasında gerçekleşen difüzyon ile bağlanmanın iyi olduğu gözlenmiştir. EDS analizleri sonucunda α Fe,Cr, Ni, Ni 3 Al, γ Fe ve XRD sonuçlarında ise Ni 3 Al ve Ni ile birlikte Ni 3 Al 4, NiAl, N i 3 C r 2,  Ni 2 Al 3 fazları meydana gelmiştir. Yapılan mikrosertlik analizlerinde ise kaplama tabakasının gözenekli yapısı nedeniyle alt tabakaya göre daha düşük sonuçlar elde edilmiştir. Sonuç olarak 1100 ° C’lik sinterleme sıcaklığında metaller arası fazların tamemen çözündüğü tespit edilmiştir.

🔖

Cite This Article

Kılıç, M., Beken, M., Özdemir, N. (2019). SHS İşlemi Sonrası Sinterleme İşleminin İntermetalik Kaplamaya Etkisinin İncelenmesi. Fırat Üniversitesi Mühendislik Bilimleri Dergisi, Cilt: 31 Sayı: 1, 167–176. https://ajindex.com/articles/1268159

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References (90)

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  31. Pascal C., Marin-Ayral R.M., Tédenac J.C. Joining of nickel monoaluminide to a superalloy substrate by high pressure self-propagating high-temperature synthesis, J. Alloys Compd, 2002; 337: 221–225
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  36. Wang L-L., Wang W., Fan L–Y., Qı X-X., Lıu H-J., Zhang Y-Z. Effects of Al and Ni doping on oxidation and corrosion resistance of electrophoretic deposited YSZ coatings, Trans. Nonferrous Met. Soc. China, 2017; 27: 1551−1557
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  47. Cakir K. Korkmaz E., Kayali S. Study on the Al2O3/Fe-Al intermetallic duplex coating prepared with a combined technique of electro-spark deposition and micro-arc oxidation on steel, Kovove Mater., 2017; 55: 81–87 [3] Özenbaş M., Yılmaz, O. FeCrC, WC ve B203 Kullanılarak Kaplanmış AISI4340 Çeliğinin Aşınma Karakteristiği. Il.Uluslararası Bor Sempozyumu; 2004; Eskişehir /Türkiye. 201-205
  48. Talako T., Ilyuschenko A., Letsko A. SHS Powders for Thermal Spray Coating, Kona Powder Part. J., 2009; 27: 55-72
  49. Mohammadnezhad M., Shamanian M., Enayati M.H., Salehi M., Hoseynian A. Microstructures and properties of NiAl–TiC nanocomposite coatings on carbon steel surfaces produced by mechanical alloying technique, Surf. Coat. Technol., 2014; 238: 180–187
  50. Yoruk, G., Ozdemir O.,The evaluation of NiAl- and TiAl-based intermetallic coatings produced on the AISI 1010 steel by an electric current-activated sintering method, Intermetallics, 2012; 25: 60-65
  51. Singh Sidhu B., Prakash S. Evaluation of the corrosion behaviour of plasma-sprayed Ni3Al coatings on steel in oxidation and molten salt environments at 900 oC, Surf. Coat. Technol., 2003; 166: 89–100
  52. Shahzad A., Zadorozhnyy V. Yu., Pavlov M.D., Zheleznyi M.V., Chirkov A.M., Zagrebin D.S., Semenov D.V., Khasenova R.S., Kaloshkin S.D. Deposition of the Ti-Al coatings on different metallic substrates by mechanical alloying and subsequent laser treatment, J. Alloys Compd., 2018; 731: 1295-1302
  53. Li Y., Liu Y., Geng H., Nie D. Synthesis and cladding of Ni3Al intermetallic on steel substrate by laser controlled reactive synthesis, J. Mater. Process. Technol., 2006; 171: 405–410
  54. Lin, C-M., Kai, W-Y., Su C-Y., Key K-H. Empirical alloys-by-design theory calculations to the microstructure evolution mechanical properties of Mo-doped laser cladding NiAl composite coatings on medium carbon steel substrates, J. Alloy Compd., 2017; 702: 679-686
  55. Koch C. C., Whittenberge J. D. Review Mechanical milling/alloying of intermetallics, Intermetallic, 1996; 4: 339-355
  56. Ozdemir O., Zeytin S., C. Bindal C. Tribological properties of Ni3Al produced by pressure-assisted volume combustion synthesis, Tribol. Int., 2012; 53: 22–27
  57. Lin L., Hui S., Lu G., Wang S-L., Wang X-D., Lee D-J. Molecular dynamics study of high temperature wetting kinetics for Al/NiAl and Al/Ni3Al systems: Effects of grain boundaries, Chem. Eng. Sci., 2017; 174: 127–135
  58. Morsi K., Review: reaction synthesis processing of Ni–Al intermetallic materials, Mater. Sci. Eng., 2001; A299: 1–15
  59. Liu H., Chen W. Reactive oxide-dispersed Ni3Al intermetallic coatings by sediment co-deposition, Intermetallics, 2005; 13: 805–817
  60. Li S., Feng D., Luo H. Microstructure and abrasive wear performance of chromium carbide reinforced Ni3Al matrix composite coating, Surf. Coat. Technol., 2007; 201; 4542–4546
  61. Chen J., Huang H., Zhang K., Wang M., Wu M., Li H., Zhang S., Wen M. Interfacial reactions in the SiCf/Ni3Al composites by employing C single coating and C+Y2O3 duplex coating as barrier layers, J. Alloys Compd., 2018; 765: 18-26 [18] Stewart L.T., Plucknett P.K. The effects of Mo2C additions on the microstructure and sliding wear of TiC0.3N0.7–Ni3Al cermets, Int. J. Refract. Met. Hard Mater., 2015; 50: 227–239
  62. Luis I, C.N. Transition metal aluminid Coatings and Initial Steps on Additive Manufacturing, 20.12.2017,
  63. Tong Z., Bao H. Decompose the electron and phonon thermal transport of intermetallic compounds NiAl and Ni3Al by first-principles calculations, Int. J. Heat Mass Transfer, 2018; 117: 972–977
  64. Nazarov A., Safronov A. V., Khmyrov S. R., Shishkovsky I. Fabrication of gradient structures in the Ni - Al system via SLM Process, Procedia IUTAM, 2017; 23: 161 – 166
  65. Li-Yuan S., Ting-Fei X., Chen L., Jian-Ting G., Yu-Feng Z. Effect of extrusion process on microstructure and mechanical properties of Ni3Al_B_Cr alloy during self-propagation high-temperature synthesis, Trans. Nonferrous Met. Soc. China, 2012; 22: 489_495
  66. Yamaguchi T., Hagino H. Formation of a titanium-carbide-dispersed hard coating on austenitic stainless steel by laser alloying with a light-transmitting resin, Vacuum, 2018; 155: 23–28
  67. Xiang, X., Wang X., Zhang G., Tang T., Lai X. Preparation technique and alloying effect of aluminide coatings as tritium permeation barriers: A review, Int. J. Hydrogen Energy, 2015; 40: 3697- 3707
  68. Sierra C., Vázquez J.A. NiAl coatings on carbon steel by self-propagating high-temperature synthesis assisted with concentrated solar energy: mass influence on adherence and porosity, Sol. Energy Mater. Sol. Cells, 2005; 86: 33–42
  69. Cammarota G.P., Casagrande A., Poli G., Veronesi P. Ni–Al–Ti coatings obtained by microwave assisted SHS: Effect of annealing on microstructural and mechanical properties, Surface & Coatings Technology, 2009; 203: 1429–1437
  70. Boromei, A., Casagrande F., Tarterini G., Poli P., Rosa R.V. Ni–Al–Ti coatings obtained by microwave assisted SHS: Oxidation behaviour in the 750–900 °C range, Surf. Coat. Technol., 2010; 204: 1793–1799
  71. Ozdemir O., Zeytin S., Bindal C. A study on NiAl produced by pressure-assisted combustion synthesis, Vacuum, 2010; 84: 430–437
  72. Riyadi T.W.B., Zhang T., Marchant D., Zhu X. Synthesis and fabrication of NiAl coatings with Ti underlayer using induction heating, Surf. Coat. Technol., 2014; 258: 154–159
  73. Zanotti C., Giuliani P., Terrosu A., Gennari S., Maglia F., Porous Ni -Ti,ignition and combustion synthesis, Intermetallics, 2007; 15: 404-412
  74. Goh C.W., Gu Y.W., Lim C.S., Tay B.Y., Influence of nanocrystalline Ni-Ti reaction agent on self-propagating high-temperature synthesized porous NiTi”, Intermetallics, 2007; 15: 461-467
  75. La P., Bai M., Xue Q., Liu W., A study of Ni3Al coating on carbon steel surface via the SHS casting route, Surf. Coat. Technol., 1999; 113: 44–51
  76. Pascal C., Marin-Ayral R.M., Tédenac J.C. Joining of nickel monoaluminide to a superalloy substrate by high pressure self-propagating high-temperature synthesis, J. Alloys Compd, 2002; 337: 221–225
  77. Kılıç M., Beken B., Kırık İ., Özdemir N. Kendi İlerliyen Yüksek Sıcaklık Sentezlemesi İle Ferritik paslanmaz Çelik Üzerine Ni3Al’nin Kaplanması Ve Mikroyapı İncelemesi, International Conference on Material Science and Technology in Cappadocia (IMSTEC’16), April 6-8, 2016, 66-72, Nevsehir, Turkey
  78. Chen, Y., Chung D.D.L. Nickel aluminid (Ni3Al) by reaktive infiltration, J. Mater. Sci, 1996; 31: 2117-2122.http://wings.buffalo.edu/academic/department/eng/mae/cmrl/Nickel%20aluminide%20fabricated%20by%20reactive%20infiltration.pdf 15.11.2015. [36] https://www.asminternational.org/ 10.11.2015 [37] Tosun G., Özler L., Kaya M., Orhan N. SHS yöntemi ile üretilen NiTi alaşımlarının gözenek oranının incelenmesi, 5th International Powder Metallurgy Conference, 2008; 1353-1367, Ankara, Turkey
  79. Wang W., Yang B., Du L., Zhang W. Diffusion research between Ni3Al coating and titanium alloy produced by plasma spraying process, Appl. Surf. Sci., 2010; 256: 3342–3345
  80. Podrabinnika A.P., Shishkovsky V.I. Laser post annealing of cold-sprayed Al–Ni composite coatings for green energy tasks, Procedia IUTAM, 2017; 23: 108 – 113
  81. Wang L-L., Wang W., Fan L–Y., Qı X-X., Lıu H-J., Zhang Y-Z. Effects of Al and Ni doping on oxidation and corrosion resistance of electrophoretic deposited YSZ coatings, Trans. Nonferrous Met. Soc. China, 2017; 27: 1551−1557
  82. Chen D., Luo F., Lou X., Qing Y., Zhou W., Zhu D. Comparison of thermal insulation capability between conventional and nanostructured plasma sprayed YSZ coating on Ni3Al substrates, Ceram. Int., 2017; 43: 4324–4329
  83. La P., Baı M., Xue O., Lıu W, A study of Ni3Al coating on carbon steel surface via the SHS casting route, Surf. Coat. Technol., 1999; 113: pp. 44-51
  84. Kotoban D., Nazarov A., Shishkovsky I. Comparative Study of Selective Laser Melting and Direct Laser Metal Deposition of Ni3Al Intermetallic Alloy, Procedia IUTAM, 2017; 23: 138 – 146
  85. Sidhu S.B., Prakash S. Evaluation of the corrosion behaviour of plasma-sprayed Ni3Al coatings on steel in oxidation and molten salt environments at 900 oC, Surf. Coat. Technol., 2003; 166: 89–100
  86. Ellner M., Keli S., Predel B. Ni3Al4 – A phone with ordered vacancies isotypic to Ni3Ga4, J. Less- Common Metals, (1989), V.154-1207-215
  87. Mishın Y. Atomistic modeling of γ and γ’-phases of the Ni-Al system, Acta mater., 2004; 52: 1451 - 1465
  88. Al – Aql A.A., Al- Salhi M.S., Ansari M.I. Precipitation in Ni-35 at pct Cr Alloy, J.Mater. Sci. Technol., 2002; V 18: No:177-79
  89. Pogrebnjak A., Beresnev V.M. Hard Nanocomposite Coatings, Their Structure and Properties, 2012; Chapter 6: 13-160,
  90. Mishra B.S., Chandra K., Prakash S., Venkataraman B. Characterisation and erosion behaviour of a plasma sprayed Ni3Al coating on a Fe-based superalloy, Mater. Lett., 2005; 59: 3694 – 3698.