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Dergiler / Ata-Kimya Dergisi / 2026 / Cilt: 4 Sayı: 1

Yeni Fenantrolin İçerikli Ditiyofosfonato Nikel Kompleksinin Sentezi ve Karakterizasyonu

Synthesis and Characterization of a New Phenanthroline-Containing Dithiophosphonato Nickel Complex

Ayşe Zeynep Varlı(MARMARA UNIVERSITY)0009-0007-0046-9297
Elif Bulat(MARMARA UNIVERSITY)0000-0002-2164-3641
Ertuğrul Gazi Sağlam(MARMARA ÜNİVERSİTESİ, FEN FAKÜLTESİ, KİMYA BÖLÜMÜ)0000-0002-7719-3934
Sayfa
20–25
Yayın Tarihi
2024-05-22
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

Sentezlenen koordinasyon bileşiğinin yapısı elementel analiz, manyetik duyarlılık ölçümleriyle beraber, FT-IR ve kütle spektroskopisi ölçümleriyle de aydınlatılmıştır.

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Amaç & Hipotez:Bu çalışmada, bilinen Ni(II) ditiyofosfonato kompleksinden Lewis bazı içerikli yeni fenantrolin Ni(II)ditiyofosfonato kompleksi sentezlendi.
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Temel Bulgular & Veri:İyonik yapıda kompleks paramanyetik özelliğe sahiptir.
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Sonuç & Katkı:Sentezlenen koordinasyon bileşiğinin yapısı elementel analiz, manyetik duyarlılık ölçümleriyle beraber, FT-IR ve kütle spektroskopisi ölçümleriyle de aydınlatılmıştır.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Ditiyofosfonato Ni(II) kompleksi · Ditiyofosfonato Nikel Fenantrolin kompleksleri · Fenantrolin

Özet

Bu çalışmada, bilinen Ni(II) ditiyofosfonato kompleksinden Lewis bazı içerikli yeni fenantrolin Ni(II)ditiyofosfonato kompleksi sentezlendi. İyonik yapıda kompleks paramanyetik özelliğe sahiptir. Sentezlenen koordinasyon bileşiğinin yapısı elementel analiz, manyetik duyarlılık ölçümleriyle beraber, FT-IR ve kütle spektroskopisi ölçümleriyle de aydınlatılmıştır.

Abstract

In this study, a new Lewis base-containing phenanthroline Ni(II) dithiophosphonato complex was synthesized from Ni(II)dithiophosphonato complex which is previously known. The complex has ionic structure and paramagnetic properties. The structure of the synthesized coordination compound was elucidated by elemental analysis, magnetic susceptibility measurements, FT-IR and mass spectroscopy measurements.

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Bu Makaleye Atıf Yap

Varlı, A. Z., Bulat, E., Sağlam, E. G. (2024). Yeni Fenantrolin İçerikli Ditiyofosfonato Nikel Kompleksinin Sentezi ve Karakterizasyonu. Ata-Kimya Dergisi, Cilt: 4 Sayı: 1, 20–25. https://doi.org/10.5281/zenodo.11219427

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Kaynakça (21)

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