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Dergiler / Ata-Kimya Dergisi / 2026 / Cilt: 4 Sayı: 1

Yeni Palladyum Ditiyofosfinato Kompleksi Sentezi ve Yapısının Aydınlatılması

Synthesis and Structure Characterization of a New Palladium Dithiophosphinato Complex

Ahsen Albaş(MARMARA ÜNİVERSİTESİ)0009-0006-6118-2364
Elif Bulat(GEBZE TEKNİK ÜNİVERSİTESİ)0000-0002-2164-3641
Ertuğrul Gazi Sağlam(MARMARA ÜNİVERSİTESİ, FEN FAKÜLTESİ, KİMYA BÖLÜMÜ)0000-0002-7719-3934
Sayfa
12–19
Yayın Tarihi
2024-05-22
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

Sentezlenen Pd(II) ditiyofosfinato kompleksinin yapısı kütle spektrometrisi (ESI), FTIR spektroskopisi, NMR (1H-, 13C- ve 31P-) ile karakterize edilmiştir.

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Amaç & Hipotez:Bilinen amonyum sek-bütil(4-metoksifenil) ditiyofosfinat ligandından, yeni Pd(II) ditiyofosfinato kompleksi sentezlendi.
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Temel Bulgular & Veri:Bilinen amonyum sek-bütil(4-metoksifenil) ditiyofosfinat ligandından, yeni Pd(II) ditiyofosfinato kompleksi sentezlendi.
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Sonuç & Katkı:Sentezlenen Pd(II) ditiyofosfinato kompleksinin yapısı kütle spektrometrisi (ESI), FTIR spektroskopisi, NMR (1H-, 13C- ve 31P-) ile karakterize edilmiştir.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Ditiyofosfinik Asitler · Ditiyofosfinatlar · Palladyum kompleksleri

Özet

Bilinen amonyum sek-bütil(4-metoksifenil) ditiyofosfinat ligandından, yeni Pd(II) ditiyofosfinato kompleksi sentezlendi. Sentezlenen Pd(II) ditiyofosfinato kompleksinin yapısı kütle spektrometrisi (ESI), FTIR spektroskopisi, NMR (1H-, 13C- ve 31P-) ile karakterize edilmiştir.

Abstract

A new Pd(II) dithiophosphinato complex was synthesised the ammonium sec-butyl (4-methoxyphenyl) dithiophosphinate ligand previously known. New Pd(II) dithiophosphinato complex’ structure was elucidated by mass spectrometry (ESI), FTIR spectroscopy, NMR (1H-, 13C- and 31P-).

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Bu Makaleye Atıf Yap

Albaş, A., Bulat, E., Sağlam, E. G. (2024). Yeni Palladyum Ditiyofosfinato Kompleksi Sentezi ve Yapısının Aydınlatılması. Ata-Kimya Dergisi, Cilt: 4 Sayı: 1, 12–19. https://doi.org/10.5281/zenodo.11219364

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