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Journals / Turkish Journal of Pharmaceutical Sciences / 2004 / Cilt: 1 - Sayı: 2

Türkiye'de yetişen dört Galanthus türünde lycorine'in yüksek basınçlı sıvı kromatografisi yöntemi ile analizi

High pressure liquid chromatographic analysis of lycorine in four Galanthus species growing in Turkey

GÜLEN İREM KAYA
Aylin FİLLİK
Yaşar HIŞIL
Nehir ÜNVER
Pages
105–114
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

External standard calibration was used to quantify lycorine.

📌 3 Key Takeaways

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Objective & Hypothesis:The detection and quantification of Lycorine in the total alkaloidal extracts prepared from aerial and underground parts of Galanthus nivalis ssp. cilicicus, G. gracilis, G. elwesii and G. plicatus ssp. byzantinus, collected during two different vegetation periods, were carried out using high performance liquid chromatography (HPLC).
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Key Findings & Data:An isocratic system with chloroform/methanol mobile phase was used for the detection and quantitative determination of lycorine.
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Conclusion & Impact:External standard calibration was used to quantify lycorine.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Galanthus · Türkiye · Liliaceae

Abstract

The detection and quantification of Lycorine in the total alkaloidal extracts prepared from aerial and underground parts of Galanthus nivalis ssp. cilicicus, G. gracilis, G. elwesii and G. plicatus ssp. byzantinus, collected during two different vegetation periods, were carried out using high performance liquid chromatography (HPLC). An isocratic system with chloroform/methanol mobile phase was used for the detection and quantitative determination of lycorine. External standard calibration was used to quantify lycorine.

Özet

Vejetasyonunun iki farklı zamanında toplanmış olan Galanthus nivalis ssp. cilicicus, G. gracilis, G. elwesii ve G. plicatus ssp. byzantinus’un topraküstü ve toprakaltı kısımlarından hazırlanan total alkaloit ekstrelerinde Lycorine’in tespiti ve miktar tayini yüksek basınçlı sıvı kromatografisi (YBSK) kullanılarak gerçekleştirilmiştir. Lycorine’in tespiti ve miktar tayini için kloroform/metanol mobil fazlı bir izokratik sistemden yararlanılmıştır. Lycorine miktarının tayininde harici standart kalibrasyon yöntemi kullanılmıştır.

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Cite This Article

KAYA, G. İ., FİLLİK, A., HIŞIL, Y., ÜNVER, N. (2004). Türkiye'de yetişen dört Galanthus türünde lycorine'in yüksek basınçlı sıvı kromatografisi yöntemi ile analizi. Turkish Journal of Pharmaceutical Sciences, Cilt: 1 - Sayı: 2, 105–114. https://ajindex.com/articles/403868

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