Journals / Hacettepe Journal of Biology and Chemistry / 2011 / Cilt: 39 - Sayı: 4

Preparation and Characterization of Poly acrylamide/maleic acid -based hydrogels Composites

Poli akrilamid-maleik asit temelli hidrojel kompozitlerin Hazırlanması ve Karakterizasyonu

Pages
359–370
Publication Date
2011-12-01
DOI
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AI Summary & Key Takeaways

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⚡ TL;DR(Too Long; Didn't Read)

The results of FT-IR, TGA, SEM, BET-porosity and PZC analysis presented certain evidences for the formation of composites, it was impressed that the composites were the mixtures composed of two phases composing of organic PAA-MA and inorganic B or Z phases rather than the formation of polymer/ mineral hybrid.

📌 3 Key Takeaways

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Objective & Hypothesis:The principle aim of this investigation was the preparation and characterization of the composites formed from Bentonite B and Zeolite Z minerals, and polyacrylamide-co-maleic acid PAA-MA hydrogel polymers.
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Key Findings & Data:The procedures used in obtaining the polymers were also applied in preparation of the composites by direct polymerization of the monomers of interests dissolved in the suspension of B or Z.
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Conclusion & Impact:The results of FT-IR, TGA, SEM, BET-porosity and PZC analysis presented certain evidences for the formation of composites, it was impressed that the composites were the mixtures composed of two phases composing of organic PAA-MA and inorganic B or Z phases rather than the formation of polymer/ mineral hybrid.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Kompozit · Poliakrilamid-ko-Maleik asit · Bentonit

Abstract

The principle aim of this investigation was the preparation and characterization of the composites formed from Bentonite B and Zeolite Z minerals, and polyacrylamide-co-maleic acid PAA-MA hydrogel polymers. The procedures used in obtaining the polymers were also applied in preparation of the composites by direct polymerization of the monomers of interests dissolved in the suspension of B or Z. The prepared PAA-MA and the composites were characterized with the data and analysis results obtained from FT-IR, TGA, SEM, BET-porosity and Zero Point of Surface Charge PZC . The results of FT-IR, TGA, SEM, BET-porosity and PZC analysis presented certain evidences for the formation of composites, it was impressed that the composites were the mixtures composed of two phases composing of organic PAA-MA and inorganic B or Z phases rather than the formation of polymer/ mineral hybrid.

Özet

B u araştırmanın temel amacı Bentonit B ve Zeolit Z minerallerinin hidrojel polimer olan Poliakrilamidko-maleik asit PAA-MA ile oluşturduğu kompozitini hazırlamak ve karakterize etmektir. Polimerlerin elde edilmesinde kullanılan yöntem, kompozitlerin hazırlanmasında da kullanılmış ve B veya Z içeren süspansiyon ortamında bulunan ilgili monomerlere doğrudan polimerleştirme işlemi uygulanmıştır. Hazırlanan PAA-MA ve kompozitlerin yapısal karakterizasyonunda FT-IR, TGA, SEM, BET-Gözeneklilik ve sıfır yüzey yük noktası PZC ile ilgili veri ve analiz sonuçları kullanılmıştır. FT-IR, XRD, TGA, SEM, BET-gözeneklilik ve PZC analiz sonuçları kompozit oluşumu ile ilgili kesin kanıtlar sunmuş, yapıların polimer/mineral hibrit oluşumundan çok biri organik PAA-MA ve diğeri inorganik özellikteki B veya Z iki faz içeren bir karışım olduğu kanısına varılmıştır

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Cite This Article

AKKAYA, R., ULUSOY, U. (2011). Preparation and Characterization of Poly acrylamide/maleic acid -based hydrogels Composites. Hacettepe Journal of Biology and Chemistry, Cilt: 39 - Sayı: 4, 359–370. https://ajindex.com/articles/256061

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