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Journals / Gazi Üniversitesi Fen Fakültesi Dergisi / 2024 / Cilt: 5 Sayı: 2

Çevre Dostu Bir Yaklaşım: One-Pot (Tek-Kap) Yeşil Sentez ile AgNP Sentezi, Kitosan Konsantrasyonunun Tanecik Boyutu Üzerine Etkisi ve Antibakteriyel Aktiviteleri

Filiz Kara(BAŞKENT ÜNİVERSİTESİ)0000-0002-5017-0783
Pages
169–180
Publication Date
2024-11-28
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Herhangi bir toksik kimyasalın kullanılmadığı, düşük maliyetli, kolay olan bu yöntem çok geniş kullanım alanına sahip AgNP’lerin eldesi için alternatif bir uygulama sunmaktadır.

📌 3 Key Takeaways

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Objective & Hypothesis:Gümüş nanopartikül (AgNP), hem indirgeyici hem de stabilize edici ajan olarak hareket eden kitosan (CH) kullanılarak one-pot yeşil sentez yöntemi ile otoklavda sentezlenmiştir.
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Key Findings & Data:Farklı konsantrasyonlarda kullanılan kitosanın (%0,3-0,9 w/v) oluşan AgNP (AgNP-CH0.3¬AgNP-CH0.9) özellikleri üzerine etkisi incelenmiştir.
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Conclusion & Impact:Herhangi bir toksik kimyasalın kullanılmadığı, düşük maliyetli, kolay olan bu yöntem çok geniş kullanım alanına sahip AgNP’lerin eldesi için alternatif bir uygulama sunmaktadır.
🔬Design:Araştırma Makalesi
📍Scope:Comprehensive Sample
⚙️Variables:Yeşil sentez · AgNP · Kitosan

Özet

Gümüş nanopartikül (AgNP), hem indirgeyici hem de stabilize edici ajan olarak hareket eden kitosan (CH) kullanılarak one-pot yeşil sentez yöntemi ile otoklavda sentezlenmiştir. Farklı konsantrasyonlarda kullanılan kitosanın (%0,3-0,9 w/v) oluşan AgNP (AgNP-CH0.3¬AgNP-CH0.9) özellikleri üzerine etkisi incelenmiştir. UV-vis spektrumları, AgNP-CH'ler için karakteristik olan 423-432 nm aralığında pik göstermiştir. Fizikokimyasal özellikler taramalı elektron mikroskobu (SEM), X-ışını kırınımı (XRD), zetasizer gibi farklı yöntemler kullanılarak değerlendirilmiştir. Sonuçlar kitosan konsantrasyonun artmasıyla nanopartikül boyutunun azaldığını ve en küçük boyuta sahip örneğin yüzey merkezli kübik (fcc) kristal yapıdaki AgNP-CH-0.9 olduğunu ortaya koyulmuştur. Tüm örnekler Escherichia coli (E. coli) ve Staphylococcus aureus (S. aureus)'a karşı antibakteriyal aktiviteye sahipken en yüksek aktiviteyi AgNP-CH-0.9 sergilemiştir. Nanopartikül boyutu küçüldükçe antibakteriyal etkinliğin arttığı belirlenmiştir. Herhangi bir toksik kimyasalın kullanılmadığı, düşük maliyetli, kolay olan bu yöntem çok geniş kullanım alanına sahip AgNP’lerin eldesi için alternatif bir uygulama sunmaktadır.

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Cite This Article

Kara, F. (2024). Çevre Dostu Bir Yaklaşım: One-Pot (Tek-Kap) Yeşil Sentez ile AgNP Sentezi, Kitosan Konsantrasyonunun Tanecik Boyutu Üzerine Etkisi ve Antibakteriyel Aktiviteleri. Gazi Üniversitesi Fen Fakültesi Dergisi, Cilt: 5 Sayı: 2, 169–180. https://ajindex.com/articles/1615310

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