Journals / İmalat Teknolojileri ve Uygulamaları / 2026 / Cilt: 7 Sayı: 2

Investigation of Fracture Behavior in an Ultra-Ductile FCC Single-Crystal Alloy

Ultra-Sünek YMK Tek Kristalli Bir Alaşımda Kırılma Davranışının İncelenmesi

Sezer Pıçak(KARABÜK ÜNİVERSİTESİ)0000-0002-1057-5970
Pages
93–101
Publication Date
2026-08-30
🏛️Bibliographic metadata and full text access for this article are provided via DergiPark.
DergiPark Record ↗
✨

AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The interplay of these mechanisms results in a pronounced enhancement in strain hardening and overall plastic deformability.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:The tensile deformation behavior of a single-crystalline multi-principal alloy system was systematically investigated at room temperature along three crystallographic orientations [111], [110], and [100] to elucidate the orientation dependence of the fracture surface behavior.
📊
Key Findings & Data:Previous studies demonstrated that the initial hardening response in the [100]-oriented crystal is governed by dislocation-mediated deformation.
💡
Conclusion & Impact:The interplay of these mechanisms results in a pronounced enhancement in strain hardening and overall plastic deformability.
🔬Design:Araştırma Makalesi
📍Scope:Comprehensive Sample
⚙️Variables:Kırılma yüzeyi · Yönelim bağımlılığı · Kayma–ikizlenme etkileşimi

Abstract

The tensile deformation behavior of a single-crystalline multi-principal alloy system was systematically investigated at room temperature along three crystallographic orientations [111], [110], and [100] to elucidate the orientation dependence of the fracture surface behavior. Previous studies demonstrated that the initial hardening response in the [100]-oriented crystal is governed by dislocation-mediated deformation. However, the tensile response in the [111]- and [110]-oriented crystals is accompanied by the progressive formation of mechanical twins and multi-slip activation. The interplay of these mechanisms results in a pronounced enhancement in strain hardening and overall plastic deformability. Moreover, the secondary or tertiary twinning activation in these orientations contributes an additional hardening stage, effectively suppressing strain localization and extending the regime of uniform plastic deformation. Scanning electron microscopy (SEM) analysis reveals an apparent paradox: while the [100]-oriented specimens, which exhibit the lowest ductility, fail via a ductile fracture mode, the more ductile [111]- and [110]-oriented crystals display features characteristic of brittle fracture. This seemingly contradictory behavior is rationalized by considering the enhanced stability against necking in the [111]- and [110]-oriented crystals, which promotes strain accumulation to higher levels and ultimately leads to brittle fracture.

Özet

Tek kristalli konsantre alaşım sisteminin çekme deformasyonu davranışı, kırılma yüzeyi davranışının yönelim bağımlılığını ortaya koymak amacıyla [111], [110] ve [100] olmak üzere üç kristalografik yönelim boyunca oda sıcaklığında sistematik olarak incelenmiştir. Önceki çalışmalar, tüm yönelimlerde başlangıçtaki pekleşme davranışının dislokasyon aracılı kayma tarafından kontrol edildiğini göstermiştir. Bununla birlikte, [111] ve [110] yönelimli kristallerde deformasyonun ilerlemesi, mekanik ikizlerin kademeli oluşumu da dahil olmak üzere karmaşık, deformasyonla indüklenen mikroyapısal bir evrimle birlikte gerçekleşmektedir. Bu mekanizmaların etkileşimi, deformasyon pekleşmesinde ve toplam plastik şekil değiştirme kapasitesinde belirgin bir artışa yol açmaktadır. Ayrıca, bu yönelimlerde ikizlenmenin gecikmeli aktivasyonu ek bir pekleşme aşaması oluşturarak deformasyon lokalizasyonunu etkin biçimde baskılamakta ve homojen plastik deformasyon rejimini genişletmektedir. Taramalı elektron mikroskobu (SEM) analizleri dikkat çekici bir karşıtlığı ortaya koymaktadır: en düşük sünekliği gösteren [100] yönelimli numuneler sünek kırılma modu ile hasara uğrarken, daha sünek olan [111] ve [110] yönelimli kristaller gevrek kırılmaya özgü özellikler sergilemektedir. İlk bakışta çelişkili görünen bu davranış, [111] ve [110] yönelimli kristallerde boyun verme kararsızlığına karşı artan stabilite dikkate alınarak açıklanabilir; bu stabilite, daha yüksek seviyelere kadar şekil değiştirme birikimini mümkün kılmakta ve nihayetinde gevrek kırılmaya yol açmaktadır.

🔖

Cite This Article

Pıçak, S. (2026). Investigation of Fracture Behavior in an Ultra-Ductile FCC Single-Crystal Alloy. İmalat Teknolojileri ve Uygulamaları, Cilt: 7 Sayı: 2, 93–101. https://doi.org/10.52795/mateca.1965706

📄 Full Text PDF Viewer

📄

PDF görüntüleyici hazırlanıyor...

References (30)

  1. S. Picak, P. Singh, D. Salas, M.A. Tunes, X. Fang, L. Zhou, M.J. Kramer, Y.I. Chumlyakov, D.D. Johnson, R. Arroyave, Y. Ren, I. Karaman, Orientation dependence of the effect of short-range ordering on the plastic deformation of a medium entropy alloy, Mater. Sci. Eng. A. (2023) 145309.
  2. S. Picak, T. Wegener, S. V Sajadifar, C. Sobrero, J. Richter, H. Kim, T. Niendorf, I. Karaman, On the low cycle fatigue response of CoCrNiFeMn high entropy alloy with ultra-fine grain structure, Acta Mater. 205 (2021) 116540.
  3. S. Picak, H.C. Yilmaz, I. Karaman, Simultaneous deformation twinning and martensitic transformation in CoCrFeMnNi high entropy alloy at high temperatures, Scr. Mater. 202 (2021) 113995.
  4. S. Picak, The role of stair-rod dislocations on the twinning and martensitic transformation in single crystalline NiCoCr, Scr. Mater. 258 (2025) 116522.
  5. S. Picak, J. Liu, C. Hayrettin, W. Nasim, D. Canadinc, K. Xie, Y.I. Chumlyakov, I. V Kireeva, I. Karaman, Anomalous work hardening behavior of Fe40Mn40Cr10Co10 high entropy alloy single crystals deformed by twinning and slip, Acta Mater. 181 (2019) 555–569.
  6. P. Singh, S. Picak, A. Sharma, Y.I. Chumlyakov, R. Arroyave, I. Karaman, D.D. Johnson, Martensitic Transformation in FexMn80−xCo10Cr10 High-Entropy Alloy, Phys. Rev. Lett. 127 (2021) 115704.
  7. B. Uzer, S. Picak, J. Liu, T. Jozaghi, D. Canadinc, I. Karaman, I. Kireeva, On the mechanical response and microstructure evolution of NiCoCr single crystalline medium entropy alloys, Mater. Res. Lett. 6 (2018) 442–449.
  8. S. Picak, Deformation Mechanisms in Single Crystalline and Ultrafine Polychrystalline Medium and High Entropy Alloys, Texas A&M University, 2021. http://hdl.handle.net/1969.1/195273.
  9. X. Gao, Z. Zhang, L. Liu, C. Tao, Lattice Rotation and Deformation Mechanisms under Tensile Loading in a Single-Crystal Superalloy with [001] Misorientation, Materials (Basel). 17 (2024) 1368. https://doi.org/10.3390/ma17061368.
  10. Z.J. Zhou, L. Wang, D. Wang, L.H. Lou, J. Zhang, Materials Science & Engineering A Effect of secondary orientation on room temperature tensile behaviors of Ni-base single crystal superalloys, Mater. Sci. Eng. A. 659 (2016) 130–142. https://doi.org/10.1016/j.msea.2016.02.013.
  11. T. Banerjee, A. Sharma, S. Picak, M. Lattemann, P. Singh, An atomistic study connecting underlying dislocation behavior with superior mechanical properties of NiCoCr medium entropy alloy, Mater. Today Commun. 44 (2025) 112065.
  12. F. Scheyvaerts, L. Delannay, P. Van Houtte, T. Pardoen, S.K. Yerra, C. Teko, International Journal of Solids and Structures Void growth and coalescence in single crystals, 47 (2010) 1016–1029.
  13. M. Janssen, J. Zuidema, R.J.H. Wanhill, Fracture Mechanics, 2nd ed., Spon Press, London, UK, 2004.
  14. G.P. Potirniche, J.L. Hearndon, Lattice orientation effects on void growth and coalescence in fcc single crystals, 22 (2006) 921–942.
  15. A. Li, W. Hu, Y. Yang, K. Li, H. Tian, Z. Zhan, Q. Meng, A microdamage model for FCC single crystals considering a mixed failure mechanism of slip and cleavage, Int. J. Plast. 173 (2024) 103888.
  16. W. Wci, Some Microstructural Aspects of Ductile Fracture of Metals, (2021) 1–28.
  17. F. Ebrahimi, J. Yanevich, D.P. Deluca, Deformation and fracture of the PWA 1472 superalloy single crystal, Acta Mater. 48 (2000) 469–479.
  18. K. Sumio, A. Yoshikazu, O. Toshihiro, K. Ryosuke, Orientation Dependence of Plasticity and Fracture in Single-Crystal Superelastic Cu-Al-Mn SMA Bars, J. Mater. Civ. Eng. 33 (2021) 4021027.
  19. M.L. Martin, J.A. Fenske, G.S. Liu, P. Sofronis, I.M. Robertson, On the formation and nature of quasi-cleavage fracture surfaces in hydrogen embrittled steels, Acta Mater. 59 (2011) 1601–1606.
  20. W.F. Hosford, Fundamentals of engineering plasticity, Cambridge university press, 2013.
  21. M.A. Meyers, K.K. Chawla, Mechanical Behavior of Materials, 2nd ed., Cambridge University Press, Cambridge, 2008.
  22. V.P. Bacurau, P.A.F.P. Moreira, G. Bertoli, A.F. Andreoli, E. Mazzer, F.F. De Assis, P. Gargarella, G. Koga, G.C. Stumpf, S.J.A. Figueroa, M. Widom, M. Kaufman, A. Fantin, Y. Cao, R. Freitas, D. Miracle, F.G. Coury, Comprehensive analysis of ordering in CoCrNi and CrNi 2 alloys, Nat. Commun. (2024) 1–11. https://doi.org/10.1038/s41467-024-52018-w.
  23. J. Meng, Y. Zhao, Y. Liu, Z. Li, B. Gao, M. Xu, W. Xia, X. Chen, H. Zhou, Y. Zhu, Impact of gradient microstructure on strain hardening via activation of multiple deformation mechanisms in CoCrNi medium entropy alloy, Mater. Futur. 3 (2024) 41002.
  24. S. Yoshida, G. Yamashita, T. Ikeuchi, Y. Bai, A. Shibata, N. Tsuji, Grain size dependent deformation microstructure evolution and work-hardening in CoCrNi medium entropy alloy, J. Alloy. Metall. Syst. 8 (2024) 100123.
  25. H.W. Deng, Z.M. Xie, B.L. Zhao, Y.K. Wang, M.M. Wang, J.F. Yang, T. Zhang, Y. Xiong, X.P. Wang, Q.F. Fang, C.S. Liu, Tailoring mechanical properties of a CoCrNi medium-entropy alloy by controlling nanotwin-HCP lamellae and annealing twins, Mater. Sci. Eng. A. 744 (2019) 241–246.
  26. N. Jia, P. Eisenlohr, F. Roters, D. Raabe, X. Zhao, Orientation dependence of shear banding in face-centered-cubic single crystals, Acta Mater. 60 (2012) 3415–3434. https://doi.org/10.1016/j.actamat.2012.03.005.
  27. C.C. Tasan, J.P.M. Hoefnagels, M.G.D. Geers, Microstructural banding effects clarified through micrographic digital image correlation, Scr. Mater. 62 (2010) 835–838.
  28. A.F. Liu, Mechanics and Mechanisms of Fracture: An Introduction, in: 2005.
  29. B.S. Adair, W.S. Johnson, S.D. Antolovich, A. Staroselsky, Crystallographic orientation and temperature effects on the fatigue crack growth rate and resulting fracture surface morphology in PWA1484 single crystal superalloy, Fatigue Fract. Eng. Mater. Struct. 38 (2015) 56–68.
  30. H. Lim, P.J. Noell, J.D. Carroll, Crystallographic orientation dependent fracture behavior in tantalum single crystals, Scr. Mater. 191 (2021) 76–80.