KaydedilenlerDerginizi ekleyin

Dergiler / Turkish Journal of Chemistry / 2016 / Cilt: 40 - Sayı: 6

Solidi ed oating organic drop microextraction for speciation of Se (IV) and Se(VI) in water samples prior to electrothermal atomic absorption spectrometricdetection

Mustafa TÜZEN
Demirhan ÇITAK
Sayfa
1012–1018
Yayın Tarihi
2022-11-03
DOI
—
🏛️Bu makalenin bibliyografik verileri ve tam metin bağlantısı DergiPark üzerinden sağlanmıştır.
DergiPark Kaydı ↗
✨

Yapay Zeka Hızlı Bakış & Çıkarımlar

AI Insight
⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

Theaccuracy of the SFODME method was con rmed with analysis of reference material (LGC 6010 Hard drinking water).The presented method was applied to water samples.

📌 3 Maddede Bu Makale

🎯
Amaç & Hipotez:A simple and fast solidi ed oating organic drop microextraction (SFODME) method is suggested for thespeciation of Se (IV) and Se (VI) in water samples prior to electrothermal atomic absorption spectrometric (ETAAS)detection.
📊
Temel Bulgular & Veri:For that purpose, 1-phenylthiosemicarbazide (PTC) was used as chelating agent and undecanol was used asextraction solvent.
💡
Sonuç & Katkı:Theaccuracy of the SFODME method was con rmed with analysis of reference material (LGC 6010 Hard drinking water).The presented method was applied to water samples.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Alan Parametreleri

Abstract

A simple and fast solidi ed oating organic drop microextraction (SFODME) method is suggested for thespeciation of Se (IV) and Se (VI) in water samples prior to electrothermal atomic absorption spectrometric (ETAAS)detection. For that purpose, 1-phenylthiosemicarbazide (PTC) was used as chelating agent and undecanol was used asextraction solvent. The pH of solution, extraction solvent volume, amount of ligand, effect of time for complex formation,and effect of possible foreign ions were also evaluated for quantitative and effective extraction of analyte. Under optimizedparameters, detection limit (0.19 g L1), limit of quanti cation (0.60 g L1), relative standard deviation (4.6%),linear range (0.60{24 g L1), relative error ({4.3%), and enrichment factor (53) were calculated, respectively. Theaccuracy of the SFODME method was con rmed with analysis of reference material (LGC 6010 Hard drinking water).The presented method was applied to water samples.

🔖

Bu Makaleye Atıf Yap

TÜZEN, M., ÇITAK, D. (2022). Solidi ed oating organic drop microextraction for speciation of Se (IV) and Se(VI) in water samples prior to electrothermal atomic absorption spectrometricdetection. Turkish Journal of Chemistry, Cilt: 40 - Sayı: 6, 1012–1018. https://ajindex.com/articles/602045

📄 Tam Metin PDF Okuyucu

📄

PDF görüntüleyici hazırlanıyor...

Kaynakça (1)

  1. Sounderajan, S.; Kiran Kumar, G.; Udas A. C.J. Hazard. Mater.2010,175, 666-672. 2.Tuzen, M.; Saygi, K. O.; Soylak, M.Talanta2007,71, 424-429. 3.Sankalia, J. M.; Mashru, R. C.; Sankalia, M. G.Spectrosc. Lett.2005,38, 61-76. 4.Shamberger, R.J. Sci. Total Environ.1981,17, 59-74. 5.Combs, G. F.Br. J. Nutr.2011,85, 517-547. 6.Sanchez-Rodas, D.; Mellano, F.; Martnez, F.; Palencia, P.; Giraldez, I.; Morales, E.Microchem. J.2016,127,120-124. 7.Maher, W.; Krikowa, F.; Foster, S.Microchem. J.2016,126, 92-95. 8.Schneider, M.; Pereira, T. R.; Castilho, I. N. B.; Carasek, E.; Welz, B.; Martens, I. B.Microchem. J.2016,125,50-55. 9.Deng, D.; Zheng, C.; Hou, X.; Wu, L.Appl. Spectrosc. Rev.2015,50, 678-705. 10.Cacho, F.; Jankuv, L.; Lauko, L.; Kroliak, M.; Manova, A.; Beinrohr, E.Talanta2013,116, 195-198. 11.Escudero, L. A.; Pacheco, P. H.; Gasquez, J. A.; Salonia, J. A.Food Chem.2015169, 73-79. 12.Asiabi, H.; Yamini, Y.; Seidi, S.; Shamsayei, M.; Safari, M.; Rezaei, F.Anal. Chim. Acta2016,922, 37-47. 13.Sarafraz-Yazdi, A.; Amiri A.Trends Anal. Chem2010,29, 1-14. 14.Pena-Pereira, F.; Lavilla, I.; Bendicho, C.Trends Anal. Chem2010,29, 617-628. 15.Kocurova, L.; Balogh, J. S.; Andruch, V.Microchem. J.2013,110, 599-607. 16.Al-Saidi, H. M.; Emara, A. A. A. J.Saudi Chem. Soc.2014,18, 745-761. 17.Wu, W. X.; Wu, Q. H.; Wang, C.; Wang, Z.Chin. Chem. Lett.2011,22, 473-476. 18.Moghadam, M. R.; Dadfarnia, S.; Shabani, A. M. H.J. Hazard. Mater.2011,186169-174. 19.Ghambariana, M.; Khalili-Zanjania, M. R.; Yamini, Y.; Esra li, A.; Yazdanfar, N.Talanta2010,81, 197-201. 20.Afzali, D.; Mohadesi, A. R.; Jahromi, B. B.; Falahnejad, M.Anal. Chim. Acta2011,684, 54-58. 21.Rivas, R. E.; Lopez-Garca, I.; Hernandez-Cordoba, M.;Anal. Methods2010,2, 225-230. 22.Pena-Pereira, F.; Lavilla, I.; Bendicho, C.Spectrochimica Acta Part B2009,64, 1-15. 23.Dadfarnia, S.; Shabani, A. M. H.; Kamranzadeh, E.Talanta2009,79, 1061-1065. 24.Dadfarnia, S.; Salmanzadeh, A. M.; Shabani, A. M. H.Anal. Chim. Acta2008,623, 163-167. 25.Wang Y. Y.; Zhao G. Y.; Chang Q. Y.; Zang X. H.; Wang, C.; Wang, Z.Chin. J. Anal Chem.2010,38, 1517-1522. 26.Fan, Z.Anal. Chim. Acta2007,585, 300-304. 27.Rivas, R. E.; Lopez-Garca,I.; Hernandez-Cordoba, M.Spectrochimica Acta Part B2009,64, 329-333. 28.Kocot, K.; Leardi, R.; Walczak, B., Sitko, R.Talanta2015,134, 360-365. 29.Tuzen, M.; Pekiner, O. Z.Food Chemistry2015,188, 619-624. 30.Zhang, Y.; Duan, J.; He, M.; Chen, B.; Hu, B.Talanta2013,115, 730-736. 31.Shabani, A. M. H.;