As a result of this study, optimum conditions were determined as amount of K2HPO4 2 g, reaction time 20 min, amount of acetylacetone 1 mL, solvent methanol and amount of solvent 10 mL
📌 3 Maddede Bu Makale
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Amaç & Hipotez:I n this work, optimum conditions for the derivatization reaction of biogenic amines histamine, tyramine, putrecine, tryptamine, phenylethylamine, cadaverine, spermidine and spermine with acetylacetone have been determined.
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Temel Bulgular & Veri:In this reaction, the amount of K2HPO4, reaction time, reagent amount, solvent choice and solvent amount were optimized.
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Sonuç & Katkı:As a result of this study, optimum conditions were determined as amount of K2HPO4 2 g, reaction time 20 min, amount of acetylacetone 1 mL, solvent methanol and amount of solvent 10 mL
I n this work, optimum conditions for the derivatization reaction of biogenic amines histamine, tyramine, putrecine, tryptamine, phenylethylamine, cadaverine, spermidine and spermine with acetylacetone have been determined. In this reaction, the amount of K2HPO4, reaction time, reagent amount, solvent choice and solvent amount were optimized. As a result of this study, optimum conditions were determined as amount of K2HPO4 2 g, reaction time 20 min, amount of acetylacetone 1 mL, solvent methanol and amount of solvent 10 mL
ASAN, A., AKMESE, B. (2022). Optimization of the Schiff-Base Reaction of Acetylacetone with Biogenic Amines. Hittite Journal of Science and Engineering, Cilt: 4 - Sayı: 1, 79–83. https://ajindex.com/articles/538074
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