Dergiler / Hacettepe Journal of Biology and Chemistry / 2007 / Cilt: 35 - Sayı: 3

Quartz crystal piezo electrode surface modification for gold nano-particles immobilization

Sayfa
203–208
Yayın Tarihi
2022-10-17
DOI
—
🏛️Bu makalenin bibliyografik verileri ve tam metin bağlantısı DergiPark üzerinden sağlanmıştır.
DergiPark Kaydı ↗
✨

Yapay Zeka Hızlı Bakış & Çıkarımlar

AI Insight
⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

Gold nanoparticles were immobilized on the modified surfaces by self-assembled monolayer (SAM) formation, for expanded crystal surface.

📌 3 Maddede Bu Makale

🎯
Amaç & Hipotez:In this study silver electrode quartz crystal surfaces were cleaned and modified to immobilize gold nanoparticles.
📊
Temel Bulgular & Veri:After the cleaning and the activation process, first cysteamine immobilization stage was performed in phosphate buffer (pH=7.0).
💡
Sonuç & Katkı:Gold nanoparticles were immobilized on the modified surfaces by self-assembled monolayer (SAM) formation, for expanded crystal surface.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Alan Parametreleri

Abstract

In this study silver electrode quartz crystal surfaces were cleaned and modified to immobilize gold nanoparticles. First, the crystal surfaces were cleaned and activated with sodium hydroxide, acetone and methanol. After the cleaning and the activation process, first cysteamine immobilization stage was performed in phosphate buffer (pH=7.0). Glutaraldehyde was used as a spacer arm and immobilized on the electrode surfaces in tetraborate buffer (pH 8.2). After then, second cysteamine immobilization step was achieved. Frequency shift were measured in all of the modification steps. Gold nanoparticles were immobilized on the modified surfaces by self-assembled monolayer (SAM) formation, for expanded crystal surface.

🔖

Bu Makaleye Atıf Yap

GÜLSU, A., AYHAN, H., AYHAN, F. (2022). Quartz crystal piezo electrode surface modification for gold nano-particles immobilization. Hacettepe Journal of Biology and Chemistry, Cilt: 35 - Sayı: 3, 203–208. https://ajindex.com/articles/529368

📄 Tam Metin PDF Okuyucu

📄

PDF görüntüleyici hazırlanıyor...

Kaynakça (13)

  1. Shubo, H.A., three-dimensional heterogeneous DNA sensing surface formed by attaching oligodeoxynucleotide-capped gold nanoparticles onto a gold coated quartz crystal, Chem. Commun., 7 (2001) 609
  2. Zhou, X.C., Microgravimetric DNA sensor based on quartz crystal microbalance: comparison of oligonucleotide immobilization methods and the application in genetic diagnosis, Biosensors and Bioelectronics, 16 (2001) 85
  3. Göpel, W. Bioelectronics and nanotechnologies, Biosensors and Bioelectronics, 13 (1998) 723
  4. DeSilva, A. P. Gunaratne, H. Q. N. McCoy, C. P., A molecular photoionic and gate based on fluorescent signalling, Nature, 364 (1993) 42
  5. Andrew N. Shipway, Nanoparticle Arrays on Surfaces for Elektronic, Optical and sensor applications, CHEMPHYSCHEM, 1 (2000) 18
  6. Csáki, A. DNA monolayer on gold substrates characterized by nanoparticle labeling and scanning force microscopy, Nucleic Acids Research, 29 (2001) 16
  7. Kimura, K. and Takashima, S., Molecular Approach to the Surface Potential Estimate of Thiolate- Modified Gold Nanoparticles, J. Phys. Chem. B, 106 (2002) 7260
  8. Lvov, Y., Munge, B., Giraldo, O., Ichinose, I., Suib, S.L., Rusling, J.F., Films of manganese oxide nanoparticles with polycations or myoglobin from alternate-layer adsorption. Langmuir, 16 (2000) 8850
  9. Tabrizi, A., Ayhan, F., Ayhan, H., Gold Nanoparticle Synthesis and Characterisation For self-assembled monolayer Immobilization on to Piezo Crystal surfaces, Journal of Biomaterial Science, Polymer Edition, (2008), submitted
  10. Koçum, C., Erdamar, A., Ayhan, H., Design of Temperature Controlled Quartz Crystal Microbalance System, Review of Scientifi Instruments, (2008) submitted
  11. Sauerbrey, G., Verwendung von Schwingquarzen zur dunner Schichten und zur. Z Phys., 155 (1959) 206
  12. Tonya M. Herne and Michael J. Tarlov, Characterization of DNA Probes Immobilized on Gold Surfaces, J. Am. Chem. Soc., 119 (1997) 8916
  13. Wang, J., Flow injection amperometric detection of OP nerve agents based on an organophosphorus– hydrolase biosensor detector, Biosensors and Bioelectronics 18 (2003) 255.