Dergiler / Records of Natural Products / 2018 / Cilt: 12 - Sayı: 2

In the present work, Microsteam distillation - Solid phase microextraction (MSD-SPME) and hydrodistillation (HD) techniques were applied to obtain volatiles from Achillea sivasica, an endemic species from Turkey. GC-FID and GC/MS analysis revealed that 1,8-cineole (22.1%) and ?-pinene (9.3%) were th

Sayfa
142–159
DOI
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Oleic and stearic acids were detected particularly in high amount in the flower lipids.

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Amaç & Hipotez:In the present work, Microsteam distillation - Solid phase microextraction (MSD-SPME) and hydrodistillation (HD) techniques were applied to obtain volatiles from Achillea sivasica, an endemic species from Turkey.
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Temel Bulgular & Veri:GC-FID and GC/MS analysis revealed that 1,8-cineole (22.1%) and ?-pinene (9.3%) were the main constituents of the hydrodistilled flower volatiles. (Z)-?-Farnesene (23.9%), decanoic acid (10.1%), ??eudesmol (8.0%), tricosane (7.3%) and hexadecanoic acid (7.2%) were the main volatiles obtained from flowers by MSDSPME.
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Sonuç & Katkı:Oleic and stearic acids were detected particularly in high amount in the flower lipids.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Alan Parametreleri

Abstract

In the present work, Microsteam distillation - Solid phase microextraction (MSD-SPME) and hydrodistillation (HD) techniques were applied to obtain volatiles from Achillea sivasica, an endemic species from Turkey. GC-FID and GC/MS analysis revealed that 1,8-cineole (22.1%) and ?-pinene (9.3%) were the main constituents of the hydrodistilled flower volatiles. (Z)-?-Farnesene (23.9%), decanoic acid (10.1%), ??eudesmol (8.0%), tricosane (7.3%) and hexadecanoic acid (7.2%) were the main volatiles obtained from flowers by MSDSPME. The leaf volatiles obtained by HD contained camphor (9.0%), ?-pinene (6.9%), 1,8-cineole (6.7%), ?-pinene (6.7%) and??-bisabolol (6.6%) as the main constituents while the leaf volatiles obtained by MSD-SPME technique were rich in (E)-geranyl acetone (10.5%), (E)-?-ionone (10.3%), camphor (10.2%), 1,8-cineole (9.6%), longiverbenone (7.9%), ?-eudesmol (7.5%), isopropyl myristate (6.7%) and epi-?-bisabolol (6.4%). The root volatiles were rich in longiverbenone (14.1%), (E)-geranyl acetone (9.3%), nonanol (12.1%) and decanol (12.5%). The enantiomeric distribution of the major volatile constituents was analyzed by using different ?-cyclodextrin chiral columns. (1R)-(+)-?-Pinene, (1S)-(-)-?-pinene, (4R)-(+)-limonene, (1R,3S,5R)-(-)-trans-pinocarveol, (1S,2R,4S)-(-)- borneol, (2S)-(-)-?-bisabolol were detected as dominant enantiomers. The lipids extracted from the flower and leaf with Folch method and methylated with BF3 reagent contained common acids: linolenic, linoleic, hexadecanoic acids. Oleic and stearic acids were detected particularly in high amount in the flower lipids.

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Bu Makaleye Atıf Yap

ÖZEK, G., TEKİN, M., HALİLOĞLU, Y., BAŞER, K. H. C., ÖZEK, T. (2018). In the present work, Microsteam distillation - Solid phase microextraction (MSD-SPME) and hydrodistillation (HD) techniques were applied to obtain volatiles from Achillea sivasica, an endemic species from Turkey. GC-FID and GC/MS analysis revealed that 1,8-cineole (22.1%) and ?-pinene (9.3%) were th. Records of Natural Products, Cilt: 12 - Sayı: 2, 142–159. https://ajindex.com/articles/308322

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Kaynakça (13)

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