KaydedilenlerDerginizi ekleyin

Dergiler / Turkish Journal of Chemistry / 2006 / Cilt: 30 - Sayı: 1

Structure of 1-(Thiophen-2-ylmethyl)-2-(thiophen-2-yl)-1H-benzimidazole

Necmi DEGE
Memet ŞEKERCİ
Süleyman SERVİ
Sayfa
103–108
Yayın Tarihi
2006-01-01
DOI
—
🏛️Bu makalenin bibliyografik verileri ve tam metin bağlantısı DergiPark üzerinden sağlanmıştır.
DergiPark Kaydı ↗
✨

Yapay Zeka Hızlı Bakış & Çıkarımlar

AI Insight
⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

N and C---H ... p contacts.

📌 3 Maddede Bu Makale

🎯
Amaç & Hipotez:The title compound, C16H12N2S2, crystallizes in the monoclinic space group P21/n with Z = 4, a = 8.950 (5) Å, b = 9.141 (5) Å, c = 17.429 (5) Å and b = 93.638 (5)°.
📊
Temel Bulgular & Veri:The benzimidazole ring is essentially planar.
💡
Sonuç & Katkı:N and C---H ... p contacts.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Turk. J. Chem. · (2006) · 103-108. Full text: pdf Other articles published in the same issue: Turk. J. Chem.

Özet

The title compound, C16H12N2S2, crystallizes in the monoclinic space group P21/n with Z = 4, a = 8.950 (5) Å, b = 9.141 (5) Å, c = 17.429 (5) Å and b = 93.638 (5)°. The benzimidazole ring is essentially planar. The crystal structure is stabilized by intermolecular C---H ... N and C---H ... p contacts.

Abstract

The title compound, C16H12N2S2, crystallizes in the monoclinic space group P21/n with Z = 4, a = 8.950 (5) Å, b = 9.141 (5) Å, c = 17.429 (5) Å and b = 93.638 (5)°. The benzimidazole ring is essentially planar. The crystal structure is stabilized by intermolecular C---H ... N and C---H ... p contacts.

🔖

Bu Makaleye Atıf Yap

DEGE, N., ŞEKERCİ, M., SERVİ, S. (2006). Structure of 1-(Thiophen-2-ylmethyl)-2-(thiophen-2-yl)-1H-benzimidazole. Turkish Journal of Chemistry, Cilt: 30 - Sayı: 1, 103–108. https://ajindex.com/articles/227787

📄 Tam Metin PDF Okuyucu

📄

PDF görüntüleyici hazırlanıyor...

Kaynakça (21)

  1. J. Lu, B. Yang and Y. Bai, Synth. Commun. 32, 3703–3709 (2002).
  2. V.K. Tandon and M. Kumar, Tetrahedron Lett. 45, 4185–4187 (2004).
  3. C. Boido, V. Boido, F. Novelli and S. Paratore, J. Heterocycl. Chem. 35, 853-858 (1998).
  4. G. Frachey, C. Crestini, R. Bernini, R. Saladino and E. Mincione, Heterocycles, 38, 2621–2630 (1994).
  5. H.I. Lee, E.H. Jeoung and C.K. Lee, J. Heterocycl. Chem. 33, 1711–1716 (1996).
  6. C.A. Ramsden and H. L. Rose, J. Chem. Soc. Perkin Trans. 16, 2319–2327 (1997).
  7. S. Servi, S. Afr. J. Chem. 55, 105–109 (2002).
  8. P. Tempest, V. Ma, S. Thomas, Z. Hua, M.G. Kelly and C. Hulme, Tetrahedron Lett. 42, 4959–4962 (2001).
  9. M.L.L. Rodriguez, B. Benhamu, M.J. Morcillo, D.I. Tejada, L. Orensaz, M. J. Alfaro and M. I. Martin, J. Med. Chem. 42, 5020–5028 (1999).
  10. T. Roth, M.L. Marningstar, P.L. Boyer, S.H. Hughes, R. W. Buckheit and C. J. Michejda, J. Med. Chem., 4199–4207 (1997). Stoe & Cie, X-AREA (Version 1.18) and X-RED32 (Version 1.04). Stoe & Cie, Darmstadt, Germany (2002).
  11. G.M. Sheldrick, SHELXL97, University of G¨ottingen, Germany (1997).
  12. L.J. Farrugia, J. Appl. Cryst. 30, 565 (1997).
  13. A.L. Spek, PLATON Molecular Grphics Program, University of Utrecht, The Netherlands (1997).
  14. L.J. Farrugia, J. Appl. Cryst. 32, 837–838 (1999).
  15. M. Ferrari Belicchi, G. Gasparri Fava, C. Pelizzi and P. Taraconi, Transition Met. Chem. 10, 295 (1985).
  16. G.R. Clark and G. J. Palenic, J. Am. Chem. Soc. 94, 4005 (1972).
  17. M. Parvez and A. P. Sabir, Acta Cryst. C52, 1572 (1996).
  18. M. Parvez, Acta Cryst. C52, 904 (1996).
  19. M. Parvez and K. Braitenbach, Acta Cryst. C56, 919 (2000).
  20. J.P. Conde, M.R.J. Elsegood and K.S. Ryder, Acta Cryst. C60, O166 (2004).
  21. C. Kazak, M. Ayg¨un, G. Turgut, M. Odaba¸so˘glu, S. ¨Ozbey and O. B¨uy¨ukg¨ung¨or, Acta Cryst. C56, 1044 (2000).