Dergiler / Turkish Journal of Chemistry / 2007 / Cilt: 31 - Sayı: 5

Direct Hydrothermal Synthesis of Palladium-Incorporated Silicate-Structured Mesoporous Catalysts

Sayfa
473–478
Yayın Tarihi
2007-05-01
DOI
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The pore size distributions of these materials were also quite narrow, indicating pores between 2 and 7 nm.

📌 3 Maddede Bu Makale

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Amaç & Hipotez:Pd-Si-structured novel mesoporous nanocomposite catalytic materials, having quite high Pd/Si ratios, were synthesized by an acidic direct hydrothermal synthesis route.
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Temel Bulgular & Veri:Unlike MCM-41, the XRD patterns indicated a rather wide d(100) band at a 2q value of about 1.9.
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Sonuç & Katkı:The pore size distributions of these materials were also quite narrow, indicating pores between 2 and 7 nm.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Mesoporous catalysts · MCM-41 · hydrothermal synthesis

Özet

Pd-Si-structured novel mesoporous nanocomposite catalytic materials, having quite high Pd/Si ratios, were synthesized by an acidic direct hydrothermal synthesis route. The nanocomposite catalytic materials were then characterized by XRD, XPS, EDS, nitrogen adsorption, and SEM techniques. Unlike MCM-41, the XRD patterns indicated a rather wide d(100) band at a 2q value of about 1.9. The materials, with very high Pd/Si wt ratios between 1.43 and 2.66, were synthesized and had BJH surface area values between 600 and 200 m2/g. The pore size distributions of these materials were also quite narrow, indicating pores between 2 and 7 nm.

Abstract

Pd-Si-structured novel mesoporous nanocomposite catalytic materials, having quite high Pd/Si ratios, were synthesized by an acidic direct hydrothermal synthesis route. The nanocomposite catalytic materials were then characterized by XRD, XPS, EDS, nitrogen adsorption, and SEM techniques. Unlike MCM-41, the XRD patterns indicated a rather wide d(100) band at a 2q value of about 1.9. The materials, with very high Pd/Si wt ratios between 1.43 and 2.66, were synthesized and had BJH surface area values between 600 and 200 m2/g. The pore size distributions of these materials were also quite narrow, indicating pores between 2 and 7 nm.

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Bu Makaleye Atıf Yap

ŞENER, C., DOĞU, T., DOĞU, G. (2007). Direct Hydrothermal Synthesis of Palladium-Incorporated Silicate-Structured Mesoporous Catalysts. Turkish Journal of Chemistry, Cilt: 31 - Sayı: 5, 473–478. https://ajindex.com/articles/184903

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