Dergiler / Bitlis Eren Üniversitesi Fen Bilimleri Dergisi / 2026 / Volume: 14 Issue: 2

Evaluation of Grinding Parameters and Microwave Pre-treatment on the Breakage Behavior and Energy Efficiency of Colemanite Ore

Serdar Yılmaz(BÜLENT ECEVİT ÜNİVERSİTESİ)0000-0002-7200-6538
Mehmet Bilen(ZONGULDAK BÜLENT ECEVİT ÜNİVERSİTESİ)0000-0003-0960-9421
Sayfa
—
Yayın Tarihi
2025-06-30
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

These findings suggest that the energy benefits of microwave-assisted grinding are marginal unless the microwave process itself is optimized for energy efficiency.

📌 3 Maddede Bu Makale

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Amaç & Hipotez:analyzing how variations in mill rotation speed and the geometry of grinding media influence the specific breakage rate.
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Temel Bulgular & Veri:The ore, sourced from the Emet Colemanite Mine, was separated into narrow particle size fractions and subjected to grinding tests at speeds between 65% and 90% of the mill’s critical velocity.
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Sonuç & Katkı:These findings suggest that the energy benefits of microwave-assisted grinding are marginal unless the microwave process itself is optimized for energy efficiency.
🔬Tür:Modelleme & Sayısal Simülasyon
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Colemanite · Specific Breakage Rate · Grinding Media Shape

Abstract

analyzing how variations in mill rotation speed and the geometry of grinding media influence the specific breakage rate. The ore, sourced from the Emet Colemanite Mine, was separated into narrow particle size fractions and subjected to grinding tests at speeds between 65% and 90% of the mill’s critical velocity. Findings indicated that higher rotational speeds resulted in increased specific breakage rates and finer particle size distributions. Moreover, cylindrical media consistently delivered better grinding performance than spherical media across all particle size intervals tested. A predictive model was developed to estimate the specific breakage rate based on particle size, rotation speed, and media shape, and was further validated under various operational conditions. Furthermore, the study examined the impact of microwave pre-treatment on colemanite grindability and energy consumption. Microwave irradiation was applied at 180 W for 5 minutes, resulting in internal thermal stress and microcracking that facilitated improved breakage, particularly in coarser fractions. Bond Work Index (BWI) values decreased by approximately 3–4% following microwave treatment—for instance, from 9.02 kWh/ton to 8.72 kWh/ton for the +3350 µm size fraction. However, the π breakage parameter remained virtually unchanged, at approximately 0.53 for both treated and untreated samples, indicating that the fundamental breakage characteristics of the material were not significantly altered. Although microwave pre-treatment enhanced grindability in specific cases, the total energy requirement for comminution—including both microwave exposure and subsequent grinding—did not demonstrate a substantial reduction. These findings suggest that the energy benefits of microwave-assisted grinding are marginal unless the microwave process itself is optimized for energy efficiency.

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Bu Makaleye Atıf Yap

Yılmaz, S., Bilen, M. (2025). Evaluation of Grinding Parameters and Microwave Pre-treatment on the Breakage Behavior and Energy Efficiency of Colemanite Ore. Bitlis Eren Üniversitesi Fen Bilimleri Dergisi, Volume: 14 Issue: 2. https://doi.org/10.17798/bitlisfen.1677736

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Kaynakça (42)

  1. P. A. Lyday, "Bromine," Minerals Yearbook, US Geological Survey, 2004. [Online]. Available: http://minerals.usgs.gov/minerals/pubs/commodity/bromine/bromimyb
  2. V. Bozkurt and I. Özgür, "Dry grinding kinetics of colemanite," Powder Technology, vol. 176, no. 2–3, pp. 88–92, 2007.
  3. D. K. Xia and C. A. Pickles, "Applications of microwave energy in extractive metallurgy: a review," CIM Bulletin, vol. 90, no. 1011, pp. 96–107, 1997.
  4. D. Bathen, "Physical waves in adsorption technology—an overview," Separation and Purification Technology, vol. 33, pp. 163–177, 2003.
  5. M. Al-Harahsheh and S. W. Kingman, "Microwave assisted leaching: a review," Hydrometallurgy, vol. 73, no. 3–4, pp. 189–203, 2004.
  6. C. A. Pickles, "Microwave heating behaviour of nickeliferous limonitic laterite ores," Minerals Engineering, vol. 17, pp. 775–784, 2004.
  7. S. Sener and G. Ozbayoglu, "Effect of heat treatment on grindability of ulexite," in Innovations in Mineral and Coal Processing, 7th Int. Mineral Processing Symp., Istanbul, Turkey, 1996, pp. 29–31.
  8. S. W. Kingman and N. A. Rowson, "Microwave treatment of minerals: a review," Minerals Engineering, vol. 11, no. 11, pp. 1081–1087, 1998.
  9. S. W. Kingman, W. Vorster, and N. A. Rowson, "The influence of mineralogy on microwave assisted grinding," Minerals Engineering, vol. 13, no. 3, pp. 313–327, 2000.
  10. A. Taşçi, "Borlanmış çeliklerin aşınma ve korozyon dayanımları," M.S. thesis, Fen Bilimleri Enstitüsü, 1993.
  11. [Online]. Available: http://www.etimaden.gov.tr/bor-mineralleri, accessed Aug. 2019.
  12. [Online]. Available: https://www.boren.gov.tr/Sayfa/bor-uretimi/27, accessed Aug. 2019.
  13. M. Silva and A. Casali, "Modeling SAG milling power and specific energy consumption including the feed percentage of intermediate size particles," Minerals Engineering, vol. 70, pp. 156–161, 2015.
  14. S. Yilmaz, "A new approach for the testing method of coal grindability," Advanced Powder Technology, vol. 30, no. 9, pp. 1932–1940, 2019.
  15. C. E. Ozer and W. J. Whiten, "A multi-component appearance function for the breakage of coal," International Journal of Mineral Processing, vol. 104–105, pp. 37–44, 2012.
  16. S. G. Malgham and D. W. Fuerstenau, "The scale-up of ball mills using PBM and specific power input," Zerkleinem. DECHEMA-Monogr., vol. 79(11), no. 1586, pp. 613–630, 1976.
  17. D. F. Kelsall, P. S. B. Stewart, and K. R. Weller, "Continuous grinding in a small wet ball mill. Part IV. A study of the influence of grinding media load and density," Powder Technology, vol. 7, no. 5, pp. 293–301, 1973.
  18. D. F. Kelsall, K. J. Reid, and C. J. Restarick, "Continuous grinding in a small wet ball mill. Part I. A study of the influence of ball diameter," Powder Technology, vol. 1, no. 5, pp. 291–300, 1968.
  19. D. F. Kelsall, K. J. Reid, and C. J. Restarick, "Continuous grinding in a small wet ball mill. Part III. A study of distribution of residence time," Powder Technology, vol. 3, no. 1, pp. 170–178, 1969.
  20. K. Shoji, S. L. G. Lohrasb, and L. G. Austin, "The variation of breakage parameters with ball and powder loading in dry ball milling," Powder Technology, vol. 25, no. 1, pp. 109–114, 1980.
  21. L. G. Austin, R. R. Klimpel, and P. T. Luckie, Process Engineering of Size Reduction: Ball Milling, New York: SME/AIME, 1984.
  22. N. Yıldız, Öğütme Teorisi, Uygulaması Değirmenler ve Sınıflandırıcılar, Ankara: TMMOB Maden Mühendisleri Odası Yayınları, 1999.
  23. M. Bilen, S. Kizgut, A. Cuhadaroglu, S. Yilmaz, and İ. Toroglu, "Coal grindability and breakage parameters," International Journal of Coal Preparation and Utilization, vol. 37, no. 5, pp. 279–284, 2017.
  24. D. Çuhadaroglu, A. A. Sirkeci, M. Bilen, S. Kizgut, S. Yilmaz, and C. E. Yilmaz, "Effect of ash reduction on the grindability of some Turkish brown coals," Unpublished.
  25. M. Bilen, S. Kızgut, S. Yilmaz, K. Baris, and D. Cuhadaroglu, "Grindability of coal changing with burial depth," International Journal of Coal Preparation and Utilization, vol. 38, no. 2, pp. 75–87, 2018.
  26. A. D. Cuhadaroglu, S. A. İ. T. Kizgut, S. Yilmaz, and Y. Zorer, "Characterization of the grinding behavior of binary mixtures of clinker and colemanite," Particulate Science and Technology, vol. 31, no. 6, pp. 596–602, 2013.
  27. A. D. Cuhadaroglu and E. Kara, "The investigation of breakage kinetics of vitrified sanitary ware wastes in laboratory scale ball and stirred mills," Particulate Science and Technology, vol. 34, no. 1, pp. 9–16, 2016.
  28. S. Samanli, D. Cuhadaroglu, and J. Y. Hwang, "An investigation of particle size variation in stirred mills in terms of breakage kinetics," Energy Sources, Part A: Recovery, Utilization, and Environmental Effects, vol. 33, no. 6, pp. 549–561, 2011.
  29. C. Bilen, "Microwave assisted limestone grinding," Particulate Science and Technology, vol. 40, no. 2, pp. 151–164, 2022.
  30. P. Prusti, K. Barik, N. Dash, S. K. Biswal, and B. C. Meikap, "Effect of limestone and dolomite flux on the quality of pellets using high LOI iron ore," Powder Technology, vol. 379, pp. 154–164, 2021.
  31. K. Li, J. Chen, J. Peng, R. Ruan, M. Omran, and G. Chen, "Dielectric properties and thermal behavior of electrolytic manganese anode mud in microwave field," Journal of Hazardous Materials, vol. 384, p. 121227, 2020.
  32. K. Li et al., "Pilot-scale study on enhanced carbothermal reduction of low-grade pyrolusite using microwave heating," Powder Technology, vol. 360, pp. 846–854, 2020.
  33. K. Li et al., "The controlled preparation and stability mechanism of partially stabilized zirconia by microwave intensification," Ceramics International, vol. 46, no. 6, pp. 7523–7530, 2020.
  34. K. Li et al., "Investigations on the microwave absorption properties and thermal behavior of vanadium slag: improvement in microwave oxidation roasting for recycling vanadium and chromium," Journal of Hazardous Materials, vol. 395, p. 122698, 2020.
  35. V. Singh, P. Dixit, R. Venugopal, and K. B. Venkatesh, "Ore pretreatment methods for grinding: Journey and prospects," Mineral Processing and Extractive Metallurgy Review, vol. 40, no. 1, pp. 1–15, 2019.
  36. Y. L. Zheng, Q. B. Zhang, and J. Zhao, "Effect of microwave treatment on thermal and ultrasonic properties of gabbro," Applied Thermal Engineering, vol. 127, pp. 359–369, 2017.
  37. D. Cuhadaroglu, S. Samanli, and S. Kizgut, "The effect of grinding media shape on the specific rate of breakage," Particulate Science and Technology, vol. 25, pp. 465–473, 2008.
  38. ASTM Standard D409-93A, Standard Test Method for Grindability of Coal by the Hardgrove-Machine Method, ASTM International, West Conshohocken, PA, 2016. [Online]. Available: https://doi.org/10.1520/D0409_D0409M-16
  39. F. Shi, "Coal breakage characterisation—Part 2: Multi-component breakage modelling," Fuel, vol. 117, pp. 1156–1162, 2014.
  40. S. K. Soni, S. C. Shukla, and G. Kundu, "Modeling of particle breakage in a smooth double roll crusher," International Journal of Mineral Processing, vol. 90, no. 1–4, pp. 97–100, 2009.
  41. F. C. Bond, "Crushing and grinding calculations, Part I," British Chemical Engineering, vol. 6, pp. 378–385, 1961.
  42. C. Bilen, "Limestone grindability in terms of HGI and a new approach for the understanding of grinding energy," Powder Technology, vol. 392, pp. 1–13, 2021.