Dergiler / Gazi University Journal of Science / 2026 / Volume: 20 Issue: 4

Determination of the Crystallographic Parameters of 2,2- Diphenyl-[1,3,2]Dithiagermole-4,5-Dicarbonitrile by Using X-Ray Powder Diffraction

Sayfa
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Yayın Tarihi
2010-03-28
DOI
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

The results of the program are in agreement with those of analytical method.

📌 3 Maddede Bu Makale

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Amaç & Hipotez:Using X-ray powder diffraction technique, diffraction pattern of compound of 2,2-diphenyl-[1,3,2]dithiagermole-4,5-dicarbonitrile was recorded.
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Temel Bulgular & Veri:According to the analytical method, the crystal system is monoclinic and unit cell parameters are; a=15.7202 Å , b=14.0053 Å , c=15.2543 Å , β=105.265º.
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Sonuç & Katkı:The results of the program are in agreement with those of analytical method.
🔬Tür:Research Article
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:X-ray powder diffraction · 2-diphenyl-[1 · 2]dithiagermole-4

Abstract

Using X-ray powder diffraction technique, diffraction pattern of compound of 2,2-diphenyl-[1,3,2]dithiagermole-4,5-dicarbonitrile was recorded. Profiting pattern, the crystal lattice and crystallographic parameters of the title compound were determined using analytic method and ITO computer program. According to the analytical method, the crystal system is monoclinic and unit cell parameters are; a=15.7202 Å , b=14.0053 Å , c=15.2543 Å , β=105.265º. Using ITO program, the type of crystal lattice was found as monoclinic and parameters of unit cell are a=15.7630 Å , b=14.0094 Å , c=15.3186 Å , β=105.451º. The results of the program are in agreement with those of analytical method.

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Bu Makaleye Atıf Yap

Güneri, E., Akkurt, M. (2010). Determination of the Crystallographic Parameters of 2,2- Diphenyl-[1,3,2]Dithiagermole-4,5-Dicarbonitrile by Using X-Ray Powder Diffraction. Gazi University Journal of Science, Volume: 20 Issue: 4. https://ajindex.com/articles/1270088

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Kaynakça (7)

  1. Eye, R. D., Wait, E., Phil, D., ‘‘X-Ray Powder Photography in Inorganic Chemistry’’, Butterworths Scientific Publications, London, 70- 97 (1960).
  2. Akkurt, M., Öztürk, S., Kök, T., Fun, H. K., “2,2- diphenyl-1,3,2-dithiagermole-4,5-dicarbonitrile”, Acta Cryst., E59, 664-665 (2003).
  3. J. W., Visser, ‘‘A Fully Automatic Program for Finding the Unit Cell from Powder Data’’, J.Appl. Cryst., 2: 89-95 (1969).
  4. H. M., Haendler, W. A., Cooney ‘‘Computer Determination of Unit-Cell from Powder- Difraction Data’’, Acta Cryst.,16: 1243-1248 (1963).
  5. User’s Manual, “Diffrac Plus WIN-INDEX Professional Powder Indexing”, Bruker AXS, Karlsruhe, 7-33, (1998).
  6. Azaroff, V., Buerger, M., ‘‘The Powder Method in X-Ray Crystallography’’, Mc. Graw-Hill Book Company, New York, 82-91 (1958).
  7. H. M., Haendler, W. A., Cooney ‘‘Computer Determination of Unit-Cell from Powder- Difraction Data’’, Acta Cryst.,16: 1243-1248 (1963).