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Journals / Gıda / 2023 / Cilt: 48 - Sayı: 2

COMPARISON OF DIFFERENT SOLID PHASE MICROEXTRACTION FIBERS IN EXTRACTION OF VOLATILE COMPOUNDS FROM ADIPOSE TISSUE

YAĞ DOKUSUNDAN UÇUCU BİLEŞENLERİN EKSTRAKSİYONUNDA FARKLI KATI FAZ MİKROEKSTRAKSİYON FİBERLERİNİN KARŞILAŞTIRILMASI

Zehra GÜLER
Ahmet DURSUN
Journal
Gıda
Pages
422–434
Publication Date
2023-04-15
DOI
—
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Furthermore, the optimum extraction time should be studied to determine the time for VCs to reach equilibrium.

📌 3 Key Takeaways

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Objective & Hypothesis:The volatile compounds (VCs) in headspace of adipose tissues (perirenal, tail, caul) were extracted by solid-phase microextraction (SPME) fiber coated with carboxen/ polydimethylsiloxane (CAR/PDMS) or divinylbenzene/ carboxen/ polydimethylsloxane (DVB/CAR/PDMS).
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Key Findings & Data:In extraction with CAR/PDMS coating compared to DVB/CAR/PDMS, more VCs were obtained in perirenal (53 versus 41), tail (51 vs 47) and caul (35 vs 33) fats.
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Conclusion & Impact:Furthermore, the optimum extraction time should be studied to determine the time for VCs to reach equilibrium.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Kuyruk yağı · aldehitler · polidimetilsiloksan

Abstract

The volatile compounds (VCs) in headspace of adipose tissues (perirenal, tail, caul) were extracted by solid-phase microextraction (SPME) fiber coated with carboxen/ polydimethylsiloxane (CAR/PDMS) or divinylbenzene/ carboxen/ polydimethylsloxane (DVB/CAR/PDMS). In extraction with CAR/PDMS coating compared to DVB/CAR/PDMS, more VCs were obtained in perirenal (53 versus 41), tail (51 vs 47) and caul (35 vs 33) fats. Increased retention index for aldehydes increased the adsorption on DVB/CAR/PDMS. This fiber also provided a good yield for carboxylic acids. CAR/PDMS fiber could be recommended for VCs from adipose tissues if the goal is to identify aldehydes, especially fatty acid oxidation products and low molecular weight hydrocarbons, as well as greater number of VCs. However, in case of targeting carboxylic acids, esters, and also high molecular weight aldehydes, DVB/CAR/PDMS could be utilized due to its high affinity for mentioned compounds. Furthermore, the optimum extraction time should be studied to determine the time for VCs to reach equilibrium.

Özet

Adipoz dokuların (böbrek, kuyruk ve gömlek yağ) tepe boşluğundan uçucu bileşenlerin ekstraksiyonu, farklı adsorbant karboksen/ polidimetilsiloksan, (CAR/PDMS) ya da divinilbenzen/ karboksen/ polidimetilsiloksan (DVB/CAR/PDMS) kaplamalı katı faz mikroekstraksiyon fiberleri ile gerçekleştirilmiştir. DVB/CAR/PDMS ile karşılaştırıldığında CAR/PDMS kaplamalı fiber ile ekstraksiyonda böbrek (53’e 41), kuyruk (51’e 47) ve gömlek (35’e 33) yağlarda daha fazla sayıda uçucu bileşen belirlenmiştir. Aldehitlerin alıkonma indeksinin artması, DVB/CAR/PDMS’e adsorpsiyonu artırmıştır. Bu fiber karboksilik asitler için de etkili bir affinite göstermiştir. Adipoz dokularda, özellikle yağ asidi oksidasyon ürünü aldehitlerin, düşük molekül ağırlıklı hidrokarbonların ve ayrıca daha fazla uçucu bileşenin tanımlanması için CAR/PDMS fiberi önerilebilir. Ayrıca, karboksilli asitler, esterler ve yüksek molekül ağırlıklı aldehitlerin belirlenmesinde ise söz edilen bileşenlere affinitesinin yüksek olması nedeniyle DVB/CAR/PDMS kullanılabilir. Bununla birlikte uçucu bileşenlerin dengeye ulaşma zamanını belirlemek için optimum ekstraksiyon sürelerinin araştırılması gerekli olabilmektedir.

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Cite This Article

GÜLER, Z., DURSUN, A. (2023). COMPARISON OF DIFFERENT SOLID PHASE MICROEXTRACTION FIBERS IN EXTRACTION OF VOLATILE COMPOUNDS FROM ADIPOSE TISSUE. Gıda, Cilt: 48 - Sayı: 2, 422–434. https://ajindex.com/articles/886153

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References (10)

  1. Alonso, A., Vazquez-Araujo, L., Garcia-Martinez, S., Ruiz, J.J., Carbonell-Barrachia, A.A. (2009). Volatile compounds of traditional and virus-resistant breeding lines of Muchamiel tomatoes. European Food Research and Technology, 230: 315–323. https://doi.org/10.1007/s00217-009-1173-2
  2. Balasubramanian, S., Panigrahi, S. (2011). Solid-phase microextraction (SPME) techniques for quality characterization of food products: A Review. Food and Bioprocess Technology, 4: 1-26. https://doi.org/10.1007/s11947-009-0299-3
  3. Bas, P., Berthelot, V., Pottier, E., Normand, J. (2007). Effect of level of linseed on fatty acid composition of muscles and adipose tissues of lambs with emphasis on trans fatty acids. Meat Science, 77: 678-688. https://doi.org/10.1016/j.meatsci.2007.05.022
  4. Body, D.R. (1977). Characterization of bovine rumen liquor isoprenoid hydrocarbons with reference to dietary phytol. Lipids, 12: 204-207. https://doi.org/10.1007/BF02533295
  5. Calkins, C.R., Hodgen, J.M. (2007). A fresh look at meat flavor. Meat Science, 77: 63-80. https://doi.org/10.1016/j.meatsci.2007.04.016
  6. Cavalli, J-F., Fernandez, X., Lizzani-Cuvelier, L., Loiseau, A-M. (2003). Comparison of static headspace, headspace solid phase microextraction, headspace sorptive extraction, and direct thermal desorption techniques on chemical composition of french olive oils. Journal of Agricultural and Food Chemistry, 51: 7709-7716. https://doi.org/10.1021/jf034834n
  7. Dursun, A., Güler, Z. (2019). Effects of types of casing with the different materials on volatile compounds (VCs) of sausages (sucuks) during the ripening. Mustafa Kemal University Journal of Agricultural Sciences, 24: 308-3016.
  8. Elmore, J.S., Cooper, S.L., Enser, M., Mottram, D.S., Sinclair, L.A., Wilkinson, R.G., Wood, J.D. (2005). Dietary manipulation of fatty acid composition in lamb meat and its effect on the volatile aroma compounds of grilled lamb. Meat Science, 69: 233-242. https://doi.org/10.1016/j.meatsci.2004.07.002
  9. Elmore, J.S., Erbahadir, M.A., Mottram, D.S. (1997). Comparison of dynamic headspace concentration on tenax with solid phase microextraction for the analysis of aroma volatiles. Journal of Agricultural and Food Chemistry, 45: 2638–2641. https://doi.org/10.1021/jf960835m
  10. Elmore, J.S., Mottram, D.S., Hierro, E. (2001). Two-fibre solid-phase microextraction combined with gas chromatography–mass spectrometry for the analysis of volatile aroma compounds in cooked pork. Journal of Chromatography A, 905: 233–240. https://doi.org/1