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Journals / Journal of Scientific Reports-A / 2022 / Sayı: 048

NEW SCHIFF BASES DERIVED from 3,4-DIAMINO-1H-1,2,4-TRIAZOLE-5(4H)-THIONE: SYNTHESIS and CHARACTERIZATION

Bülent BÜYÜKKIDAN
Nurgün BÜYÜKKIDAN
Aslı ATAR
Pages
25–41
Publication Date
2022-03-31
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The structures of the new compounds were characterized by spectral (IR, 1H and 13C NMR) and elemental analysis.

📌 3 Key Takeaways

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Objective & Hypothesis:A new synthetic approach has been applied to obtain a compound 3,4-diamino-1H-1,2,4-triazole-5(4H)-thione (2) by using 5-amino-1,3,4-thiadiazole-2-sulfonamide (1) and hydrazine hydrate as starting materials.
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Key Findings & Data:New Schiff bases (3a-d) are obtained by the reaction of the compound 3,4-diamino-1H-1,2,4-triazole-5(4H)-thione (2) and varied aldehydes.
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Conclusion & Impact:The structures of the new compounds were characterized by spectral (IR, 1H and 13C NMR) and elemental analysis.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Thione · Schiff base · Sulfonamide

Abstract

A new synthetic approach has been applied to obtain a compound 3,4-diamino-1H-1,2,4-triazole-5(4H)-thione (2) by using 5-amino-1,3,4-thiadiazole-2-sulfonamide (1) and hydrazine hydrate as starting materials. New Schiff bases (3a-d) are obtained by the reaction of the compound 3,4-diamino-1H-1,2,4-triazole-5(4H)-thione (2) and varied aldehydes. The structures of the new compounds were characterized by spectral (IR, 1H and 13C NMR) and elemental analysis.

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Cite This Article

BÜYÜKKIDAN, B., BÜYÜKKIDAN, N., ATAR, A. (2022). NEW SCHIFF BASES DERIVED from 3,4-DIAMINO-1H-1,2,4-TRIAZOLE-5(4H)-THIONE: SYNTHESIS and CHARACTERIZATION. Journal of Scientific Reports-A, Sayı: 048, 25–41. https://ajindex.com/articles/778963

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