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AI Summary & Key Takeaways
AI Insight⚡ TL;DR(Too Long; Didn't Read)
The structural determinations were accomplished by NOESY 1 H NMR and X-ray crystallography.
📌 3 Key Takeaways
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Objective & Hypothesis:Regio- and stereoselective synthesis of N -substituted azole acrylonitriles has been achieved smoothly inN, N -dimethylformamide (DMF) in the presence of potassium carbonate (K2 CO3) as a base catalyst.
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Key Findings & Data:N -Substituted azole acrylonitriles were obtained in moderate to good yields (39%–87%) with a one-pot reaction between readily available N -acetylazoles and Baylis-Hillman nitriles.
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Conclusion & Impact:The structural determinations were accomplished by NOESY 1 H NMR and X-ray crystallography.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters
Abstract
Regio- and stereoselective synthesis of N -substituted azole acrylonitriles has been achieved smoothly inN, N -dimethylformamide (DMF) in the presence of potassium carbonate (K2 CO3) as a base catalyst. N -Substituted azole acrylonitriles were obtained in moderate to good yields (39%–87%) with a one-pot reaction between readily available N -acetylazoles and Baylis-Hillman nitriles. The structural determinations were accomplished by NOESY 1 H NMR and X-ray crystallography.
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Cite This Article
AYDIN, O., KÖKTEN, Ş., ÇELİK, İ., ÜNVER, H. (2022). N -Acylazole mediated stereoselective and regioselective synthesis of N -substituted azole acrylonitriles. Turkish Journal of Chemistry, Cilt: 43 - Sayı: 4, 1134–1148. https://ajindex.com/articles/601732