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Journals / Tekstil ve Mühendis / 2020 / Cilt: 27 - Sayı: 120

Preparation of Silver Cyclohexane di Carboxylate: Β-cyclodextrin Inclusion Complexes and Their Use in the Production of Poly(vinyl alcohol) Nanowebs

Gümüş Siklohekzan Di Karboksilat: Β-Siklodekstrin Inklüzyon Komplekslerinin Hazirlanmasi Ve Polivinil Alkol Nanoağ Üretiminde Kullanimlari

Rıza ATAV
Aylin YILDIZ
Derman VATANSEVER BAYRAMOL
Ahmet Özgür AĞIRGAN
Uğur ERGÜNAY
Pages
230–235
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Obtained FTIR and TGA results showed that formation of silver cyclohexane di carboxylate (Ag-CdC): β-cyclodextrin (β-CD) inclusion complexes occurred at a mass ratio of both 1:1 and 1:2.

📌 3 Key Takeaways

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Objective & Hypothesis:In this study, guest:host inclusion complexes of silver cyclohexane di carboxylate (Ag-CdC) with β-cyclodextrin were prepared by kneading and physical mixing techniques, and analyzed via Fourier transformed infrared spectroscopy (FTIR) and thermogravimetric analyser (TGA).
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Key Findings & Data:The 1:1 and 1:2 stoichiometry of the guest:host were prepared.
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Conclusion & Impact:Obtained FTIR and TGA results showed that formation of silver cyclohexane di carboxylate (Ag-CdC): β-cyclodextrin (β-CD) inclusion complexes occurred at a mass ratio of both 1:1 and 1:2.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:β-siklodekstrin · gümüş siklohekzan di karboksilat · inklüzyon kompleks

Abstract

In this study, guest:host inclusion complexes of silver cyclohexane di carboxylate (Ag-CdC) with β-cyclodextrin were prepared by kneading and physical mixing techniques, and analyzed via Fourier transformed infrared spectroscopy (FTIR) and thermogravimetric analyser (TGA). The 1:1 and 1:2 stoichiometry of the guest:host were prepared. Obtained FTIR and TGA results showed that formation of silver cyclohexane di carboxylate (Ag-CdC): β-cyclodextrin (β-CD) inclusion complexes occurred at a mass ratio of both 1:1 and 1:2. Furthermore, these prepared inclusion complexes were doped in poly(vinyl alcohol) nanofibers during electrospinning process for obtaining nanowebs. The formation of nanowebs were investigated with scanning electron microscopy (SEM). Besides, FTIR and TGA analysis were also carried out. Results showed that both inclusion complex preparation and inclusion complex added PVA nanowebs production were successful.

Özet

Bu çalışmada, gümüş sikloheksan di karboksilat (Ag-CdC) ile β-siklodekstrin içeren konuk:konak inklüzyon kompleksleri yoğurma ve fiziksel karıştırma teknikleriyle hazırlanmış ve Fourier dönüştürülmüş kızılötesi spektroskopi (FTIR) ve termogravimetrik analizör (TGA) ile analiz edilmiştir. Konuk:konak, 1:1 ve 1:2 stokiyometri ile hazırlandı. Elde edilen FTIR ve TGA sonuçları, gümüş sikloheksan di karboksilat (Ag-CdC): β-siklodekstrin (β-CD) inklüzyon komplekslerinin oluşumunun hem 1:1 hem de 1:2'lik kütle oranında gerçekleştiğini gösterdi. Ayrıca, hazırlanan bu inklüzyon kompleksleri, nanoweb elde etmek için elektrospinning işlemi sırasında poli(vinil alkol) nanofiberlere katılmıştır. Nanoweblerin oluşumu taramalı elektron mikroskobu (SEM) ile araştırıldı. FTIR ve TGA analizleri de ayrıca yapıldı. Sonuçlar, hem inklüzyon kompleksi hazırlama hem de inklüzyon kompleksi eklenmiş PVA nanoweb üretiminin başarılı olduğunu gösterdi.

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Cite This Article

ATAV, R., YILDIZ, A., BAYRAMOL, D. V., AĞIRGAN, A. Ö., ERGÜNAY, U. (2020). Preparation of Silver Cyclohexane di Carboxylate: Β-cyclodextrin Inclusion Complexes and Their Use in the Production of Poly(vinyl alcohol) Nanowebs. Tekstil ve Mühendis, Cilt: 27 - Sayı: 120, 230–235. https://ajindex.com/articles/364709

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References (1)

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