SavedAdd your journal

Journals / Bilecik Şeyh Edebali Üniversitesi Fen Bilimleri Dergisi / 2020 / Cilt: 7 - Sayı: 1

Synthesis and Characterization of Co-Doped SnO2 Samples

Co Katkılı SnO2 Numunelerinin Sentez ve Karakterizasyonu

Tankut ATEŞ
Omer KAYGİLİ
Niyazi BULUT
Havva Esma OKUR
Serhat KESER
İ.s. YAHIA
Süleyman KÖYTEPE
Turgay SEÇKİN
İmren ÖZCAN
Turan INCE
Pages
152–160
Publication Date
2020-06-28
DOI
—
🏛️Bibliographic metadata and full text access for this article are provided via DergiPark.
DergiPark Record ↗
✨

AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The morphology was affected by Co content, and energy dispersive X-ray results verified the introduction of Co into the SnO2 structure.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:The un-doped and Co-doped SnO2 samples having high crystallinity were successfully prepared.
📊
Key Findings & Data:The effects of Co content on the structural, thermal and morphological properties of SnO2 were investigated.
💡
Conclusion & Impact:The morphology was affected by Co content, and energy dispersive X-ray results verified the introduction of Co into the SnO2 structure.
🔬Design:Research Article
📍Scope:2 samples
⚙️Variables:Crystal structure · Electron microscopy · X-ray diffraction

Abstract

The un-doped and Co-doped SnO2 samples having high crystallinity were successfully prepared. The effects of Co content on the structural, thermal and morphological properties of SnO2 were investigated. Changes in the crystallite size and unit cell parameters were detected with adding of Co. The phase composition did not alter with the addition of Co. Both X-ray diffraction and Fourier transform infrared results confirmed the formation of the SnO2 structure for each sample. The thermal stability of the as-produced samples from room temperature to 900 °C was observed. The morphology was affected by Co content, and energy dispersive X-ray results verified the introduction of Co into the SnO2 structure.

Özet

Yüksek kristalleşmeye sahip katkısız ve Co katkılı SnO2 numuneleri başarılı bir biçimde hazırlandı. Co içeriğinin SnO2’nin termal ve morfolojik özellikleri üzerine etkileri araştırıldı. Co ilavesiyle Kristal büyüklüğünde ve birim hücre parametrelerinde değişimler tespit edildi. Co ilavesiyle faz bileşimi değişmedi. Hem X-ışını kırınımı hem de Fourier dönüşümlü kızılötesi sonuçları her bir numune için SnO2 fazının oluşumunu doğruladı. Üretilen numunelerin oda sıcaklığından 900 °C’ye kadar termal kararlılığı gözlendi. Morfoloji Co içeriğinden etkilendi ve enerji dağılımlı X-ışını sonuçları SnO2 yapısı içerisine Co’ın nüfuz ettiğini doğruladı.

🔖

Cite This Article

ATEŞ, T., KAYGİLİ, O., BULUT, N., OKUR, H. E., KESER, S., YAHIA, İ., KÖYTEPE, S., SEÇKİN, T., ÖZCAN, İ., INCE, T. (2020). Synthesis and Characterization of Co-Doped SnO2 Samples. Bilecik Şeyh Edebali Üniversitesi Fen Bilimleri Dergisi, Cilt: 7 - Sayı: 1, 152–160. https://ajindex.com/articles/251549

📄 Full Text PDF Viewer

📄

PDF görüntüleyici hazırlanıyor...

References (13)

  1. Xu, L., Zeng, W., & Li, Y. (2018). Synthesis of morphology and size-controllable SnO2 hierarchical structures and their gas-sensing performance. Appl. Surf. Sci, 457, 1064–1071
  2. Das, S., & Jayaraman, V. (2014). SnO2: A comprehensive review on structures and gas sensors. Prog. Mater. Sci, 66, 112–255
  3. Palakawong, N., Sun, Y.Y., Thienprasert, J.T., Zhang, S., & Limpijumnong, S. (2017). Ga acceptor defects in SnO2 revisited: A hybrid functional study. Ceram. Int., 43, S364–S368
  4. Jiang, Q., Zhang, X., & You, J. (2018). SnO2: A wonderful electron transport layer for perovskite solar cells. Small,14, 1-14
  5. Yu, S., Zheng, H., Li, L., & Chen, S. (2017). Highly conducting and transparent antimony doped tin oxide thin films: The role of sputtering power density. Ceram. Int., 43, 5654–5660
  6. Manikandan, K., Dhanuskodi, S., Thomas, A.R., Maheswari, N., Muralidharan, G., & Sastikumar, D., (2016). Size–strain distribution analysis of SnO2 nanoparticles and their multifunctional applications as fiber optic gas sensors, supercapacitors and optical limiters. RSC Adv., 6, 90559–90570
  7. Liu, D., Pan, J., Tang, J., Liu, W., Bai, S., & Luo, R., (2019). Ag decorated SnO2 nanoparticles to enhance formaldehyde sensing properties. J. Phys. Chem. Solids., 124, 36–43
  8. Bhatnagar, M., Dhall, S., Kaushik, V., Kaushal, A., & Mehta, B.R., (2017). Improved selectivity of SnO2:C alloy nanoparticles towards H2 and ethanol reducing gases; role of SnO2:C electronic interaction, sensor. Actuat. B-Chem., 246, 336–343
  9. Wang, H., Jiang, G., Tan, X., Liao, J., Yang, X., Yuan, R., & Chai, Y., (2018). Simple preparation of SnO2/C nanocomposites for lithium ion battery anode. Inorg. Chem. Commun., 95, 67–72
  10. Li, H., Su, Q., Kang, J., Huang, M., Feng, M., Feng, H., Huang, P., & Du, G., (2018). Porous SnO2 hollow microspheres as anodes for high-performance lithium ion battery. Mater. Lett., 217, 276–280
  11. Kang, Y., Li, Z., Xu, K., He, X., Wei, S., & Cao, Y., (2019). Hollow SnO2 nanospheres with single-shelled structure and the application for supercapacitors. J. Alloys Compds., 779, 728–734
  12. Horti, N.C., Kamatagi, M.D., Patil, N.R., Wari, M.N., & Inamdar, S.R., (2018). Photoluminescence properties of SnO2 nanoparticles: Effect of solvents. Optik, 169, 314–320
  13. Razeghizadeh, A.R., Kazeminezhad, I., Zalaghi, L., & Rafee, V., (2018). Effects of sol concentration on the structural and optical properties of SnO2 nanoparticle. Iran. J. Chem. Chem. Eng., 37