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Journals / Uluslararası Çevresel Eğilimler Dergisi / 2023 / Cilt: 7 Sayı: 2

Determination of Elements in Turkish Bottled Drinking Waters Using ICP-OES: Method Validation

Türk Şişelenmiş İçme Sularındaki Elementlerin ICP-OES Kullanılarak Belirlenmesi: Yöntem Validasyonu

Fuat Gökbel(KARAMANOĞLU MEHMETBEY ÜNİVERSİTESİ, MÜHENDİSLİK FAKÜLTESİ)0000-0002-0265-1881
Numan Emre Gümüş(KARAMANOĞLU MEHMETBEY ÜNİVERSİTESİ, KAZIM KARABEKİR MESLEK YÜKSEKOKULU)
Pages
101–112
Publication Date
2023-12-31
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Method validation data results showed that the method is applicable for elemental analysis in bottled drinking water samples.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:Heavy metal pollution has been a major problem in drinking water all over the world.
📊
Key Findings & Data:Increase in water pollution due to population growth, also inadequate municipality services, people have preferred consuming bottled water more.
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Conclusion & Impact:Method validation data results showed that the method is applicable for elemental analysis in bottled drinking water samples.
🔬Design:Araştırma Makalesi
📍Scope:Comprehensive Sample
⚙️Variables:Şişelenmiş içme suları · ICP-OES · eser elementler

Abstract

Heavy metal pollution has been a major problem in drinking water all over the world. Increase in water pollution due to population growth, also inadequate municipality services, people have preferred consuming bottled water more. Hence, it is crucial to determine mineral composition of the bottled drinking water. In this study, Antimony (Sb), Arsenic (As), Beryllium (Be), Cadmium (Cd), Chromium (Cr), Cobalt (Co), Copper (Cu), Iron (Fe), Lead (Pb), Lithium (Li), Manganese (Mn), Nickel (Ni), Strontium (Sr) and Vanadium (V) were analyzed by inductively coupled plasma optic emission spectrometry (ICP-OES) in bottled drinking water samples sold in supermarkets. Linearity, limit of detection (LOD), limit of quantification (LOQ), reproducibility and recovery (%) values were determined. Method validation data results showed that the method is applicable for elemental analysis in bottled drinking water samples. As, Cr, Cu, Fe, Ni, Pb and Zn were not detected in the samples (<LOD). To evaluate the obtained data, Factor Analysis (FA) and Pearson Correlation Index (PCI), which are widely preferred statistical methods, were used. The results were compared with the limit values of the authorities' regulations Rebuplic of Türkiye Ministry of Health Regulation on Water for Human Consumption (RWHC), World Health Organization (WHO) and the United States Environmental Protection Agency (EPA). It has been determined that the measured element levels of bottled drinking water except for two samples from two brands do not pose any significant risk to human health.

Özet

Ağır metal kirliliği tüm dünyada içme suyunda önemli bir sorun olmuştur. Nüfus artışı ve yetersiz belediye hizmetleri nedeniyle su kirliliğinin artması, insanların şişelenmiş su tüketimini daha fazla tercih etmesine neden olmuştur. Bu nedenle, şişelenmiş içme suyunun mineral bileşiminin belirlenmesi büyük önem taşımaktadır. Bu çalışmada, süpermarketlerde satılan şişelenmiş içme suyu örneklerinde Antimon (Sb), Arsenik (As), Berilyum (Be), Kadmiyum (Cd), Krom (Cr), Kobalt (Co), Bakır (Cu), Demir (Fe), Kurşun (Pb), Lityum (Li), Mangan (Mn), Nikel (Ni), Stronsiyum (Sr) ve Vanadyum (V) indüktif eşleşmiş plazma optik emisyon spektrometresi (ICP-OES) ile analiz edilmiştir. Algılama sınırı (LOD), tayin sınırı (LOQ), tekrarlanabilirlik ve geri kazanım (%) değerleri belirlenmiştir. Metot validasyon verileri, metodun şişelenmiş içme suyu örneklerinde element analizi için uygulanabilir olduğunu göstermiştir. Örneklerde As, Cr, Cu, Fe, Ni, Pb ve Zn tespit edilmemiştir (<LOD). Elde edilen verileri değerlendirmek için yaygın olarak tercih edilen istatistiksel yöntemler olan Faktör Analizi (FA) ve Pearson Korelasyon İndeksi (PCI) kullanılmıştır. Sonuçlar, T.C. Sağlık Bakanlığı İnsani Tüketim Amaçlı Sular Hakkında Yönetmelik, Dünya Sağlık Örgütü (WHO) ve Amerika Birleşik Devletleri Çevre Koruma Ajansı (EPA) limit değerleri ile karşılaştırılmıştır. İki markaya ait iki numune dışında şişelenmiş içme suyunda ölçülen element seviyelerinin insan sağlığı açısından önemli bir risk oluşturmadığı tespit edilmiştir.

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Cite This Article

Gökbel, F., Gümüş, N. E. (2023). Determination of Elements in Turkish Bottled Drinking Waters Using ICP-OES: Method Validation. Uluslararası Çevresel Eğilimler Dergisi, Cilt: 7 Sayı: 2, 101–112. https://ajindex.com/articles/1565907

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