iKi KUTUPLU DAMLAMALI REAKTORDE KOBAL Till ASETAT SENTEZi ve TOZ KOBALT III ASETAT URETiMi

SYNTHESIS OF COBALT III ACETATE IN BIPOLAR TRICKLE REACTOR AND PRODUCTION OF POWDER COBALT III ACETATE

Özet

Bu cahsrnada Kobalt III Asetatmm iki kutuplu darnlamah reakrorde; granul kok kornurelektrot kullanilarak elektrokimyasal sentezi yapilrms ve organik rnaddc inyukseltgenrnelerinde katalizor olarak kullaruldrktan sonra rejenerasyonu arasunirm,Sentez verilerine; uygulanan gerilim, akirn elektrolit akis hrzlannm f "siincelenmistir. Zarnanm bir fonksiyonu olarak akim verirni, zaman vcr imi. enerji,tuketimi ve hacim zaman verirni hesaplanrrusnr.Kobalt III asetati %27'lik bir donusurnle elde edilrnis, cozelti halindeki bu urun %89.2Kobalt III asetau iceren toz urune donusturulmustur.

Abstract

In this study, Cobalt 1II acetate was electrochemically synthesized by using granulecoke electrodes in a bipolar trickle reactor and its regeneration was researched afterusing as a catalyst in the oxidation of organic compounds.The influence of applied voltage. current and the flow rates of electrolyte on thesynthesis data. Current efficiency. time efficiency. energy consumption and volumetimeyield were calculated as a function of time.Cobalt II acetate was obtained by %27 conversion, the product in the form ofsolution was converted into powder product containing %89.2 Cobalt III acetate.

Anahtar kelimeler: Kobalt III Asetat, Kobalt, ] Asetat, Sentez, Damlamah Reaktor