Dergiler / Journal of the Turkish Chemical Society, Section A: Chemistry / 2015 / Cilt: 2 - Sayı: 2
SYNTHESIS OF NANO AND MICRO PARTICLES CuSbSe2 - ONE OF HIGH RESPECTIVE SOLOR CELL COMPONENTS
- Sayfa
- 45–47
- DOI
- —
Özet
Kaliumantimoniltartrat ile bakır (I) klorür karışımı etilen glikol çözülerek üzerine selenidl?şdirici reaktif olarak sodyum selenesulfat çözeltisi ilave edilir. Deney kabı teflon küvetd? Speedwave four mikrodalga elektrik qızdırıcısında 1800C de 10 saat süreyle saklanır. Alınan çöküntü süzülür, zayıf hidroklorik asit solüsyonu, ultra saf su ve alkolle yıkandıktan sonra 60 -700C de vakumda kurutulur. Çıxım 92 - 94% teşkil etmiştir. Alınan CuSbSe2-in kimyasal, termoqrafik, morfolojik analizleri yapıldı ve kristaller nanoçubuqdan ibaret olduğu belirlenmiştir
Abstract
The mix potassium antimonytitrate with chloride of copper (I) is dissolved in ethyleneglycol and to it increases as seleniruyushchy reagent selenidesulphate sodium. The experimental ware in a teflon ditch is located in the microwave electric oven. Test within 10 hours at 1800С to temperature remains in the furnace. The received deposit is filtered via the glass filter, washed out by the diluted solution of hydrochloric acid, ultrapure water, at last, ethyl alcohol, is dried up at 60-70 C in vacuum. The exit makes 92-94%. Chemical, thermographic and morphological analyses СuSbSe2 are executed, and is established that crystals of connection are presented in the form of nanocores