Dergiler / Journal of the Turkish Chemical Society, Section A: Chemistry / 2019 / Cilt: 6 - Sayı: 2
Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6)
- Sayfa
- 97–102
- DOI
- —
Abstract
In this study, iron oxyborate (Fe3BO6) was synthesized through the solution combustion methodas a potential anode material for lithium-ion batteries. Urea, glycine, citric acid, carbohydrazide,hexamethylene tetramine, and starch were used as fuel sources and the effects of the fuels wereinvestigated. The obtained materials were structurally characterized by FT-IR, powder-XRD, solid UV-Vis,TGA and VSM. The pure crystalline Fe3BO6 was synthesized at low temperature and short reaction timeusing glycine-assisted solution combustion method. It was thermally stable up to 945 °C with a non-uniformmorphology and a highly porous structure. The magnetic properties were also studied and Fe3BO6 showsantiferromagnetic behavior.