Dergiler / Sakarya University Journal of Science / 2022 / Cilt: 26 Sayı: 5

Effect of Glutaraldehyde Crosslinking Parameters on Mechanical and Wetting Properties of PVA/NaAlg Electrospun Mat

Sayfa
990–999
Yayın Tarihi
2022-10-20
DOI
—
🏛️Bu makalenin bibliyografik verileri ve tam metin bağlantısı DergiPark üzerinden sağlanmıştır.
DergiPark Kaydı ↗
✨

Yapay Zeka Hızlı Bakış & Çıkarımlar

AI Insight
⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

The intended usage of the materials should be considered, as the concentration of the crosslinking process and duration might affect the water-soluble polymers' mechanical and wetting properties.

📌 3 Maddede Bu Makale

🎯
Amaç & Hipotez:Electrospun alginate-based materials are used in a wide range of applications, including wound dressings, tissue engineering, batteries, water treatment, bioremediation, and food packaging.
📊
Temel Bulgular & Veri:To investigate the effect of the process parameters on the mechanical properties of the materials, different concentrations (1.25, 2.5 and 5 v %) and different application times (10 min, 60 min and 24 h) of the crosslinking agent were used.
💡
Sonuç & Katkı:The intended usage of the materials should be considered, as the concentration of the crosslinking process and duration might affect the water-soluble polymers' mechanical and wetting properties.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:crosslinking · glutaraldehyde · mechanical property

Abstract

Electrospun alginate-based materials are used in a wide range of applications, including wound dressings, tissue engineering, batteries, water treatment, bioremediation, and food packaging. However, they have low resistance to water. Crosslinking is usually used to enhance the mechanical properties of water-soluble polymers. Process parameters also play a key role in the crosslinking process. In this study, materials from sodium alginate (NaAlg) and poly (vinyl alcohol) (PVA) were prepared using the electrospinning method. To investigate the effect of the process parameters on the mechanical properties of the materials, different concentrations (1.25, 2.5 and 5 v %) and different application times (10 min, 60 min and 24 h) of the crosslinking agent were used. The wettability and mechanical properties of the electrospun mats were evaluated using a water contact angle device and a tensile strength tester, respectively. The maximum tensile strength was measured at 7 MPa which is the sample treated at 5% glutaraldehyde (GA) concentration and 60 min of application time. The sample treated with 2.5% GA concentration and 60 min of treatment time had the highest measured elongation of 11.5%. The sample treated with 2.5% GA concentration and for 10 min had the lowest water contact angle, which was measured at 27.5°. The intended usage of the materials should be considered, as the concentration of the crosslinking process and duration might affect the water-soluble polymers' mechanical and wetting properties.

🔖

Bu Makaleye Atıf Yap

PAKOLPAKÇIL, A. (2022). Effect of Glutaraldehyde Crosslinking Parameters on Mechanical and Wetting Properties of PVA/NaAlg Electrospun Mat. Sakarya University Journal of Science, Cilt: 26 Sayı: 5, 990–999. https://ajindex.com/articles/940903

📄 Tam Metin PDF Okuyucu

📄

PDF görüntüleyici hazırlanıyor...

Kaynakça (11)

  1. S. Thomas, S. Gopi, A. Amalraj, Biopolymers and their industrial applications from plant, animal, and marine sources, to Functional Products, 1st ed. Elsevier, 2020
  2. M. A. Taemeh, A. Shiravandi, M. A. Korayem and H. Daemi, “Fabrication challenges and trends in biomedical applications of alginate electrospun nanofibers,” Carbohydrate Polymers, vol. 228, 115419, 2020
  3. I. P. S. Fernando, W. W. Lee, E. J. Han, G. Ahna, “Alginate-based nanomaterials: Fabrication techniques, properties, and applications,” Chemical Engineering Journal, vol. 391, 123823, 2020
  4. Grand View Research, Inc., Alginate Market Size, Share & Trends Analysis Report By Type (High M, High G), By Product (Sodium, Propylene Glycol), By Application (Pharmaceutical, Industrial), By Region, And Segment Forecasts, 2021-2028, https://www.grandviewresearch.com/industry-analysis/alginate-market (accessed on 16 March 2022)
  5. S. Ramakrishna, K. Fujihara, W. Teo, T. Lim, Z. Ma, An Introduction to Electrospinning and Nanofibers, World Scientific Publishing Co., Singapore, 2005
  6. W. Xu, R. Shen, Y. Yan, J. Gao, “Preparation and characterization of electrospun alginate/PLA nanofibers as tissue engineering material by emulsion eletrospinning,” Journal of the Mechanical Behavior of Biomedical Materials, vol. 65, pp 428-438, 2017
  7. M. A. Teixeira, M. T. P. Amorim, H. P. Felgueiras, “Poly(vinyl alcohol)-based nanofibrous electrospun scaffolds for tissue engineering applications,” Polymers, 12, 7, 2020
  8. A. Pakolpakçıl, Z. Draczynski, “Preparation and characterization of the advanced alginate-based nanofibrous nonwoven using EDC/NHS coupling agent by electrospinning,” The Journal of the Textile Institute, vol. 113, pp. 1908-1916, 2021
  9. S. Amjadi, H. Almasi, M.Ghorbani, S. Ramazani, “Preparation and characterization of TiO2NPs and betanin loaded zein/ sodium alginate nanofibers,” Food Package and Shelf Life, vol. 24, 100504, 2020
  10. M. Wang, X. Li, T. Zhang, L. Deng, P. Li, X. Wang, B. S. Hsiao, “Eco-friendly poly(acrylic acid)-sodium alginate nanofibrous hydrogel: A multifunctional platform for superior removal of Cu(II) and sustainable catalytic applications,” Colloids and Surfaces A: Physicochemical and Engineering Aspects, vol. 558, pp. 228-241, 2018
  11. Q. Wang, J. Ju, Y. Tan, L. Hao, Y. Ma, Y. Wu, H. Zhang, Y. Xia, K. Sui, “Controlled synthesis of sodium alginate electrospun nanofiber membranes for multi-occasion adsorption and separation of methylene blue,” Carbohydrate