Dergiler / Journal of the Turkish Chemical Society Section A: Chemistry / 2019 / Cilt: 6 - Sayı: 2

Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6)

Sayfa
97–102
Yayın Tarihi
2019-06-15
DOI
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

The magnetic properties were also studied and Fe3BO6 show antiferromagnetic behavior.

📌 3 Maddede Bu Makale

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Amaç & Hipotez:In this study, iron oxyborate (Fe3BO6) was first synthesized through solution combustion method as a potential anode material for lithium-ion batteries.
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Temel Bulgular & Veri:The pure crystalline Fe3BO6 was synthesized at low temperature and short reaction time using glycine assisted solution combustion method.
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Sonuç & Katkı:The magnetic properties were also studied and Fe3BO6 show antiferromagnetic behavior.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Fe3BO6 · solution combustion synthesis · fuel effect

Abstract

In this study, iron oxyborate (Fe3BO6) was first synthesized through solution combustion method as a potential anode material for lithium-ion batteries. Urea, glycine, citric acid, carbohydrazide, hexamethylene tetramine, and starch were used as fuel sources and the effects of fuels were investigated. The obtained materials were structurally characterized by FT-IR, powder-XRD and solid UV-Vis. The pure crystalline Fe3BO6 was synthesized at low temperature and short reaction time using glycine assisted solution combustion method. It was thermally stable up to 945 °C with non-uniform morphology and a highly porous structure. The magnetic properties were also studied and Fe3BO6 show antiferromagnetic behavior.

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Bu Makaleye Atıf Yap

OZER, D., ICTEN, O. (2019). Solution Combustion Synthesis of Iron Oxyborate (Fe3BO6). Journal of the Turkish Chemical Society Section A: Chemistry, Cilt: 6 - Sayı: 2, 97–102. https://ajindex.com/articles/777761

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Kaynakça (13)

  1. Ram S, Kumari K, Kotnala R. Synthesis of norbergite Fe3BO6 of single crystallites from a borate glass. Transactions of the Indian Ceramic Society. 2010;69(3):165-70
  2. Meydan E, Öztürk ÖF. Synthesis, Characterization, Magnetic Properties and Catalytic Performance of Iron Orthoborate. Asian Journal of Chemistry. 2016;28(6)
  3. Buchelnikov V, Danchin N, Dolgushin D, Isotov A, Shavrov V, Tsymbal L, et al. The magnetoacoustic anomaly in Fe3BO6. Journal of magnetism and magnetic materials. 2004;272:2113-4
  4. Tsymbal L, Bazaliy YB, Bezmaternykh L, Slawska-Waniewska A, Vasiliev S, Nedelko N, et al. Orientation phase transition in Fe 3 BO 6: Experimental determination of the order of the transition. Physical Review B. 2006;74(13):134429
  5. Kumari K. Magnetic and dielectric properties of Fe3BO6 nanoplates prepared through self-combustion method. Journal of Advanced Dielectrics. 2017;7(06):1750043
  6. Fernandes J, Guimarães R, Continentino M, Ziemath E, Walmsley L, Monteverde M, et al. Transport properties of the transverse charge-density-wave system Fe 3 O 2 BO 3. Physical Review B. 2005;72(7):075133
  7. Kumari K. Phase analysis, FTIR/Raman, and optical properties of Fe3BO6 nanocrystallites prepared by glass route at moderate temperature in ambient air. Journal of Molecular Structure. 2018;1173:417-21
  8. Beutier G, Ovchinnikova E, Collins S, Dmitrienko V-E, Lorenzo J-E, Hodeau J-L, et al. Interplay of inequivalent atomic positions in resonant x-ray diffraction of Fe3BO6. Journal of Physics: Condensed Matter. 2009;21(26):265402
  9. Ibarra-Palos A, Darie C, Proux O, Hazemann J, Aldon L, Jumas J, et al. Electrochemical reactions of iron borates with lithium: Electrochemical and in situ Mössbauer and X-ray absorption studies. Chemistry of materials. 2002;14(3):1166-73
  10. Rowsell J, Gaubicher J, Nazar L. A new class of materials for lithium-ion batteries: iron (III) borates. Journal of power sources. 2001;97:254-7
  11. Tian J, Wang B, Zhao F, Ma X, Liu Y, Liu HK, et al. Highly active Fe 3 BO 6 as an anode material for sodium-ion batteries. Chemical Communications. 2017;53(34):4698-701
  12. Shi X, Chang C, Xiang J, Xiao Y, Yuan L, Sun J. Synthesis of nanospherical Fe3BO6 anode material for lithium-ion battery by the rheological phase reaction method. Journal of Solid State Chemistry. 2008;181(9):2231-6
  13. Li S, Xu L, Zhai Y, Yu H. Co-pyrolysis synthesis of Fe 3 BO 6 nanorods as high-performance anodes for lithium-ion batteries. RSC Advances. 2014;4(16):8245-9.