Characterization of polyconidine and its derivatives was achieved by size-exclusion chromatography (SEC) with on line quadruple detection system, ATR FT-IR and UV Spectroscopy.
📌 3 Maddede Bu Makale
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Amaç & Hipotez:In this study we offer a new method to synthesize positively charged poly(1-Azabicyclo[4.2.0]octane)-common name is polyconidine- and its water-soluble polyampholyte derivative synthesized with bromoacetic acid using microwave irradiation as a model carrier system for biological macromolecules like peptides, proteins and etc. 1-Azabicyclo[4.2.0]octane containing unsubstituted four-membered azetidine ring was synthesized using microwaveassisted synthesis method and used as monomer in cationic ring-opening polymerization.
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Temel Bulgular & Veri:Different alkyl halide derivatives were used as initiators to start polymerization.
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Sonuç & Katkı:Characterization of polyconidine and its derivatives was achieved by size-exclusion chromatography (SEC) with on line quadruple detection system, ATR FT-IR and UV Spectroscopy.
🔬Tür:Modelleme & Sayısal Simülasyon
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Alan Parametreleri
Abstract
In this study we offer a new method to synthesize positively charged poly(1-Azabicyclo[4.2.0]octane)-common name is polyconidine- and its water-soluble polyampholyte derivative synthesized with bromoacetic acid using microwave irradiation as a model carrier system for biological macromolecules like peptides, proteins and etc. 1-Azabicyclo[4.2.0]octane containing unsubstituted four-membered azetidine ring was synthesized using microwaveassisted synthesis method and used as monomer in cationic ring-opening polymerization. Different alkyl halide derivatives were used as initiators to start polymerization. Microwave-assisted synthesis of polyconidine derivatives was carried out by bromoacetic acid using microwave irradiation. Characterization of polyconidine and its derivatives was achieved by size-exclusion chromatography (SEC) with on line quadruple detection system, ATR FT-IR and UV Spectroscopy.
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Bu Makaleye Atıf Yap
SARIÇAY, Y., KARABULUT, E., YOLAÇAN, Ç., MUSTAFAEVA, Z., ÖZDEMİR, Z. Ö. (2022). Microwave-assisted synthesis and characterization of poly(1-Azabicyclo[4.2.0]octane) and its water-soluble derivatives. Hacettepe Journal of Biology and Chemistry, Cilt: 36 - Sayı: 4, 319–328. https://ajindex.com/articles/529340
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