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Dergiler / Sakarya University Journal of Science / 2026 / Volume: 22 Issue: 5

Synthesis of Tin Powders Using Dynamic CRN Method

Nuray Canikoğlu(Sakarya University)0000-0003-3480-5096
Betül Özdemir0000-0001-9461-7930
Yıldız Yaralı Özbek0000-0001-9198-4612
Ali Osman Kurt0000-0002-0204-9655
Sayfa
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Yayın Tarihi
2018-10-01
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

The phases and microstructures of the powders were characterized by XRD, SEM and FESEM analyses.

📌 3 Maddede Bu Makale

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Amaç & Hipotez:Dynamic carbotermal reduction-nitridation (DCRN) is a new approach developed to produce more effective ceramic powder production than classical static system of carbothermal reduction-nitridation (CRN) method.
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Temel Bulgular & Veri:The granules were prepared using TiO 2 and carbon black powders in the stoichiometric ratio (C/TiO 2 =2).
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Sonuç & Katkı:The phases and microstructures of the powders were characterized by XRD, SEM and FESEM analyses.
🔬Tür:Research Article
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Titanium nitride · Titanium dioxide · Powder synthesis

Abstract

Dynamic carbotermal reduction-nitridation (DCRN) is a new approach developed to produce more effective ceramic powder production than classical static system of carbothermal reduction-nitridation (CRN) method. In this new technique of DCRN, powder is produced in a moving system and production takes place at relatively lower temperatures and/or shorter times than CRN method. This study examines production of TiN powder by the DCRN method. The granules were prepared using TiO 2 and carbon black powders in the stoichiometric ratio (C/TiO 2 =2). TiN powders of sub-micron were obtained in a graphite reactor from the prepared granules under N 2 gas flow. The effects of various test parameters were investigated for TiN synthesis, such as temperatures of reaction (1350-1450°C), reaction time (0.5-3 h), N 2 gas flow rate (60-120 L/h) and reactor rotation speed (2-6 rpm). The phases and microstructures of the powders were characterized by XRD, SEM and FESEM analyses.

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Bu Makaleye Atıf Yap

Canikoğlu, N., Özdemir, B., Özbek, Y. Y., Kurt, A. O. (2018). Synthesis of Tin Powders Using Dynamic CRN Method. Sakarya University Journal of Science, Volume: 22 Issue: 5. https://doi.org/10.16984/saufenbilder.384247

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