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Dergiler / Beykent Üniversitesi Fen ve Mühendislik Bilimleri Dergisi / 2026 / Cilt: 13 Sayı: 1

RADAR VE DAHA GENİŞ FREKANS ARALIĞINDA KOLEMANİT/PANI/SiO2 KOMPOZİTLERİN ELEKTROMANYETİK KALKANLAMA PERFORMANSLARI

ELECTROMAGNETIC SHIELDING PERFORMANCES OF COLEMANITE / PANI / SIO2 COMPOSITES IN RADAR AND WIDER FREQUENCY RANGES

Ethem İlhan Şahin(İSTANBUL TEKNİK ÜNİVERSİTESİ, BİLİŞİM ENSTİTÜSÜ, UYDU HABERLEŞMESİ VE UZAKTAN ALGILAMA (DR))
Mehriban Emek(ADIYAMAN ÜNİVERSİTESİ, GÖLBAŞI MESLEK YÜKSEKOKULU)
Burcu Ertug(Nisantasi University, Faculty of Engineering and Archıtecture, Department of Archıtecture)
Mesut Kartal(ISTANBUL TECHNICAL UNIVERSITY, FACULTY OF ELECTRICITY AND ELECTRONICS, DEPARTMENT OF ELECTRICAL ENGINEERING, DEPARTMENT OF ELECTRICAL ENGINEERING)
Sayfa
34–42
Yayın Tarihi
2020-06-30
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This shielding performance can be modulated simply by controlling the content of polyaniline and content of colemanite-SiO2 in the samples for the required frequency bands.

📌 3 Maddede Bu Makale

🎯
Amaç & Hipotez:In this study, colemanite-SiO2 were produced by using mixed oxide technique.
📊
Temel Bulgular & Veri:The results of the structural analysis indicated that second phase did not form in colemanite and SiO2.
💡
Sonuç & Katkı:This shielding performance can be modulated simply by controlling the content of polyaniline and content of colemanite-SiO2 in the samples for the required frequency bands.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Elektromagnetic shielding effectiveness · elektromagnetic shielding effectiveness · polyaniline

Özet

In this study, colemanite-SiO2 were produced by using mixed oxide technique. The composition was formed with various proportions for the structural analysis. The results of the structural analysis indicated that second phase did not form in colemanite and SiO2. Addionality, the colemanite/polyaniline/SiO2 composites were produced by hot pressing using the compositions of colemanite-SiO2 in different proportions and aniline. The weight ratios of colemanite-SiO2 and aniline were 1:1 respectively and epoxy resin was used to produce microwave shielding composites. The microwave shielding performances of colemanite/polyaniline/SiO2 composites were investigated by shielding effectiveness in 8 –18 GHz using two–port vector network analyzer. A minimum of – 41.1 dB shielding effectiveness performance was obtained in 16.09 GHz at the thickness of 1.5 mm. This shielding performance can be modulated simply by controlling the content of polyaniline and content of colemanite-SiO2 in the samples for the required frequency bands.

Abstract

In this study, colemanite-SiO2 were produced by using mixed oxide technique. The composition was formed with various proportions for the structural analysis. The results of the structural analysis indicated that second phase did not form in colemanite and SiO2. Addionality, the colemanite/polyaniline/SiO2 composites were produced by hot pressing using the compositions of colemanite-SiO2 in different proportions and aniline. The weight ratios of colemanite-SiO2 and aniline were 1:1 respectively and epoxy resin was used to produce microwave shielding composites. The microwave shielding performances of colemanite/polyaniline/SiO2 composites were investigated by shielding effectiveness in 8 –18 GHz using two–port vector network analyzer. A minimum of – 41.1 dB shielding effectiveness performance was obtained in 16.09 GHz at the thickness of 1.5 mm. This shielding performance can be modulated simply by controlling the content of polyaniline and content of colemanite-SiO2 in the samples for the required frequency bands.

🔖

Bu Makaleye Atıf Yap

Şahin, E. İ., Emek, M., Ertug, B., Kartal, M. (2020). RADAR VE DAHA GENİŞ FREKANS ARALIĞINDA KOLEMANİT/PANI/SiO2 KOMPOZİTLERİN ELEKTROMANYETİK KALKANLAMA PERFORMANSLARI. Beykent Üniversitesi Fen ve Mühendislik Bilimleri Dergisi, Cilt: 13 Sayı: 1, 34–42. https://doi.org/10.20854/bujse.742821

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Kaynakça (72)

  1. Yang, S., Lozano, K., Lomeli, A., Foltz H. D., and Jones, R. Composites Part A: Applied Science and Manufacturing, 2005, 36, 691-697
  2. Li, N., Huang, Y., Du, F.,. He, X., Lin, X., Gao, H., Ma, Y.,. Li, F., Chen Y., and Eklund,P. C., Nano Letters,2006, 6, 1141-1145
  3. M. H. Al-Saleh and U. Sundararaj, Carbon, 2009, 47, 1738-1746
  4. F. Shahzad, M. Alhabeb, C.B. Hatter, B. Anasori, S.M. Hong, C.M. Koo, Y.Gogotsi, Electromagnetic interference shielding with 2D transition metal carbides (MXenes), Science 353(6304) (2016) 1137-1140
  5. N. Yousefi, X. Sun, X. Lin, X. Shen, J. Jia, B. Zhang, B. Tang, M. Chan, J. K. Kim, Highly aligned graphene/polymer nanocomposites with excellent dielectric properties for high-performance electromagnetic interference shielding, Adv. Mater. 26(31) (2014) 5480-5487
  6. J. Liu, H.B. Zhang, R. Sun, Y. Liu, Z. Liu, A. Zhou, Z.Z. Yu, Hydrophobic, flexible, and lightweight MXene foams for high-performance electromagnetic-interference shielding, Adv. Mater. 29(38) (2017) 1702367
  7. F. Kargar, Z. Barani, M. Balinskiy, A.S. Magana, J.S. Lewis, A.A. Balandin,Dual-functional graphene composites for electromagnetic shielding and thermal management, Adv. Electron. Mater. 5(1) (2019) 1800558
  8. X. Jia, B. Shen, Z. Chen, L. Zhang, W. Zheng, High-performance carbonized waste corrugated boards reinforced with epoxy coating as lightweight structured electromagnetic shields, ACS Sustainable Chem. Eng. 7(22) (2019) 18718-18725
  9. X. Zhang, Y. Rao, J. Guo, G. Qin, Multiple-phase carbon-coated FeSn2/Sn nanocomposites for high-frequency microwave absorption, Carbon. 96 (2016) 972-979
  10. C.S. Zhang, Q.-Q. Ni, S.Y. Fu, K. Kurashiki, Electromagnetic interference shielding effect of nanocomposites with carbon nanotube and shape memory polymer, Compos. Sci. Technol. 67(14) (2007) 2973-2980
  11. S.H. Lee, S. Yu, F. Shahzad, J.P. Hong, W.N. Kim, C. Park, S.M. Hong, C.M. Koo, Highly anisotropic Cu oblate ellipsoids incorporated polymer composites with excellent performance for broadband electromagnetic interference shielding, Compos. Sci. Technol. 144 (2017) 57-62
  12. W.L. Song, P. Wang, L. Cao, A. Anderson, M.J. Meziani, A.J. Farr, Y.P. Sun, Polymer/boron nitride nanocomposite materials for superior thermal transport performance, Angew. Chem. Int. Ed. 51(26) (2012) 6498-6501
  13. M.J. Meziani, W.L. Song, P. Wang, F. Lu, Z. Hou, A. Anderson, H. Maimaiti, Y.-P. Sun, Boron nitride nanomaterials for thermal management applications, Chemphyschem 16(7) (2015) 1339-1346
  14. Z. Chen, D. Yi, B. Shen, L. Zhang, X. Ma, Y. Pang, L. Liu, X. Wei, W. Zheng, Semi-transparent biomass-derived macroscopic carbon grids for efficient and tunable electromagnetic shielding, Carbon 139 (2018) 271-278
  15. P. Li, Z. Jin, L. Peng, F. Zhao, D. Xiao, Y. Jin, G. Yu, Stretchable all-gel-state fiber-shaped supercapacitors enabled by macromolecularly interconnected 3D graphene/nanostructured conductive polymer hydrogels, Adv. Mater. 30(18) (2018) 1800124
  16. A. I. Gopalan, S. Komathi, N. Muthuchamy, K. P. Lee, M.J. Whitcombe, L. Dhana, G. Sai-Anand, Functionalized conjugated polymers for sensing and molecular imprinting applications, Prog. Polym. Sci. 88 (2019) 1-129
  17. W. Zhang, X. Zhang, Z. Wu, K. Abdurahman, Y. Cao, H. Duan, D. Jia, Mechanical, electromagnetic shielding and gas sensing properties of flexible cotton fiber/polyaniline composites, Compos. Sci. Technol. (2019) 107966
  18. Schnitzler, D.C., Meruvia, M.S., Hümmelgen, I., Aldo, J., Zarbin, G. Preparation and Characterization of Novel Hybrid Materials Formed from (Ti,Sn)O2 Nanoparticles and Polyaniline Chemistry of Materials 15 (24) 2003: pp. 4658 – 4665.
  19. Ma, X., Zhang, X., Li, Y., Li, G., Wang, M., Chen, H., Mi, Y. Preparation of Nano-Structured Polyaniline Composite Film Via ‘‘Carbon Nanotubes Seeding’’ Approach and its Gas-Response Studies Macromolecular Materials and Engineering 1 (291) 2006: pp. 75 – 82.
  20. Sahin, E.I., Paker S., Kartal M., 2019 “Characterization, Production and Microwave Absorbing Properties of Polyaniline-NiFe2O4: Tb Composites”,Materials Science (Medziagotyra). Vol. 25, 2019: pp. 322-327
  21. Y. Zhang, Z. Yang, Y. Yu, B. Wen, Y. Liu, M. Qiu, Tunable electromagnetic interference shielding ability in a one-dimensional bagasse fiber/polyaniline heterostructure, ACS Appl. Polym. Mater. 1 (2019) 737-745
  22. M.S. Celik, F. Suner, A Thermodynamic Analysis of the Decrepitation Process, Thermochim. Acta. 1995,254, 167
  23. R.L. Frost, Y. Xi, R. Scholz, F.M. Belotti, M. Cândido Filho, Infrared and Raman Spectroscopic Characterization of the Borate Mineral Colemanite-CaB3O4(OH)3•H2O-Implications for the Molecular Structure, J. Mol. Struct. 2013,1037, 23. doi:10.1016/j.molstruc.2012.11.047
  24. Stober, W., Fink, A., and Bohn, E., J. Colloid Interface Sci. 26, 62 (1968)
  25. Xia, Y. N., Gates, B., and Yin, Y. D., Adv. Mater. 12, 693 (2000
  26. J.N. Pereira, C.M. Costa, S.L. Mendez, Polymer composites and blends for battery separators: state of the art, challenges and future trends, J. Power Sources 281 (2015) 378–398,
  27. C.M. Costa, J.L.G. Ribelles, S.L. Mendez, G.B. Appetecchi, B. Scrosati, Poly (vinylidene fluoride)-based, co-polymer separator electrolyte membranes for lithium-ion battery systems, J. Power Sources 245 (2014) 779–786, https://doi. org/10.1016/j.jpowsour.2013.06.151
  28. N. Angulakshmi, A.M. Stephan, Electrospun trilayer polymeric membranes as separator for lithium–ion batteries, Electrochim. Acta 127 (2014) 167–172,
  29. D.J. Chen, Z.Q. Zhou, C. Feng, W.Q. Lv, Z.H. Wei, K.H.L. Zhang, B. Lin, S.H. Wu, T. Y. Lei, X.Y. Guo, G.L. Zhu, X. Jian, J. Xiong, E. Traversa, S.X. Dou, W.D. He, An upgraded lithium ion battery based on a polymeric separator incorporated with anode active materials, Adv. Energy. Mater. 9 (2019) 1803627, https://doi.org/ 10.1002/aenm.201803627
  30. Z. Feng, X.L. Ma, C.B. Cao, J.L. Li, Y.Q. Zhu, Poly(vinylidene fluoride)/SiO2 composite membranes prepared by electrospinning and their excellent properties for nonwoven separators for lithium-ion batteries, J. Power Sources 251 (2014) 423–431,
  31. E.S. Choi, S.Y. Lee, Particle size-dependent, tunable porous structure of a SiO2/poly (vinylidene fluoride-hexafluoropropylene)-coated poly(ethylene terephthalate) nonwoven composite separator for a lithium-ion battery, J. Mater. Chem. 21 (2011) 14747–14754,
  32. C.M. Costa, M. Kundu, V.F. Cardoso, A.V. Machado, M.M. Silva, S. Lanceros- Mendez, Silica/poly(vinylidene fluoride) porous composite membranes for lithiumion battery separators, J. Membr. Sci. 564 (2018) 842–851, https://doi.org/ 10.1016/j.memsci.2018.07.092
  33. Y. Chen, Y. Li, M. Yip and N. Tai, Composites Science and Technology, 2013, 80, 80-86
  34. S.-S. Tzeng and F.-Y. Chang, Materials Science and Engineering: A, 2001, 302, 258-267
  35. Chung, D.D.L. (2000). Materials for electromagnetic interference shielding, Journal of Materials Engineering and Performance., 9–350-354
  36. Ting, T. H., Yu, R. P., Jau, Y. N. (2011). Synthesis and microwave absorption characteristics of polyaniline/NiZn ferrite composites in 2–40 GHz, Materials Chemistry and Physics, 126, 364-36
  37. Yang, S., Lozano, K., Lomeli, A., Foltz H. D., and Jones, R. Composites Part A: Applied Science and Manufacturing, 2005, 36, 691-697
  38. Li, N., Huang, Y., Du, F.,. He, X., Lin, X., Gao, H., Ma, Y.,. Li, F., Chen Y., and Eklund,P. C., Nano Letters,2006, 6, 1141-1145
  39. M. H. Al-Saleh and U. Sundararaj, Carbon, 2009, 47, 1738-1746
  40. F. Shahzad, M. Alhabeb, C.B. Hatter, B. Anasori, S.M. Hong, C.M. Koo, Y.Gogotsi, Electromagnetic interference shielding with 2D transition metal carbides (MXenes), Science 353(6304) (2016) 1137-1140
  41. N. Yousefi, X. Sun, X. Lin, X. Shen, J. Jia, B. Zhang, B. Tang, M. Chan, J. K. Kim, Highly aligned graphene/polymer nanocomposites with excellent dielectric properties for high-performance electromagnetic interference shielding, Adv. Mater. 26(31) (2014) 5480-5487
  42. J. Liu, H.B. Zhang, R. Sun, Y. Liu, Z. Liu, A. Zhou, Z.Z. Yu, Hydrophobic, flexible, and lightweight MXene foams for high-performance electromagnetic-interference shielding, Adv. Mater. 29(38) (2017) 1702367
  43. F. Kargar, Z. Barani, M. Balinskiy, A.S. Magana, J.S. Lewis, A.A. Balandin,Dual-functional graphene composites for electromagnetic shielding and thermal management, Adv. Electron. Mater. 5(1) (2019) 1800558
  44. X. Jia, B. Shen, Z. Chen, L. Zhang, W. Zheng, High-performance carbonized waste corrugated boards reinforced with epoxy coating as lightweight structured electromagnetic shields, ACS Sustainable Chem. Eng. 7(22) (2019) 18718-18725
  45. X. Zhang, Y. Rao, J. Guo, G. Qin, Multiple-phase carbon-coated FeSn2/Sn nanocomposites for high-frequency microwave absorption, Carbon. 96 (2016) 972-979
  46. C.S. Zhang, Q.-Q. Ni, S.Y. Fu, K. Kurashiki, Electromagnetic interference shielding effect of nanocomposites with carbon nanotube and shape memory polymer, Compos. Sci. Technol. 67(14) (2007) 2973-2980
  47. S.H. Lee, S. Yu, F. Shahzad, J.P. Hong, W.N. Kim, C. Park, S.M. Hong, C.M. Koo, Highly anisotropic Cu oblate ellipsoids incorporated polymer composites with excellent performance for broadband electromagnetic interference shielding, Compos. Sci. Technol. 144 (2017) 57-62
  48. W.L. Song, P. Wang, L. Cao, A. Anderson, M.J. Meziani, A.J. Farr, Y.P. Sun, Polymer/boron nitride nanocomposite materials for superior thermal transport performance, Angew. Chem. Int. Ed. 51(26) (2012) 6498-6501
  49. M.J. Meziani, W.L. Song, P. Wang, F. Lu, Z. Hou, A. Anderson, H. Maimaiti, Y.-P. Sun, Boron nitride nanomaterials for thermal management applications, Chemphyschem 16(7) (2015) 1339-1346
  50. Z. Chen, D. Yi, B. Shen, L. Zhang, X. Ma, Y. Pang, L. Liu, X. Wei, W. Zheng, Semi-transparent biomass-derived macroscopic carbon grids for efficient and tunable electromagnetic shielding, Carbon 139 (2018) 271-278
  51. P. Li, Z. Jin, L. Peng, F. Zhao, D. Xiao, Y. Jin, G. Yu, Stretchable all-gel-state fiber-shaped supercapacitors enabled by macromolecularly interconnected 3D graphene/nanostructured conductive polymer hydrogels, Adv. Mater. 30(18) (2018) 1800124
  52. A. I. Gopalan, S. Komathi, N. Muthuchamy, K. P. Lee, M.J. Whitcombe, L. Dhana, G. Sai-Anand, Functionalized conjugated polymers for sensing and molecular imprinting applications, Prog. Polym. Sci. 88 (2019) 1-129
  53. W. Zhang, X. Zhang, Z. Wu, K. Abdurahman, Y. Cao, H. Duan, D. Jia, Mechanical, electromagnetic shielding and gas sensing properties of flexible cotton fiber/polyaniline composites, Compos. Sci. Technol. (2019) 107966
  54. Schnitzler, D.C., Meruvia, M.S., Hümmelgen, I., Aldo, J., Zarbin, G. Preparation and Characterization of Novel Hybrid Materials Formed from (Ti,Sn)O2 Nanoparticles and Polyaniline Chemistry of Materials 15 (24) 2003: pp. 4658 – 4665.
  55. Ma, X., Zhang, X., Li, Y., Li, G., Wang, M., Chen, H., Mi, Y. Preparation of Nano-Structured Polyaniline Composite Film Via ‘‘Carbon Nanotubes Seeding’’ Approach and its Gas-Response Studies Macromolecular Materials and Engineering 1 (291) 2006: pp. 75 – 82.
  56. Sahin, E.I., Paker S., Kartal M., 2019 “Characterization, Production and Microwave Absorbing Properties of Polyaniline-NiFe2O4: Tb Composites”,Materials Science (Medziagotyra). Vol. 25, 2019: pp. 322-327
  57. Y. Zhang, Z. Yang, Y. Yu, B. Wen, Y. Liu, M. Qiu, Tunable electromagnetic interference shielding ability in a one-dimensional bagasse fiber/polyaniline heterostructure, ACS Appl. Polym. Mater. 1 (2019) 737-745
  58. M.S. Celik, F. Suner, A Thermodynamic Analysis of the Decrepitation Process, Thermochim. Acta. 1995,254, 167
  59. R.L. Frost, Y. Xi, R. Scholz, F.M. Belotti, M. Cândido Filho, Infrared and Raman Spectroscopic Characterization of the Borate Mineral Colemanite-CaB3O4(OH)3•H2O-Implications for the Molecular Structure, J. Mol. Struct. 2013,1037, 23. doi:10.1016/j.molstruc.2012.11.047
  60. Stober, W., Fink, A., and Bohn, E., J. Colloid Interface Sci. 26, 62 (1968)
  61. Xia, Y. N., Gates, B., and Yin, Y. D., Adv. Mater. 12, 693 (2000
  62. J.N. Pereira, C.M. Costa, S.L. Mendez, Polymer composites and blends for battery separators: state of the art, challenges and future trends, J. Power Sources 281 (2015) 378–398,
  63. C.M. Costa, J.L.G. Ribelles, S.L. Mendez, G.B. Appetecchi, B. Scrosati, Poly (vinylidene fluoride)-based, co-polymer separator electrolyte membranes for lithium-ion battery systems, J. Power Sources 245 (2014) 779–786, https://doi. org/10.1016/j.jpowsour.2013.06.151
  64. N. Angulakshmi, A.M. Stephan, Electrospun trilayer polymeric membranes as separator for lithium–ion batteries, Electrochim. Acta 127 (2014) 167–172,
  65. D.J. Chen, Z.Q. Zhou, C. Feng, W.Q. Lv, Z.H. Wei, K.H.L. Zhang, B. Lin, S.H. Wu, T. Y. Lei, X.Y. Guo, G.L. Zhu, X. Jian, J. Xiong, E. Traversa, S.X. Dou, W.D. He, An upgraded lithium ion battery based on a polymeric separator incorporated with anode active materials, Adv. Energy. Mater. 9 (2019) 1803627, https://doi.org/ 10.1002/aenm.201803627
  66. Z. Feng, X.L. Ma, C.B. Cao, J.L. Li, Y.Q. Zhu, Poly(vinylidene fluoride)/SiO2 composite membranes prepared by electrospinning and their excellent properties for nonwoven separators for lithium-ion batteries, J. Power Sources 251 (2014) 423–431,
  67. E.S. Choi, S.Y. Lee, Particle size-dependent, tunable porous structure of a SiO2/poly (vinylidene fluoride-hexafluoropropylene)-coated poly(ethylene terephthalate) nonwoven composite separator for a lithium-ion battery, J. Mater. Chem. 21 (2011) 14747–14754,
  68. C.M. Costa, M. Kundu, V.F. Cardoso, A.V. Machado, M.M. Silva, S. Lanceros- Mendez, Silica/poly(vinylidene fluoride) porous composite membranes for lithiumion battery separators, J. Membr. Sci. 564 (2018) 842–851, https://doi.org/ 10.1016/j.memsci.2018.07.092
  69. Y. Chen, Y. Li, M. Yip and N. Tai, Composites Science and Technology, 2013, 80, 80-86
  70. S.-S. Tzeng and F.-Y. Chang, Materials Science and Engineering: A, 2001, 302, 258-267
  71. Chung, D.D.L. (2000). Materials for electromagnetic interference shielding, Journal of Materials Engineering and Performance., 9–350-354
  72. Ting, T. H., Yu, R. P., Jau, Y. N. (2011). Synthesis and microwave absorption characteristics of polyaniline/NiZn ferrite composites in 2–40 GHz, Materials Chemistry and Physics, 126, 364-36.