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Dergiler / Academic Platform Journal of Engineering and Smart Systems / 2018 / Volume: 6 Issue: 3

The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride

Fatma Tuğçe Şenberber(Atasehir Adiguzel Vocational School, Istanbul, Turkey)0000-0002-3257-1524
Sayfa
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Yayın Tarihi
2018-09-30
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⚡ TL;DR(1 Cümlede Hızlı Çıkarım)

The reaction yields were in the range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.

📌 3 Maddede Bu Makale

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Amaç & Hipotez:In this study, the synthesis and characterization of potassium borate were studied using KCl, NaOH and H 3 BO 3 as the starting materials.
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Temel Bulgular & Veri:The effects of the boron precursor, reaction temperature and time on the structure of the synthesized potassium borate were investigated.
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Sonuç & Katkı:The reaction yields were in the range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.
🔬Tür:Research Article
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:Hydrothermal synthesis · Potassium borate · Spectroscopy

Özet

In this study, the synthesis and characterization of potassium borate were studied using KCl, NaOH and H 3 BO 3 as the starting materials. The effects of the boron precursor, reaction temperature and time on the structure of the synthesized potassium borate were investigated. X-ray diffraction (XRD) showed the synthesized sample was santite, which has the chemical formula KB 5 O 8 4H 2 O (Powder diffraction file number: 01-1072-1688). The XRD scores increased upon decreasing the reaction temperature and time. The characteristic band values observed for boron and oxygen were investigated using Fourier transform infrared (FT-IR) and Raman spectroscopy. The morphology of the synthesized samples was characterized using scanning electron microscopy (SEM). The samples were found to be on the micro-scale with particle sizes <2.54 µm. The reaction yields were in the range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.

Abstract

In this study, the synthesis and characterization of potassium borate were studied using KCl, NaOH and H 3 BO 3 as the starting materials. The effects of the boron precursor, reaction temperature and time on the structure of the synthesized potassium borate were investigated. X-ray diffraction (XRD) showed the synthesized sample was santite, which has the chemical formula KB 5 O 8 4H 2 O (Powder diffraction file number: 01-1072-1688). The XRD scores increased upon decreasing the reaction temperature and time. The characteristic band values observed for boron and oxygen were investigated using Fourier transform infrared (FT-IR) and Raman spectroscopy. The morphology of the synthesized samples was characterized using scanning electron microscopy (SEM). The samples were found to be on the micro-scale with particle sizes <2.54 µm. The reaction yields were in the range of 75.01–95.03% for Set-1 and 72.04–92.22% for Set-2.

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Bu Makaleye Atıf Yap

Şenberber, F. T. (2018). The Effect of The Reaction Conditions on The Synthesis and Characterization of Potassium Borate from Potassium Chloride. Academic Platform Journal of Engineering and Smart Systems, Volume: 6 Issue: 3. https://doi.org/10.21541/apjes.382382

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Kaynakça (16)

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