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Dergiler / Sakarya University Journal of Science / 2023 / Cilt: 27 Sayı: 6

Determination of Pesticide Residues in Water Using Extraction Method

Ali ŞAMİL
Erdal KUŞVURAN
Sayfa
1355–1366
Yayın Tarihi
2023-12-18
DOI
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Additionally, the important values of pesticides with double benzene rings were detected in the following decreasing order: 4.4'-DDE > 4.4'-DDD > o.p'-DDE > Chlorfenapyr > 2.4'-DDD.

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Amaç & Hipotez:In this work organochlorine pesticides were first extracted from water using a solvent mixture (hexane:dichloromethane) and the quantities were then determined using a GC-MS fitted with an Electron Ionization (EI) and Selective Ion Monitoring (SIM) method.
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Temel Bulgular & Veri:At the same time changes in the recovery ratios of spike levels were seen ranging from 73.6% to 96.1% (Chlorfenapyr).
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Sonuç & Katkı:Additionally, the important values of pesticides with double benzene rings were detected in the following decreasing order: 4.4'-DDE > 4.4'-DDD > o.p'-DDE > Chlorfenapyr > 2.4'-DDD.
🔬Tür:Araştırma Makalesi
📍Kapsam:Genişletilmiş Akademik Örneklem
⚙️Değişkenler:analysis · Residue · analysis

Abstract

In this work organochlorine pesticides were first extracted from water using a solvent mixture (hexane:dichloromethane) and the quantities were then determined using a GC-MS fitted with an Electron Ionization (EI) and Selective Ion Monitoring (SIM) method. At the same time changes in the recovery ratios of spike levels were seen ranging from 73.6% to 96.1% (Chlorfenapyr). The recovery values that we found to be the lowest and greatest were 0.100 µg L-1 and 1.600 µg L-1 respectively. We also noticed that the Bromophos-ethyl, Bromophos-methyl and Chlorfenapyr pesticides had the lowest recovery efficiency. Additionally, the important values of pesticides with double benzene rings were detected in the following decreasing order: 4.4'-DDE > 4.4'-DDD > o.p'-DDE > Chlorfenapyr > 2.4'-DDD.

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Bu Makaleye Atıf Yap

ŞAMİL, A., KUŞVURAN, E. (2023). Determination of Pesticide Residues in Water Using Extraction Method. Sakarya University Journal of Science, Cilt: 27 Sayı: 6, 1355–1366. https://ajindex.com/articles/1022324

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Kaynakça (10)

  1. N. Alexandratos, J. Bruinsma, “World agriculture towards 2030/2050,”ESA Working Paper No.12-03, 2012.
  2. M. W. Bevan, R. B. Flavell, M. D. A. Chilton, “Chimaeric antibiotic resistan-ce gene as a selectable marker for plant cell transformation,” Nature, vol. 304, pp. 184-187, 1983. A. F. Hernández, T. Parrón, A.M. Tsat-sakis, M. Requena, R. Alarcon, O. L. Guarnido “Toxic effects of pesticide mixtures at a molecular level: Their relevance to human healt,” Toxicology, vol. 377, pp. 136-145, 2013.
  3. M. Kanpolat, K. Kara, T. Balkan, “Verification of QuEChERS method for the analysis of pesticide residues and their risk assessment in some fruits grown in Tokat, Turkey,” Journal of Agricultural Sciences (Tarim Bilimleri Dergisi), vol. 29, no. 2, pp. 573-588, 2023.
  4. E. B. Serbes, O. Tiryaki, “Determination of insecticide residues in Bayramiç Beyazı nectarines and their risk analysis for consumers,” Turkish Journal of Entomology, vol. 47, no. 1, pp. 73-85, 2023.
  5. D. K. Soydan, N. Turgut, M. Yalçın, C. Turgut, P. B. K. Karakuş, “Evaluation of pesticide residues in fruits and vegetables from the Aegean region of Turkey and assessment of risk to consumers,” Environmental Science and Pollution Research, vol. 28, pp. 27511-27519, 2021. P. A. Abrams, “Implications of dynami-cally variable traits for identifying, classifying and measuring direct and indirect effects in ecological communities,” The American Natura-list, vol. 146, no. 1, pp. 112-134, 1995.
  6. Z. N. Top, O. Tiryaki, B. Polat, “Monitoring and environmental risk assessment of agricultural fungicide and insecticides in water, sediment from Kumkale Plain, Çanakkale, Turkey,” Journal of Environmental Science and Health, Part B, vol. 58, pp. 304-315, 2023.
  7. B. Polat, O. Tiryaki, “Determination of insecticide residues in soils from Troia agricultural fields by the QuEChERS method,” Turkish Journal of Entomolgy, vol. 46, pp. 251-261, 2022. WHO “Public health impact of pesticides used in agriculture,” accessed june, 2019.
  8. W. Boedeker, M. Watts, P. Clausing, E. Marquez, “The global distribution of acute unintentional pesticide poisoning: estimations based on systematic review, ” BMC Public Health, vol. 20, pp. 1-19, 2020.
  9. L. Douglas, G. MacKinnon, G. Cook, H. Duncan, A. Briddon, S. Seamark, “Determination of chlorpropham (CIPC) residues in the concrete flooring of potato stores using quantitative (HPLC-UV/VIS) and qualitative (GCMS) methods,” Chemosphere, vol. 195, pp. 119-124, 2018.
  10. J. Wu, C. Tragas, H. Lord, J. Pawliszyn, “Anal