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Journals / Ata-Kimya Dergisi / 2022 / Cilt: 2 - Sayı: 1

Synthesis and structure analysis of the novel 4-(2-aminoethyl)morpholine substituted cyclotriphosphazene

Yeni 4-(2-aminoetil)morfolin substitüe siklotrifosfazenin sentezi ve yapı analizi

Elif YILDIZ GÜL
Merve BAL
Buse KÖSE
Esra TANRIVERDİ EÇİK
Pages
40–45
Publication Date
2022-11-11
DOI
—
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The possible progress mechanism of the reaction was proposed using the structure analysis of the product formed.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:In this study, the reaction of hexachlorocyclotriphosphazene with 4-(2-aminoethyl) morpholine which is a primary amine was carried out in the presence of Trimethylamine in THF.
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Key Findings & Data:The molecular structure of the final compound was confirmed by mass spectrometry, FT-IR, 31P, 1H and 13C NMR spectroscopies.
💡
Conclusion & Impact:The possible progress mechanism of the reaction was proposed using the structure analysis of the product formed.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Siklotrifosfazen · aminoetilmorfolin · NMR

Abstract

In this study, the reaction of hexachlorocyclotriphosphazene with 4-(2-aminoethyl) morpholine which is a primary amine was carried out in the presence of Trimethylamine in THF. The molecular structure of the final compound was confirmed by mass spectrometry, FT-IR, 31P, 1H and 13C NMR spectroscopies. The possible progress mechanism of the reaction was proposed using the structure analysis of the product formed.

Özet

Bu çalışmada, hekzaklorosiklotrifosfazenin primer bir amin olan 4-(2-aminoetil) morfolin ile reaksiyonu THF içerisinde trimetilamin varlığında gerçekleştirilmiştir. Final bileşiğin moleküler yapısı, kütle spektrometresi, FT-IR 31P, 1H ve 13C NMR spektroskopi teknikleri ile doğrulandı. Oluşan ürünün yapı analizi kullanılarak, reaksiyon için olası ilerleme mekanizması önerildi.

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Cite This Article

GÜL, E. Y., BAL, M., KÖSE, B., EÇİK, E. T. (2022). Synthesis and structure analysis of the novel 4-(2-aminoethyl)morpholine substituted cyclotriphosphazene. Ata-Kimya Dergisi, Cilt: 2 - Sayı: 1, 40–45. https://ajindex.com/articles/850416

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