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Journals / Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi / 2011 / Cilt: 16 - Sayı: 1

4-(5-metil-2- (2-fenilpropan-2-il) siklohekziloksi) ftalonitrilden Hazırlanan Ftalosiyaninlerin Sentezi ve Karakterizasyonu

Characterizationand Synthesis of Phthalocyanines Preparedfrom 4-(5-methyl-2-(2-phenylpropan-2-yl) cyclohexyloxy) phthalonitrile

M. Salih AĞIRTAŞ
Bedrettin SAVAŞ
Pages
12–16
Publication Date
2011-06-01
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Key words: Phthalonitrile derivative; Solubility; Magnesium; Metallophthalocyanine; Zinc.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:A new the phthalonitrile derivative was synthesized from reaction of 4- nitrophthalonitrile with 5-methyl-2-(2-phenylpropan-2-yl) cyclohexanol.
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Key Findings & Data:These compounds were characterized by elemental analysis, IR, 1H-and 13C -NMR, UV-vis, MALDI-TOF mass spectral data .
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Conclusion & Impact:Key words: Phthalonitrile derivative; Solubility; Magnesium; Metallophthalocyanine; Zinc.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Çinko · Çözünürlük · Ftalonitril türevi

Abstract

A new the phthalonitrile derivative was synthesized from reaction of 4- nitrophthalonitrile with 5-methyl-2-(2-phenylpropan-2-yl) cyclohexanol. Phthalocyanines prepared from cyclotetramerization of this phthalonitrile in present metal salts. The products were purified by several techniques such as crystallization and washed with different solvents. These compounds were characterized by elemental analysis, IR, 1H-and 13C -NMR, UV-vis, MALDI-TOF mass spectral data . Key words: Phthalonitrile derivative; Solubility; Magnesium; Metallophthalocyanine; Zinc.

Özet

5-metil-2-(2-fenilpropan-2-il)siklohekzanol ile 4-nitroftalonitrilin reaksiyonundan yeni bir ftalonitril türevi sentezlendi. Ftalosiyaninler metal tuzlarının varlığında bu ftalonitril türevinin siklotetramerizasyonundan hazırlandı. Ürünler kristallendirme ve farklı çözücülerle yıkama gibi birkaç teknikle saflaştırıldı. Bu bileşikler IR, 1H - NMR, 13C - NMR, UV-vis, MALD I- TOF kütle spektrumu ve elemental analiz ile karakterize edildi.

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Cite This Article

AĞIRTAŞ, M. S., SAVAŞ, B. (2011). 4-(5-metil-2- (2-fenilpropan-2-il) siklohekziloksi) ftalonitrilden Hazırlanan Ftalosiyaninlerin Sentezi ve Karakterizasyonu. Yüzüncü Yıl Üniversitesi Fen Bilimleri Enstitüsü Dergisi, Cilt: 16 - Sayı: 1, 12–16. https://ajindex.com/articles/725270

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