Journals / Turkish Journal of Nuclear Sciences / 2020 / Cilt: 32 - Sayı: 1

DETECTION OF IRRADIATED FOODS BY ESR AND TL METHODS IN THE SCOPE OF INTERCOMPARISON TESTS

Pages
73–84
Publication Date
2020-09-23
DOI
—
🏛️Bibliographic metadata and full text access for this article are provided via DergiPark.
DergiPark Record ↗
✨

AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

It can be concluded that immediate reach of samples to the laboratories after irradiation and relatively higher irradiation doses of samples lead to all methods being successful in this intercomparison tests, even though biological techniques are screening methods.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:Different kinds of foodstuffs such as spices and legumes (leguminosae) have been investigated whether they are irradiated or not according to TS EN standards.
📊
Key Findings & Data:These investigations have been performed as intercomparion tests on detection of irradiated foodstuffs between different laboratories in Radiation and Accelerator Technologies Department (earlier called Sarayköy Nuclear Research and Training Center -SANAEM) of Turkish Atomic Energy Authority (TAEA) and Magnetic Resonance Laboratory of Physics Engineering Department in Hacettepe University to fulfill the accreditation requirements of TS EN ISO/IEC 17025 standard.
💡
Conclusion & Impact:It can be concluded that immediate reach of samples to the laboratories after irradiation and relatively higher irradiation doses of samples lead to all methods being successful in this intercomparison tests, even though biological techniques are screening methods.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Keywords: foodstuffs · irradiation · EN 1787 -1788

Abstract

Different kinds of foodstuffs such as spices and legumes (leguminosae) have been investigated whether they are irradiated or not according to TS EN standards. These investigations have been performed as intercomparion tests on detection of irradiated foodstuffs between different laboratories in Radiation and Accelerator Technologies Department (earlier called Sarayköy Nuclear Research and Training Center -SANAEM) of Turkish Atomic Energy Authority (TAEA) and Magnetic Resonance Laboratory of Physics Engineering Department in Hacettepe University to fulfill the accreditation requirements of TS EN ISO/IEC 17025 standard. SANAEM's Quality Management Section (QMS) organized these intercomparison tests by carrying out stages such as the provision of foodstuffs, irradiation, distribution of samples to laboratories and evaluation of results. The samples were irradiated with Co-60 gamma cell at the SANAEM. Randomly coded samples were provided to the laboratories. The foodstuffs samples were analyzed using various methods proposed as EN standards: (1) Physical techniques TS EN 1787: Electron Spin Resonance (ESR) technique for foodstuffs containing cellose and TS EN 1788: thermoluminescence (TL) technique and biological techniques. The results evaluation was done according to criteria as correctly detection of irradiated /unirradiated samples by the QMS. We present here the details of physical methods applying ESR ans TL techniques to detect irradiated/unirradiated foods which were chickpea, beans, lentil red, red mullet,lentil green, mint, cumin, ground cumin, thyme, black pepper, red pepper and pistachio. As QMS reported, the results of ESR and TL methods were considered satisfactory like all methods. It can be concluded that immediate reach of samples to the laboratories after irradiation and relatively higher irradiation doses of samples lead to all methods being successful in this intercomparison tests, even though biological techniques are screening methods.

🔖

Cite This Article

ÇAM, S. T., TETİK, C. A., AYDIN, T. (2020). DETECTION OF IRRADIATED FOODS BY ESR AND TL METHODS IN THE SCOPE OF INTERCOMPARISON TESTS. Turkish Journal of Nuclear Sciences, Cilt: 32 - Sayı: 1, 73–84. https://ajindex.com/articles/70734

📄 Full Text PDF Viewer

📄

PDF görüntüleyici hazırlanıyor...

References (14)

  1. Anonymous. Wholesomeness of Irradiated Food. (1981). Report of Joint FAO/IAEA/WHO Expert Commitiee. World Health Organisation, Geneva. Technical Report Series 659
  2. Bayram G. & Delincée H. (2004). Identification of irradiated Turkish foodstuffs combining various physical detection methods. Food Control, 15, 2,81-91
  3. Raffi, J., Evans, J.C., Agnel, J.P., Rowlands, C.C. & Lesgards, G. (1989). ESR analysis of irradiated frog's legs and fishes. Applied Radiation and Isotopes 40, 1215-1218
  4. Desrosiers, M.F. (1991). Electron spin resnance for monitoring radiation-processed meats containing bone. Journal of Food Science. 56, 1104- 1105
  5. Raffi,J., Yordanov,N.D., Chabane,S., Douifi,L., Gancheva,V. & Ivanova,S. (2000). Identification of Irradiation Treatment of Aromatic Herbs, Spices and Fruits by Electron Paramagnetic Resonance and Thermoluminescence. Spectrochim. ActaA, 56, 409–416
  6. Korkmaz, M. & Polat, M. (2001). Radical kinetics and characterization of the free radicals in gamma irradiated red pepper. Radiation Physics and Chemistry, 62, 411–421
  7. Polovka, M., Brezova,V., Stasko,A., Mazur, M., Suhaj, M. & Simko, P. (2006). EPR investigations of gamma-irradiated ground black pepper. Radiation Physics and Chemistry, 75, 309–321
  8. EN 13708, Determination of Irradiated Food Containing Crystalline Sugar:Analysis by EPR. (2001). European Committee for Standardization: Brussels
  9. EN 1786, Detection of Irradiated Food Containing Bone: Analysis by Electron Paramagnetic Resonance. (1997). European Committee for Standardization: Brussels
  10. EN 1787, Determination of Irradiated Food Containing Cellulose: Analysis by EPR. (2000). European Committee for Standardization: Brussels
  11. Yordanov, N.D. & Gancheva,V. (2000). A new approach for extension of the identification period of irradiated cellulose containing foodstuffs by EPR spectroscopy. Applied Radiation and Isotopes. 52, 195–198
  12. Engin, B., Aydaş, C. & Polat, M. (2011). Detection of gamma irradiated fig seeds by analysing electron spin resonance. Food Chemistry. 126, 1877–1882
  13. Yordanov, N.D. & Aleksieva, K. (2004). X- and Q- band studies on fine powders of irradiated plants. New approach for detection of their radiation history by using Q-band EPR spectrometry. Radiation Physics and Chemistry. 69, 59–64
  14. Yordanov, N.D., Aleksieva, K. & Mansour,I. (2005). Improvement of the EPR detection of irradiated dry plants using microwave saturation and thermal treatment. Radiation Physics and Ch