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Journals / Turkish Journal of Chemistry / 2009 / Cilt: 33 - Sayı: 2

Synthesis, spectral characterization, and antimicrobial activity of arsenic (ııı) and bismuth (ııı) tri (3(2'-hydroxyphenyl)-5-(4-subsituted phenyl) pyrazolinates)

Arpan BHARDWAJ
Tulsi Ram THAPAK
Umesh Nath TRIPATHI
Mohammad Safi AHMAD
Afshan SIDDIQUI
Jeeven Singh SOLANKI
Pages
257–266
Publication Date
2022-11-05
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Antibacterial and antifungal potential of free pyrazoline and some arsenic(III) tripyrazolinates and bismuth(III) tripyrazolinates have also been discussed.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:Arsenic(III) tripyrazolinates and bismuth(III) tripyrazolinates of the type M(C15H12N2OX) 3 [where C15H12N2OX = 3(2’-hydroxyphenyl)-5-(4-substituted phenyl)pyrazoline] have been synthesized by the reaction of MCl 3 and sodium salt of pyrazolines in 1:3 molar ratio in anhydrous benzene at elevated temperature.
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Key Findings & Data:These newly synthesized derivatives have been characterized by elemental analysis (C, H, N, As, and Bi), molecular weight measurement, spectral [IR and multinuclear NMR ( 1H & 13 C)] and x-ray diffraction studies.
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Conclusion & Impact:Antibacterial and antifungal potential of free pyrazoline and some arsenic(III) tripyrazolinates and bismuth(III) tripyrazolinates have also been discussed.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

Arsenic(III) tripyrazolinates and bismuth(III) tripyrazolinates of the type M(C15H12N2OX) 3 [where C15H12N2OX = 3(2’-hydroxyphenyl)-5-(4-substituted phenyl)pyrazoline] have been synthesized by the reaction of MCl 3 and sodium salt of pyrazolines in 1:3 molar ratio in anhydrous benzene at elevated temperature. These newly synthesized derivatives have been characterized by elemental analysis (C, H, N, As, and Bi), molecular weight measurement, spectral [IR and multinuclear NMR ( 1H & 13 C)] and x-ray diffraction studies. The bonding mode of pyrazolines and coordination no. of arsenic(III) and bismuth(III) in these derivatives have been discussed. Antibacterial and antifungal potential of free pyrazoline and some arsenic(III) tripyrazolinates and bismuth(III) tripyrazolinates have also been discussed.

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Cite This Article

BHARDWAJ, A., THAPAK, T. R., TRIPATHI, U. N., AHMAD, M. S., SIDDIQUI, A., SOLANKI, J. S. (2022). Synthesis, spectral characterization, and antimicrobial activity of arsenic (ııı) and bismuth (ııı) tri (3(2'-hydroxyphenyl)-5-(4-subsituted phenyl) pyrazolinates). Turkish Journal of Chemistry, Cilt: 33 - Sayı: 2, 257–266. https://ajindex.com/articles/602133

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