Journals / Turkish Journal of Chemistry / 2016 / Cilt: 40 - Sayı: 6

An application of coacervate-based extraction for the separation andpreconcentration of cadmium, lead, and nickel ions prior to their determinationby ame atomic absorption spectrometry in various water samples

Pages
979–987
Publication Date
2022-11-05
DOI
—
🏛️Bibliographic metadata and full text access for this article are provided via DergiPark.
DergiPark Record ↗
✨

AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

In addition, the method was successfully implemented for thedetermination of Cd(II), Pb(II), and Ni(II) in water samples and standard reference materials and satisfactory recoveryvalues were obtained.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:Cloud point extraction (CPE), which is the most popular coacervate-based extraction method, was utilizedfor the separation and preconcentration of trace amounts of cadmium, lead, and nickel.
📊
Key Findings & Data:Quinalizarin was used ascomplexing agent and Triton X-114 was used as surfactant.
💡
Conclusion & Impact:In addition, the method was successfully implemented for thedetermination of Cd(II), Pb(II), and Ni(II) in water samples and standard reference materials and satisfactory recoveryvalues were obtained.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

Cloud point extraction (CPE), which is the most popular coacervate-based extraction method, was utilizedfor the separation and preconcentration of trace amounts of cadmium, lead, and nickel. Quinalizarin was used ascomplexing agent and Triton X-114 was used as surfactant. After extraction, analyte ions were determined by ameatomic absorption spectrometry. The detection limits (3s) of 1.8 g L1for Cd(II), 3.2 g L1for Pb(II), and 2.8 g L1for Ni(II) were obtained using 50 mL of solutions. The relative standard deviation was calculated as 4.3% for10 g L1Cd(II), 4.9% for 50 g L1Pb(II), and 4.6% for 50 g L1Ni(II). Obtained enrichment factors of Cd(II),Pb(II), and Ni(II) were 144, 129 and 92, respectively. In addition, the method was successfully implemented for thedetermination of Cd(II), Pb(II), and Ni(II) in water samples and standard reference materials and satisfactory recoveryvalues were obtained.

🔖

Cite This Article

TEMUGE, İ. D., BEKTAS, S., SATTI, A. A., ŞAHİN, Ç. A. (2022). An application of coacervate-based extraction for the separation andpreconcentration of cadmium, lead, and nickel ions prior to their determinationby ame atomic absorption spectrometry in various water samples. Turkish Journal of Chemistry, Cilt: 40 - Sayı: 6, 979–987. https://ajindex.com/articles/602048

📄 Full Text PDF Viewer

📄

PDF görüntüleyici hazırlanıyor...

References (1)

  1. Emoyan, O. O.; Ogban, F. E.; Akarah, E.J. Appl. Sci. Environ. Mgt.2006,10, 121-127. 2.Mekkawy, I. A. A.; Mahmoud U. M.; Wassif, E. T.; Naguib, M.Fish. Physiol. Biochem.2011,37, 71-84. 3.Monteiro, C. M.; Fonseca, S. C.J. Appl. Phycol.2011,23, 97-103. 4.Naeemullah; Kazi, T. G.; Afridi, H. I.; Shah, F.; Arain, S. S.; Brahman, K. D.; Ali, J.; Arain, M. S.Arab. J. Chem.2016,9, 105-113. 5.Aras, N. K.; Ataman, O. Y.Trace Element Analysis of Food and Diet, Royal Society of Chemistry: Cambridge,UK, 2006, pp. 241. 6.Sauer, A.; Cohen, H.; Meyerstein, D.Inorg. Chem.1988,27, 4578-4581. 7.Jabri, E.; Karplus, P. A.Biochem.1996,35, 10616-10626. 8.Shemirani, F.; Jamali, M. R.; Kozani, R. R.Sep. Sci. Tech.2006,41, 3065-3077. 9.Krawczyk, M.; Jeszka-Skowron, M.Microchem. J.2016,126, 296-301. 10.Tuzen, M; Melek, E.; Soylak, M.J. Hazard. Mater.2006,136, 597-603. 11.Durukan, I.; Arpa Sahin, C.; Satroglu, N.; Bektas, S.Microchem. J.2011,99, 159-163. 12.Melnyk, A.; Namiesnik, J.; Wolska, L.Trac-Trend. Anal. Chem.2015,71, 282-292. 13.Moftakhara, M. K.; Yaftiana, M. R.; Zamanib, A.J. Anal. Chem.2015,70, 1085-1091. 14.Abd El-Hay, S. S.; Gouda, A. A.J. Radioanal. Nucl. Chem.DOI 10.1007/s10967-016-4780-y. 15.Shemirani, F.; Baghdadi, M.; Ramezani, M.; Jamali, M. R.Anal. Chim. Acta2005,534, 163-169. 16.Durukan, I.; Soylak, M.; Dogan, M.Atom. Spectrosc.2013,34, 20-25. 17.Satroglu, N.; Arpa C.Microchim. Acta2008,162, 107-112. 18.Ghaedi, M.; Shokrollahi, A.; Niknam, K.; Niknam, E.; Najibi, A.; Soylak, M.J. Hazard. Mater.2009,168, 1022-1027. 19.Coelho, L. M.; Arruda, M. A. Z.Spectrochim. Acta B2005,60, 743-748. 20.Fan, C.; Luo, S; Liu, R.RSC Adv.2015,5, 65321-65327. 21.Rahnama, R.; Naja, M.Environ. Monit. Assess.2016,188, 150-159 22.Xiang, G.; Wen, S.; Wu, X.; Jiang, X.; He, L.; Liu, Y.Food Chem.2012,132, 532-536. 23.Citak, D.; Tuzen, M.Food Chem. Toxicol.2010,48, 1399-1404. 24.Galbeiro, R.; Garcia, S.; Gaubeur, I.J. Trace Elem. Med. Biol.2014,28, 160-165. 25.Wen, X.; Deng, Q.; Ji, S.; Yang, S.; Li, S.Microchem. J.2012,100, 31-35. 26.Naeemullah, Kazi, T. G.; Tuzen, M.J. Ind. Eng. Chem.2016,35, 93-98.987