Journals / Turkish Journal of Chemistry / 2018 / Cilt: 42 - Sayı: 2

Voltammetric determination of vanillin in commercial food products using overoxidized poly(pyrrole) film-modified glassy carbon electrodes

Pages
291–305
Publication Date
2022-11-01
DOI
—
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Moreover, the proposed method was successfully used for the assessment of vanillin contents in commercial food products with satisfactory results.

📌 3 Key Takeaways

🎯
Objective & Hypothesis:In this work, a very simple, rapid, cheap, sensitive, and selective polymer film-modified electrode for vanillin determination in commercial food products was developed via electrochemical polymerization and overoxidation of pyrrole.
📊
Key Findings & Data:Under optimized conditions, the calibration graph comprises two linear segments of $0.032–1.500 µmol L ^{−1} and 3.00–150.00 µmol L ^{−1} with a detection limit of 0.012 µmol L ^{−1}$.
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Conclusion & Impact:Moreover, the proposed method was successfully used for the assessment of vanillin contents in commercial food products with satisfactory results.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

In this work, a very simple, rapid, cheap, sensitive, and selective polymer film-modified electrode for vanillin determination in commercial food products was developed via electrochemical polymerization and overoxidation of pyrrole. The formation of both poly(pyrrole) and overoxidized poly(pyrrole) films on a glassy carbon electrode surface was characterized by electrochemical impedance spectroscopy, scanning electron microscopy, and X-ray photoelectron spectroscopy. Under optimized conditions, the calibration graph comprises two linear segments of $0.032–1.500 µmol L ^{−1} and 3.00–150.00 µmol L ^{−1} with a detection limit of 0.012 µmol L ^{−1}$. The selectivity of the modified electrode was examined in the presence of metals, inorganic ions, and organic substances. Moreover, the proposed method was successfully used for the assessment of vanillin contents in commercial food products with satisfactory results.

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Cite This Article

KARABİBEROĞLU, Ş. U., KOÇAK, Ç. C. (2022). Voltammetric determination of vanillin in commercial food products using overoxidized poly(pyrrole) film-modified glassy carbon electrodes. Turkish Journal of Chemistry, Cilt: 42 - Sayı: 2, 291–305. https://ajindex.com/articles/601839

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