Journals / Pamukkale Üniversitesi Mühendislik Bilimleri Dergisi / 2020 / Cilt: 26 - Sayı: 7

Production of essential oil-based composite nanofibers by emulsionelectrospinning

Emülsiyon elektro lif çekim yöntemi ile uçucu yağ esaslı kompozit nanoliflerin üretimi

Pages
1178–1185
Publication Date
2022-10-18
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

While the addition of gelatin affected solution properties and average fiber diameter, the addition of LEO did not affect fiber properties.

📌 3 Key Takeaways

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Objective & Hypothesis:Abstract ÖzThis study aimed to produce polyvinylpyrrolidone (PVP)/gelatin (GEL)/lavender essential oil (LEO)-based nanofibers by means of oil-inwater emulsion electrospinning.
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Key Findings & Data:As gelatin was added to the PVP solution, viscosity was found to increase while surface tension and conductivity decreased.
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Conclusion & Impact:While the addition of gelatin affected solution properties and average fiber diameter, the addition of LEO did not affect fiber properties.
🔬Design:Modeling & Simulation
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

Abstract ÖzThis study aimed to produce polyvinylpyrrolidone (PVP)/gelatin (GEL)/lavender essential oil (LEO)-based nanofibers by means of oil-inwater emulsion electrospinning. Firstly, the polymer solution properties were measured, and then optimization of nanofiber production and characterization of the nanofibrous web were carried out. As gelatin was added to the PVP solution, viscosity was found to increase while surface tension and conductivity decreased. PVP/GEL (50/50) was determined to be the optimum sample in terms of nanoweb quality, fiber diameter, diameter uniformity, and gelatin content. Nanofiber production proceeded with PVP/GEL (50/50) and various concentrations of LEO. FT-IR results confirmed that LEO, PVP, and gelatin were incorporated in the chemical structure of the nanofibers. Generally, ultra-fine and uniform nanofibers were obtained, except when using pure PVP or PVP/GEL (50/50) including 8 wt % LEO. The finest fibers were obtained from PVP/GEL (100/0) (183 nm), and the most uniform fibers were obtained from PVP/GEL (50/50) (fiber diameter uniformity coefficient of 1.04). All nanofiber samples displayed unimodal distribution curves of histograms. While the addition of gelatin affected solution properties and average fiber diameter, the addition of LEO did not affect fiber properties.

Özet

Bu çalışmada, su içinde yağ emülsiyon elektro lif çekimi ilepolivinilpirolidon (PVP)/jelatin (GEL)/lavanta uçucu yağ (LEO) esaslınanolif üretilmesi amaçlanmıştır. Öncelikle; polimer çözeltiözelliklerinin ölçümü ve daha sonra nanolif üretim optimizasyonu venanolifli ağ yapının karakterizasyonu gerçekleştirilmiştir. PVPçözeltisine jelatin ilavesi ile viskozite artar iken, iletkenlik ve yüzeygerilimi azalmaktadır. Nano ağ kalitesi, lif çapı, çap üniformitesi vejelatin içeriği bakımından PVP/GEL (50/50) optimum numune olarakbelirlenmiştir. Çeşitli konsantrasyonlarda LEO içeren PVP/GEL(50/50)’den nanolif üretimine devam edilmiştir. FT-IR sonuçları,nanoliflerin kimyasal yapısında LEO, PVP ve jelatin varlığınıdoğrulamıştır. Saf PVP ve %8 LEO içeren PVP/GEL (50/50) hariç,genellikle oldukça ince ve üniform nanolifler elde edilmiştir. En incelifler PVP/GEL (100/0) (183 nm) çözeltisinden ve en üniform liflerPVP/GEL (50/50) (1.04 lif çapı üniformite katsayısı) çözeltisinden eldeedilmiştir. Tüm nanolif numunelerinin histogramında tek tepeli dağılımeğrileri elde edilmiştir. Jelatin ilavesi, çözelti özelliklerini ve ortalama lifçapını istatistiksel olarak etkilemiştir fakat LEO ilavesi lif özelliklerinietkilememiştir.

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Cite This Article

GÜLER, H. K., ÇALLIOĞLU, F. C. (2022). Production of essential oil-based composite nanofibers by emulsionelectrospinning. Pamukkale Üniversitesi Mühendislik Bilimleri Dergisi, Cilt: 26 - Sayı: 7, 1178–1185. https://ajindex.com/articles/587373

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References (12)

  1. Agarwal S, Greine A. “On the way to clean and safe electrospinning-green electrospinning: emulsion and suspension electrospinning”. Polymers for Advanced Technologies, 22, 372-378, 2011
  2. Hu J, Wei J, Liu W, Chen Y. “Preparation and characterization of electrospun PLGA/gelatin nanofibers as a drug delivery system by emulsion electrospinning”. Journal of Biomaterials Science, Polymer Edition, 24(8), 972-985, 2013
  3. Briggs T, Arinzeh TL. “Examining the formulation of emulsion electrospinning for improving the release of bioactive proteins from electrospun fibers”. Journal of Biomedical Materials Research Part A, 102, 674-684, 2014
  4. Kesici Güler H, Cengiz Çallıoğlu F, Sesli Çetin E. “Antibacterial PVP/cinnamon essential oil nanofibers by emulsion electrospinning”. The Journal of the Textile Institute, 110(2), 302-310, 2019
  5. Padil VVT, Wacławek S, Černík M. “Green Synthesis: Nanoparticles and Nanofibres Based on Tree Gums for Environmental Applications”. Ecological Chemistry and Engineering S, 23(4), 533-557, 2016
  6. Castilla-Casadiego DA, “’Green’ electrospinning of a collagen/hydroxyapatite composite nanofibrous scaffold”. MRS Communications, 6(4), 402-407, 2016
  7. Burke L, Mortimer CJ, Curtis DJ, Lewis AR, Williams R, Hawkins K, Wright CJ. “In-situ synthesis of magnetic ironoxide nanoparticle-nanofibre composites using electrospinning”. Materials Science & Engineering. C, Materials for Biological Applications, 70(1), 512-519, 2017
  8. Han D, Sasaki M, Yoshino H, Kofuji S, Sasaki AT, Steckl AJ. “In-vitro evaluation of MPA-loaded electrospun coaxial fiber membranes for local treatment of glioblastoma tumor cells”. Journal of Drug Delivery Science and Technology, 40, 45-50, 2017
  9. Gharib R, Najjar A, Auezova L, Charcosset C, Greige-Gerges H, “Interaction of Selected Phenylpropenes with Dipalmitoylphosphatidylcholine Membrane and Their Relevance to Antibacterial Activity”. The Journal of Membrane Biology, 250(3), 259-271, 2017
  10. Wang L, Chang MW, Ahmad Z, Zheng H, Li JS. “Mass and controlled fabrication of aligned PVP fibers for matrix type antibiotic drug delivery systems”. Chemical Engineering Journal, 307, 661-669, 2017
  11. Yu DG, Wang X, Li XY, Chian W, Li Y, Liao YZ. “Electrospun biphasic drug release polyvinylpyrrolidone/ethyl cellulose core/sheath nanofibers”. Acta Biomaterialia, 9(3), 5665-5672, 2013
  12. Jiang YN, Mo HY, Yu DG. “Electrospun drug-loaded core-sheath PVP/zein nanofibers for biphasic drug release”. Interna