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Journals / Fırat Üniversitesi Fen ve Mühendislik Bilimleri Dergisi / 2002 / Cilt: 14 - Sayı: 2

The synthesis of new substituted vic-dioxime ligands and their Co(II) and Co(III) complexes

Yeni substitue vic-dioksim ligandları ile Co(II) ve Co(III) komplekslerinin sentezi

Erdal CANPOLAT
Osman GÜNGÖR
Mehmet KAYA
Pages
115–121
Publication Date
2022-10-17
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

Using TGA techniques also carried out the thermal characterizations of ligands and their complexes.

📌 3 Key Takeaways

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Objective & Hypothesis:9,10-bis(hydroxyimino)-4,8,11,15-tetraaza-l,2,17,18-O-diizo-propilideneoktadekan $(H_2L^1)$ and l,2-di(hydroxyimino)-3,6-diaza-8,9-O-benzalnonane $(H_2L^2)$ ligands and their Co(II) and Co(III) complexes were synthesized.
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Key Findings & Data:Their structures were determined with IR, $^1H,^{13} C$-NMR spectroscopy, magnetic susceptibility and elemental analyses.
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Conclusion & Impact:Using TGA techniques also carried out the thermal characterizations of ligands and their complexes.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

9,10-bis(hydroxyimino)-4,8,11,15-tetraaza-l,2,17,18-O-diizo-propilideneoktadekan $(H_2L^1)$ and l,2-di(hydroxyimino)-3,6-diaza-8,9-O-benzalnonane $(H_2L^2)$ ligands and their Co(II) and Co(III) complexes were synthesized. Their structures were determined with IR, $^1H,^{13} C$-NMR spectroscopy, magnetic susceptibility and elemental analyses. Using TGA techniques also carried out the thermal characterizations of ligands and their complexes.

Özet

9,10-bis(hidroksiimino)-4,8,11,15-tetraaza-l,2,17,18-O-diizo-propilidenoktadekan $(H_2L^1)$ ve l,2-di(hidroksiimino)-3,6-diaza-8,9-O-benzalnonan $(H_2L^2)$ ligandları ve bu ligandların Co(II) ve Co(III) kompleksleri sentezlendi. Bunların yapıları, IR, $^1H,^{13}C$ NMR spektroskopisi, manyetik duyarlılık ve elementel analiz ile aydınlatıldı. Ayrıca ligand ve komplekslerin termal özellikleri TGA teknikleriyle karakterize edildi.

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Cite This Article

CANPOLAT, E., GÜNGÖR, O., KAYA, M. (2022). The synthesis of new substituted vic-dioxime ligands and their Co(II) and Co(III) complexes. Fırat Üniversitesi Fen ve Mühendislik Bilimleri Dergisi, Cilt: 14 - Sayı: 2, 115–121. https://ajindex.com/articles/513743

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