Comparison of the infrared and Raman spectra of $Ph_4P_2S_2$ and the complex has indicated that a chelate structure is most likely.
📌 3 Key Takeaways
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Objective & Hypothesis:Copper (I) chloride complex of tetraphenyldithioxodi -$lambda^5$ -phosphane (tetraphenyldiphosphine disulfide), $(CuCl.Ph_4P_2S_2)_n$, was synthesized by reacting equimolar quantities of anhydrous $CuCl_2$ and $Ph_4P_2S_2$ in freshly distilled acetone.
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Key Findings & Data:Copper (I) chloride complex of tetraphenyldithioxodi -$lambda^5$ -phosphane (tetraphenyldiphosphine disulfide), $(CuCl.Ph_4P_2S_2)_n$, was synthesized by reacting equimolar quantities of anhydrous $CuCl_2$ and $Ph_4P_2S_2$ in freshly distilled acetone.
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Conclusion & Impact:Comparison of the infrared and Raman spectra of $Ph_4P_2S_2$ and the complex has indicated that a chelate structure is most likely.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters
Abstract
Copper (I) chloride complex of tetraphenyldithioxodi -$lambda^5$ -phosphane (tetraphenyldiphosphine disulfide), $(CuCl.Ph_4P_2S_2)_n$, was synthesized by reacting equimolar quantities of anhydrous $CuCl_2$ and $Ph_4P_2S_2$ in freshly distilled acetone. Comparison of the infrared and Raman spectra of $Ph_4P_2S_2$ and the complex has indicated that a chelate structure is most likely.
Özet
Susuz $CuCl_2$ ile tetrafenilditiyoksodi-$lambda^5$ -fosfanın (tetrafenildifosfin disülfür), $Ph_4P_2S_2$, eş molar miktarları yeni damıtılmış asetonda tepkimeye sokularak, $(CuCl.Ph_4P_2S_2)_n$ sentezlendi. $Ph_4P_2S_2$ ve kompleksin kırmızı ötesi ve Raman spekrumlarının karşılaştırılması, şelat oluşumunun çok muhtemel olduğunu gösterdi.
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Cite This Article
ÇELEBİ, A., ÖZKALAY, Y., SARIKAHYA, Y. (2022). Tetrafenilditiyoksidi $lambda^5$-fosfan'ın (tetrafenildifosfin disülfür) bakır (I) klorür kompleksi. Ege University Journal of The Faculty of Science, Cilt: 21 - Sayı: 1, 61–67. https://ajindex.com/articles/496222