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Journals / Düzce Üniversitesi Bilim ve Teknoloji Dergisi / 2019 / Cilt: 7 - Sayı: 1

Production and characterization of Li 2 O-Al 2 O 3 -SiO 2 -NiO glass- ceramic

Li 2 O-Al 2 O 3 -SiO 2 -NiO cam-seramiğinin üretimi ve karakterizasyonu

Ömer KAYGILI
Pages
457–465
Publication Date
2022-10-12
DOI
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AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The morphology of the sample was investigated and no impurity in the sample was detected.

📌 3 Key Takeaways

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Objective & Hypothesis:In this study, a Li2O-Al2O3-SiO2-NiO glass-ceramic sample was produced using the conventional method and it was characterized by X-ray diffraction (XRD) analysis, Fourier transform infrared (FTIR) spectroscopy, differential thermal analysis (DTA), thermogravimetric analysis (TGA) and scanning electron microscopy (SEM) techniques.
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Key Findings & Data:The thermal behavior of the as-produced sample was investigated in the range of room temperature to 1000 °C.
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Conclusion & Impact:The morphology of the sample was investigated and no impurity in the sample was detected.
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

In this study, a Li2O-Al2O3-SiO2-NiO glass-ceramic sample was produced using the conventional method and it was characterized by X-ray diffraction (XRD) analysis, Fourier transform infrared (FTIR) spectroscopy, differential thermal analysis (DTA), thermogravimetric analysis (TGA) and scanning electron microscopy (SEM) techniques. It was seen that the sample has the biphasic polycrystalline structure. The bands belonging to the vibration modes of Si-O-Si ve Si-O-Al bonds were observed in the FTIR spectrum. The thermal behavior of the as-produced sample was investigated in the range of room temperature to 1000 °C. The morphology of the sample was investigated and no impurity in the sample was detected.

Özet

Bu çalışmada, Li 2 O-Al 2 O 3 -SiO 2 -NiO cam-seramik numunesi geleneksel yöntem kullanılarak üretildi ve X-ışınıkırınımı (XRD) analizi, Fourier dönüşümlü kızılötesi (FTIR) spektroskopisi, diferansiyel termal analiz (DTA),termogravimetrik analiz (TGA) ve taramalı elektron mikroskopisi (SEM) teknikleri kullanılarak karakterizeedildi. Numunenin iki fazlı çok kristalli bir yapıya sahip olduğu görüldü. Si-O-Si ve Si-O-Al bağlarının titreşimmodlarına ait bantlar FTIR spektrumunda gözlendi. Üretilen numunenin oda sıcaklığı ile 1000 °C aralığındatermal davranışı araştırıldı. Numunenin morfolojisi incelendi ve numune içerisinde bir safsızlık tespit edilmedi.

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Cite This Article

KAYGILI, Ö. (2022). Production and characterization of Li 2 O-Al 2 O 3 -SiO 2 -NiO glass- ceramic. Düzce Üniversitesi Bilim ve Teknoloji Dergisi, Cilt: 7 - Sayı: 1, 457–465. https://ajindex.com/articles/494363

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References (10)

  1. P.W. McMillan, Non-metallic Solids: Glass-ceramics, 1st Edition,
  2. London, England: Academic Press, 1964, p. 1. E.D. Zanotto, “A bright future for glass-ceramics,” American Ceramic Society Bulletin, vol. 89, no. 8, pp. 19-27, 2010. Ö. Kaygılı, “Radyasyonun cam-seramik maddelerin kristalleşme ve mekanik özellikleri üzerine etkisi,” Yüksek lisans tezi, Fizik Bölümü, Fırat Üniversitesi,
  3. Elazığ, Türkiye, 2005.
  4. S. Barbi, P. Miselli, and C. Siligardi, “Failure analysis of glazed LAS glass-ceramic containing cerium oxide,” Ceramics International, vol. 43, no. 1, pp. 1472-1478, 2017.
  5. R. Krsmanovic, S. Bals, G. Bertoni, and G.V. Tendeloo, “Structural characterization of Er- doped Li 2 O-Al 2 O 3 -SiO 2 glass ceramics,” Optical Materials, vol. 30, no. 7, pp. 1183-1188, 2008. O. Kaygili, and H. Yavuz, “The effects of gamma irradiation on non-isothermal crystallization kinetics and microhardness of the Li 2 O-Al 2 O 3 -SiO 2 glass–ceramic,” Journal of Thermal Analysis and Calorimetry, vol. 102, no. 2, pp. 681-684, 2010. Z. Qing, “The effects of B 2 O 3 on the microstructure and properties of lithium aluminosilicate glass-ceramics for LTCC applications,” Materials Letters, vol. 212, pp. 126-129, 2018. T. Yang, and S. Liu, “Li 2 O-Al 2 O 3 -SiO 2 glass–ceramic coating on a porous silica ceramic substrate,” Journal of Alloys and Compounds, vol. 600, pp. 51-54, 2014.
  6. B. Li, S. Wang, and Y. Fang, “Effect of Cr 2 O 3 addition on crystallization, microstructure and properties of Li 2 O-Al 2 O 3 -SiO 2 glass-ceramics,” Journal of Alloys and Compounds, vol. 693, pp. 9-15, 2017. X. Guo, and H. Yang, “Effects of fluorine on crystallization, structure and performances of lithium aluminosilcate glass ceramic,” Materials Research Bulletin, vol. 41, no. 2, pp. 396-405, 2006.
  7. L. Lilensten, Q. Fu, B.R. Wheaton, A.J. Credle, R.L. Stewart, and J.T. Kohli, “Kinetic study on lithium-aluminosilicate (LAS) glass-ceramics containing MgO and ZnO,” Ceramics International, vol. 40, no. 8, pp. 11657-11661, 2014.
  8. A.M. Hu, K.M. Liang, F. Zhou, G.L. Wang, and F. Peng, “Phase transformations of Li 2 O- Al 2 O 3 -SiO 2 glasses with CeO 2 addition,” Ceramics International, vol. 31, no. 1, pp. 11-14, 2005.
  9. I. Alekseeva, O. Dymshits, M. Tsenter, and A. Zhilin, “Influence of various alkali and divalent metal oxides on phase transformations in NiO-doped glasses of the Li 2 O-Al 2 O 3 -SiO 2 -TiO 2 system,” Journal of Non-Crystalline Solids, vol. 357, no. 11-13, pp. 2209-2214, 2011.
  10. P. Lu, Y. Zheng, J. Cheng