Journals / Cumhuriyet Science Journal / 2017 / Cilt: 38 - Sayı: 4

Improvement of Affecting Parameters to Synthesis Grafene Oxide by Hummer Method)

Grafen Oksitin Hummers Metodu ile Sentezlenmesine Etki Eden Parametrelerin İyileştirilmesi

Pages
674–680
Publication Date
2022-10-12
DOI
—
🏛️Bibliographic metadata and full text access for this article are provided via DergiPark.
DergiPark Record ↗
✨

AI Summary & Key Takeaways

AI Insight
⚡ TL;DR(Too Long; Didn't Read)

The characterization analyses of this obtained products were made

📌 3 Key Takeaways

🎯
Objective & Hypothesis:This study contains observation of parameters that affect the synthesis of graphene oxide by using of chemically Hummers Method.
📊
Key Findings & Data:The Hummers parameters such as acid type and rate, amount of KMnO4 and H2O2, temperature and mixing time were changed and approximately 44 graphene oxide products were synthesized.
💡
Conclusion & Impact:The characterization analyses of this obtained products were made
🔬Design:Research Article
📍Scope:Comprehensive Sample
⚙️Variables:Domain Parameters

Abstract

This study contains observation of parameters that affect the synthesis of graphene oxide by using of chemically Hummers Method. In this respect, it is aimed to determination of parameters that affects the synthesis of the graphene oxide such as duration, quality and chemical substance amount. The Hummers parameters such as acid type and rate, amount of KMnO4 and H2O2, temperature and mixing time were changed and approximately 44 graphene oxide products were synthesized. The characterization analyses of this obtained products were made

Özet

Bu çalışmada, kimyasal bir yöntem olan Hummers metodu ile Grafen oksitin sentezlenmesine etki eden parametreler araştırılmıştır. Bu kapsamda Hummers metodu kullanılarak Grafen oksitin kısa sürede, daha kaliteli ve daha az kimyasal madde kullanılarak sentezlenmesine etki eden parametrelerin belirlenmesi amaçlanmıştır. Bu amaçla asit tipi, asit miktarı, KMnO4 miktarı, H2O miktarı, sıcaklık ve karıştırma süresi gibi Hummers metodu parametreleri değiştirilerek yaklaşık 44 adet grafen oksit sentezlenmiş ve bu ürünlerin bir kısmının karakterizasyon analizleri yapılmıştır. Karakterizasyon analizi sonunda, grafen oksitin en iyi hangi koşullarda sentezleneceğine karar verilmiştir

🔖

Cite This Article

TEMEL, Ü. N., TEMEL, N. K., METHOD, H., SERTAKAN, K. (2022). Improvement of Affecting Parameters to Synthesis Grafene Oxide by Hummer Method). Cumhuriyet Science Journal, Cilt: 38 - Sayı: 4, 674–680. https://ajindex.com/articles/478067

📄 Full Text PDF Viewer

📄

PDF görüntüleyici hazırlanıyor...

References (1)

  1. . Jannathul Firdhouse M., Lalitha P. Ecofriendly synthesis of graphene using the aqueous extract of Amaranthus dubius. Carbon - Sci. Tech.,2013; 5: 253-259. [2]. Kozal B. Karbon Tabanlı Petek Örgülerin Elektronik Özellikleri, doktora tezi, 2012. [3]. Allen M.J., Tung V.C., Kaner R.B. Honeycomb carbon: a review of graphene. Chem. Rev. 2010; 110: 132-145. [4]. Choi W., Lahiri I., Seelaboyina R., Kang Y.S. Synthesis of graphene and its applications: a review. Crit. Rev. Solid. State. Mater. Sci. 2010; 35: 52-71. [5]. Zhu Y., Murali S., Cai W. Graphene and graphene oxide: synthesis, properties, and applications. Adv. Mater. 2010; 22: 3906- 3924. [6]. Choi W., Lee, J. Graphene synthesis and applications. CRC Press/Taylor&Francis Group, Boca Raton. 2012. [7]. Van bommel A.J. Crombeen J.E., Van Tooren A., LEED and Auger electron observations of the SiC(0001) surface, Surface Science 1975; 48: 463-472. [8]. Juang Z.Y, Wu C.Y., Lo C.W., Chen W.Y., Huang C.F., Hwang J.C., Chen F.R., Leou K.C., Tsai C.H., Synthesis of graphene on silicon carbide substrates at low temperature. Carbon 2009; 47: 2026-2031. [9]. Wu W., Liu Z., Jauregui L.A., Yu Q., Pillai R., Cao H., Bao J., Chen Y.P., Pei S.S. Wafer-scale synthesis of graphene by chemical vapor deposition and its application in hydrogen sensing, Sensors and Actuators B: Chemical, 2010; 150: 296- 300. [10]. Wang G., Wang B., Park J., Wang Y., Sun B., Yao J. Highly efficient and large-scale synthesis of graphene by electrolytic exfoliation. Carbon 2009; 47: 3242-3246. [11]. Brodie B.C. On the atomic weight of graphite. Philos. Trans. R. Soc. London 1859;14: 249-259. [12]. Staudenmaier L. Verfahren zur Darstellung der Graphitsa¨ure. Ber. Dtsch. Chem. Ges. 1898; 31: 1481-1487. [13]. Hummers W.S. Offeman, R. E. Preparation of graphitic oxide. J. Am. Chem. Soc. 1958; 80:1339-1339. [14]. Karteri İ., Karataş Ş., Al-Ghamdi A., Yakuphanoğlu F. The electrical characteristics of thin film transistors with graphene oxide and organic insulators. Synthetic Metals 2015;199: 241-245. [15]. Hanifah M.F.R., Jaafar J., Aziz M., Ismail A.F., Rahman M.A., Othman M.H.D. Synthesis of Graphene Oxide Nanosheets via Modified Hummers Method and Its Physicochemical Properties. Jurnal Teknologi 2015; 74: 189-192.